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11. 发明授权

US06500879B1 Dental composition and method 失效
标题翻译：牙科成分及方法
公开(公告)号：US06500879B1
公开(公告)日：2002-12-31
申请号：US08259833
申请日：1994-06-15
申请人： Chin-Teh Huang , Kewang Lu , Mingxin Fan , Paul Hammesfahr
发明人： Chin-Teh Huang , Kewang Lu , Mingxin Fan , Paul Hammesfahr
IPC分类号： A61K6083
CPC分类号： C07C69/92 , A61C5/66 , A61K6/0017 , A61K6/0023 , A61K6/083 , A61K6/0835 , C08L33/00 , C08L43/02
摘要： The invention provides dental cement compositions and methods of using them for binding hard tooth material, metal and ceramic. The cement compositions include shelf stable complexes of ethylenically unsaturated monomers reacted with cations. The cements have superior adhesion to tooth without separately acid etching dentin or enamel. Compositions of are useful as dental luting cements, liners, pit and fissure seal bases and restoratives.
摘要翻译：本发明提供了牙科用水泥组合物及其用于结合硬质牙科材料，金属和陶瓷的方法。水泥组合物包括与阳离子反应的烯属不饱和单体的稳定的络合物。水泥具有优异的牙齿附着力，无需单独酸蚀牙本质或牙釉质。作为牙科用水泥，衬垫，坑和裂缝密封基座和修复体的组合物是有用的。

12. 发明授权

US5767150A Cycloaliphatic epoxide compounds 失效
标题翻译：环脂族环氧化合物
公开(公告)号：US5767150A
公开(公告)日：1998-06-16
申请号：US831677
申请日：1997-04-10
申请人： Mingxin Fan , Gary W. Ceska , James Horgan , Henri Strub
发明人： Mingxin Fan , Gary W. Ceska , James Horgan , Henri Strub
IPC分类号： C07D301/12 , C07D303/16 , C07D303/40 , C08G59/24 , C08G59/32 , A61K31/335 , C07D303/00
CPC分类号： C08G59/24 , C07D301/12 , C07D303/16 , C07D303/40 , C08G59/3218
摘要： Compounds having the formula ##STR1## wherein X is selected from O, (CH.sub.2).sub.m O, S, (CH.sub.2).sub.m S, NH, (CH.sub.2).sub.m NH, COO.sup.-, (CH.sub.2).sub.m COO.sup.-, .sup.- OOC and .sup.- OOC (CH.sub.2).sub.m ; m is 1 to 6; n is 1 to 100; R.sub.1 is (C.sub.1 -C.sub.20) ester; and A is a saturated organic linking group selected from residues of polyol, polythiol, polyamine, and polyacid, are prepared by reacting compounds according to formula II ##STR2## with hydrogen peroxide in the presence of (a) tungstic acid or its metal salts, (b) phosphoric acid or its metal salts, and (c) at least one phase transfer catalyst.
摘要翻译：具有式（I）的化合物其中X选自O，（CH 2）m O，S，（CH 2）m S，NH，（CH 2）m NH，COO-，（CH 2）m COO-， - OOC和 -OOC（CH 2）m; m为1〜6; n为1〜100; R1是（C1-C20）酯; 并且A是选自多元醇，多硫醇，多胺和多元酸的残基的饱和有机连接基团，其通过使式II（II）的化合物与（a）钨酸或其金属盐，（b）磷酸或其金属盐，和（c）至少一种相转移催化剂。

13. 发明授权

US06559260B1 Allyl urethane resin compositions 有权
标题翻译：烯丙基聚氨酯树脂组合物
公开(公告)号：US06559260B1
公开(公告)日：2003-05-06
申请号：US09535176
申请日：2000-03-27
申请人： Mingxin Fan , Gary W. Ceska , James Horgan
发明人： Mingxin Fan , Gary W. Ceska , James Horgan
IPC分类号： C08L7516
CPC分类号： C09D175/16 , C08G18/6715
摘要： The present invention is for a new class of allyl urethane resin which can be cured with peroxide at high temperature alone or in combination with some accelerators. These allyl urethane resins can be sued alone or in combination with other free radically polymerizable materials such as allyl monomers and ligomers or (meth)acrylate monomers and oligomers. These new allyl urethane resins contain at least two allyl functional groups.
摘要翻译：本发明是一种新的烯丙基聚氨酯树脂，其可以单独或与一些加速剂组合使用，可以在高温下用过氧化物固化。这些烯丙基聚氨酯树脂可以单独或与其它可自由基聚合的材料如烯丙基单体和连接体或（甲基）丙烯酸酯单体和低聚物组合起来。这些新的烯丙基聚氨酯树脂含有至少两个烯丙基官能团。

14. 发明授权

US06124418A Selective catalysts for the synthesis of epoxysilicone monomers and polymers 失效
标题翻译：用于合成环氧硅氧烷单体和聚合物的选择性催化剂
公开(公告)号：US06124418A
公开(公告)日：2000-09-26
申请号：US195897
申请日：1994-02-14
申请人： James Vincent Crivello , Mingxin Fan
发明人： James Vincent Crivello , Mingxin Fan
IPC分类号： C07F7/08 , C07F7/18 , C08G77/38 , C08G77/06 , C08G77/08
CPC分类号： C07F7/0829 , C07F7/0879 , C07F7/1876 , C08G77/38
摘要： The invention provides a method for making a curable epoxysilicone composition through the hydrosilation reaction between an ethylenically unsaturated epoxide and an SiH-containing silicone to produce an epoxysilicone product, and catalyzed by a quaternary ammonium, phosphonium or arsonium hexahaloplatinate which does not promote the oxirane ring-opening reaction of either the ethylenically unsaturated epoxide starting material or the epoxysilicone product. The invention also provides for a curable epoxysilicone composition made by the above method.
摘要翻译：本发明提供一种通过烯键式不饱和环氧化物和含SiH的硅氧烷之间的硅氢化反应制备可固化环氧硅氧烷组合物以制备环氧硅氧烷产物的方法，并且通过不促进环氧乙烷环的季铵，鏻或六卤化钌催化烯键式不饱和环氧化物起始材料或环氧硅氧烷产物的开环反应。本发明还提供了通过上述方法制备的可固化环氧硅氧烷组合物。

15. 发明授权

US6084111A Method for making cycloaliphatic epoxides 失效
标题翻译：制备脂环族环氧化物的方法
公开(公告)号：US6084111A
公开(公告)日：2000-07-04
申请号：US62593
申请日：1998-04-17
申请人： Mingxin Fan , Gary W. Ceska , James Horgan , Henri Strub
发明人： Mingxin Fan , Gary W. Ceska , James Horgan , Henri Strub
IPC分类号： C07D301/12 , C07D303/16 , C07D303/40 , C08G59/24 , C08G59/32 , C07D303/00
CPC分类号： C08G59/24 , C07D301/12 , C07D303/16 , C07D303/40 , C08G59/3218
摘要： Compounds having the formula ##STR1## wherein X is selected from O, (CH.sub.2).sub.m O, S, (CH.sub.2).sub.m S, NH, (CH.sub.2).sub.m NH, COO.sup.-, (CH.sub.2).sub.m COO.sup.-, .sup.- OOC and .sup.- OOC (CH.sub.2).sub.m ;m is 1 to 6;n is 1 to 100;R.sub.1 is selected from H, (C.sub.1 -C.sub.20) alkyl, (C.sub.1 -C.sub.20) alkoxy and (C.sub.1 -C.sub.20) ester; andA is a saturated organic linking group selected from residues of polyol, polythiol, polyamine, and polyacid, are prepared by reacting compounds according to formula II ##STR2## with hydrogen peroxide in the presence of (a) tungstic acid or its metal salts, (b) phosphoric acid or its metal salts, and (c) at least one phase transfer catalyst.
摘要翻译：具有下式的化合物其中X选自O，（CH 2）m O，S，（CH 2）m S，NH，（CH 2）m NH，COO-，（CH 2）m COO-， - OOC和-OOC（CH 2）m; m为1〜6; n为1〜100; R1选自H，（C1-C20）烷基，（C1-C20）烷氧基和（C1-C20）酯; （a）钨酸或其金属盐的存在下，通过使根据式II的化合物与过氧化氢反应制备A是选自多元醇，多硫醇，多胺和多元酸的残基的饱和有机连接基团，（b）磷酸或其金属盐，以及（c）至少一种相转移催化剂。

16. 发明授权

US5763629A Alkoxylated glycidyl (meth)acrylates and method of preparation 失效
标题翻译：（甲基）丙烯酸缩水甘油酯及其制备方法
公开(公告)号：US5763629A
公开(公告)日：1998-06-09
申请号：US772979
申请日：1996-12-23
申请人： Mingxin Fan , Gary W. Ceska , James Horgan , Thomas W. Hazell
发明人： Mingxin Fan , Gary W. Ceska , James Horgan , Thomas W. Hazell
IPC分类号： C07D303/16 , C08F20/32 , C08G65/14 , C08L71/02 , C07D301/12
CPC分类号： C08G65/14 , C07D303/16 , C08F20/32 , C08L71/02
摘要： Compounds of the formula ##STR1## wherein R.sub.1 32 H, CH.sub.3 ; R.sub.2 =H, (C.sub.1 -C.sub.6)alkyl; and x=1-20; and process for preparing such compounds by reacting a compound of the formula ##STR2## with hydrogen peroxide in the presence of (a) tungstic acid or its metal salts, (b) phosphoric acid or its metal salts, and (c) at least one phase transfer catalyst.
摘要翻译：式（I）的化合物其中R 13 2 H，CH 3; R2 = H，（C1-C6）烷基; 和x = 1-20; 和（a）钨酸或其金属盐，（b）磷酸或其金属盐的存在下，使式（II）化合物与过氧化氢反应制备此类化合物的方法，和（c）至少一种相转移催化剂。

17. 发明授权

US06469071B1 Radiation curable acrylate-terminated polymers having polycarbonate repeating units 有权
标题翻译：具有聚碳酸酯重复单元的可辐射固化的丙烯酸酯封端聚
公开(公告)号：US06469071B1
公开(公告)日：2002-10-22
申请号：US09835240
申请日：2001-04-13
申请人： Mingxin Fan , Gary Ceska , James Horgan , Robert Adams , William Schaeffer , Josh Oliver
发明人： Mingxin Fan , Gary Ceska , James Horgan , Robert Adams , William Schaeffer , Josh Oliver
IPC分类号： C08F248
CPC分类号： C08G64/045 , C08F299/0492 , C08G64/42 , C09D169/00 , Y10T428/249982 , Y10T428/31504 , Y10T428/31507 , Y10T428/31786 , Y10T428/31826 , Y10T428/31855
摘要： Polyester based polycarbonate (meth)acrylates prepared by the reaction of a alkylene or arylene diol polycarbonate with an anhydride or its dicarboxylic acid to form a carboxyl terminated diester, reacting the diester with a diglycidyl ether and an acrylic or methacrylic acid to form an acrylate terminate polymer which is useful for radiation cured coatings which have superior adhesion and reverse impact strength when applied to plastic substrates.
摘要翻译：通过亚烷基或亚芳基二醇聚碳酸酯与酸酐或其二羧酸的反应制备的聚酯基聚碳酸酯（甲基）丙烯酸酯以形成羧基封端的二酯，使二酯与二缩水甘油醚和丙烯酸或甲基丙烯酸反应形成丙烯酸酯末端可用于辐射固化涂层的聚合物，其在施加到塑料基材上时具有优异的粘附性和反冲击强度。

18. 发明授权

US06451958B1 Radiation curable acrylate-terminated polymers having polycarbonate repeating units 有权
标题翻译：具有聚碳酸酯重复单元的可辐射固化的丙烯酸酯封端的聚合物
公开(公告)号：US06451958B1
公开(公告)日：2002-09-17
申请号：US09932559
申请日：2001-04-06
申请人： Mingxin Fan , Gary Ceska , James Horgan
发明人： Mingxin Fan , Gary Ceska , James Horgan
IPC分类号： C08G6400
CPC分类号： C09D175/16 , C08G18/672 , Y10T428/31504 , Y10T428/31507 , Y10T428/31551 , C08G18/44
摘要： Polymer having repeating polycarbonate moieties of the formula (I) (Acr)y(A)(Q)(PC)[(Q)(PC)]x(Q)(A)(Acr)y (I) wherein (Acr)y(A) is the residue of hydroxyalkyl acrylate or hydroxyalkyl methacrylate having an alkyl moiety, A, and where said alkyl, A, has 2 to 5 carbon atoms and wherein Acr is an acrylate or methacrylate moiety; Q is the residue of one or more organic polyisocyantes which are connected with A via a urethane linkage; PC is the residue of an alkylene diol polycarbonate of the formula (II) HO(ROCOO)nROH (II) R is one or more (C2 to C10) alkylene or one or more (C6 to C12) aromatic group; y is an integer from 1 to 5; x is from 1 to 20; PC and Q are connected via a urethane group. The acrylate terminate polymers are useful for radiation cured coatings which have superior adhesion and reverse impact strength, especially when applied to plastic substrates.
摘要翻译：具有式（I）的重复聚碳酸酯部分的聚合物其中（Acr）y（A）是具有烷基部分A的丙烯酸羟烷基酯或甲基丙烯酸羟烷基酯的残基，并且其中所述烷基A具有2至5个碳原子，其中 Acr是丙烯酸酯或甲基丙烯酸酯部分; Q是通过氨基甲酸酯键与A连接的一种或多种有机聚异氰酸酯的残基; PC是式（II）的亚烷基二醇聚碳酸酯的残基R是一个或多个（C2 至C10）亚烷基或一个或多个（C6至C12）芳族基团; y为1至5的整数; x为1至20; PC和Q通过氨基甲酸酯基团连接。丙烯酸酯末端聚合物可用于辐射具有优异的附着力和反冲击强度的固化涂层，特别是当应用于塑料基材时。

19. 发明授权

US06391463B1 Silicon-containing alkoxylated (meth)acrylate monomers 失效
标题翻译：含硅烷氧基化（甲基）丙烯酸酯单体
公开(公告)号：US06391463B1
公开(公告)日：2002-05-21
申请号：US08772980
申请日：1996-12-23
申请人： Mingxin Fan , Gary W. Ceska , James Horgan , Thomas Hazell
发明人： Mingxin Fan , Gary W. Ceska , James Horgan , Thomas Hazell
IPC分类号： C08F3008
CPC分类号： C08F30/08 , C07F7/081 , C07F7/12 , C07F7/1804 , C09D4/00 , Y10T428/31663 , C08F230/08
摘要： Compounds of the formula wherein R1=H, CH3 R2=H, CH3, CH2CH3, or CH2CH2CH3 n=1-10 X=halogen, (C1-C6) alkyl, (C1-C6) alkoxy, or aromatic radical are shown to be useful as coupling agents or adhesion promotors in free radically curable compositions such as UV curable and peroxide curable (meth)acrylate based coating compositions. The associated methods, curable compositions, coatings, adhesives and coated articles are also disclosed.
摘要翻译：化合物R1 = H，CH3R2 = H，CH3，CH2CH3或CH2CH2CH3n = 1-10X =卤素，（C1-C6）烷基，（C1-C6）烷氧基或芳族基团可用作偶联剂或可自由基固化组合物中的粘合促进剂，例如UV可固化和可过氧化物固化的（甲基）丙烯酸酯基涂料组合物。还公开了相关方法，可固化组合物，涂料，粘合剂和涂覆制品。

20. 发明授权

US06380278B1 Polyurethane salts 失效
标题翻译：聚氨酯盐
公开(公告)号：US06380278B1
公开(公告)日：2002-04-30
申请号：US09932560
申请日：2001-01-19
申请人： Mingxin Fan , Xiaoxing Chuck Dong , Jeffrey Allan Klang , James Horgan , Gary W. Ceska
发明人： Mingxin Fan , Xiaoxing Chuck Dong , Jeffrey Allan Klang , James Horgan , Gary W. Ceska
IPC分类号： C08G1830
CPC分类号： C08G18/34 , C08G18/672
摘要： A urethane (meth)acrylate metal salt obtained by reacting (A) one or more polyisocyanates, (B) one or more hydroxy functional (meth)acrylates, and (C) one or more metal salt polyols which are the reaction product of a metal oxide and a half ester containing a hydroxy group and a carboxylic acid group. Processes of preparing such salts and polymers prepared from such salts are also disclosed. The polymers are useful for coating and adhesive compositions prepared by radiation or peroxide curing processes.
摘要翻译：通过使（A）一种或多种多异氰酸酯，（B）一种或多种羟基官能（甲基）丙烯酸酯和（C）一种或多种金属盐多元醇反应得到的氨基甲酸酯（甲基）丙烯酸酯金属盐，氧化物和含有羟基和羧酸基团的半酯。还公开了由这些盐制备这种盐和聚合物的方法。聚合物可用于通过辐射或过氧化物固化方法制备的涂料和粘合剂组合物。

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