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11. 发明授权

US5100939A Bituminous compositions and method of making 失效
标题翻译：沥青组合物和制造方法
公开(公告)号：US5100939A
公开(公告)日：1992-03-31
申请号：US647954
申请日：1991-01-30
申请人： John F. Vitkuske , Lu H. Tung , Ronald R. Pelletier , Ronald E. Snyder , William A. Gros
发明人： John F. Vitkuske , Lu H. Tung , Ronald R. Pelletier , Ronald E. Snyder , William A. Gros
IPC分类号： C08L95/00
CPC分类号： C08L95/00
摘要： Disclosed are bituminous blends having improved toughness and elasticity. The blends contain a bituminous binder and a tapered block copolymer formed from a monovinyl aromatic compound and a conjugated diene. Suitable tapered block copolymers include a tapered A-B-A type block copolymer of the A-t-B-t-A configuration, particularly those having an isolated monovinyl aromatic compound content of about 20 to about 90 weight percent, and tapered A-B-A type block copolymers of the A-B-t-A configuration having an isolated monovinyl aromatic compound content of about 20 to about 90 weight percent of the total monovinyl aromatic compound in the tapered block copolymer. Further disclosed is a method of making the blends. Further disclosed is a tapered A-B-A type block copolymer having an isolated monovinyl aromatic compound content of about 29 to about 75 weight percent.
摘要翻译：公开了具有改进的韧性和弹性的沥青混合物。共混物含有沥青粘合剂和由单乙烯基芳族化合物和共轭二烯形成的渐缩嵌段共聚物。合适的锥形嵌段共聚物包括AtBtA构型的锥形ABA型嵌段共聚物，特别是具有约20至约90重量％的单一乙烯基芳族化合物含量的渐缩ABA型嵌段共聚物和具有分离的单乙烯基芳族化合物的ABtA构型的锥形ABA型嵌段共聚物含量为锥形嵌段共聚物中总单乙烯基芳族化合物的约20至约90重量％。进一步公开了制备共混物的方法。进一步公开了具有约29-约75重量％的分离的单乙烯基芳族化合物含量的锥形A-B-A型嵌段共聚物。

12. 发明授权

US5688842A Process for preparing high internal phase ratio emulsions and latexes derived thereof 失效
标题翻译：制备高内相比乳液和衍生自其的胶乳的方法
公开(公告)号：US5688842A
公开(公告)日：1997-11-18
申请号：US630187
申请日：1996-04-10
申请人： James E. Pate, III , Nanette E. Lutenske , James Peters , Ronald R. Pelletier
发明人： James E. Pate, III , Nanette E. Lutenske , James Peters , Ronald R. Pelletier
IPC分类号： B01F3/08 , B01F15/04 , B01J13/00 , C08J3/03 , C08J3/09 , C08J3/02
CPC分类号： B01J13/0086 , B01J13/00 , C08J3/03 , C08J3/09 , Y10S516/929
摘要： The present invention is a method of preparing a high internal phase ratio emulsion without phase inversion comprising the steps of: a) continuously merging into a disperser and in the presence of an emulsifying and a stabilizing amount of a surfactant, a continuous phase liquid stream having a flow rate R.sub.1, and a disperse phase liquid stream having a flow rate R.sub.2 ; and b) mixing the merged streams with a sufficient amount of shear, and with R.sub.2 :R.sub.1 sufficiently constant, to form the high internal phase ratio emulsion without phase inversion or stepwise distribution of an internal phase into an external phase; wherein R.sub.2 :R.sub.1 encompasses a range, the lower limit of which range being defined by a point where the volume average particle size of the high internal phase ratio emulsion begins to show an inverse dependence on R.sub.2 :R.sub.1, and wherein the upper limit of which range is just less than an R.sub.2 :R.sub.1 where a phase inversion of the high internal phase ratio emulsion takes place. Monodisperse submicron particles can be prepared using the process of the present invention. Useful latexes can be prepared from these high internal phase ratio emulsions.
摘要翻译：本发明是一种制备不含相转化的高内相比乳液的方法，包括以下步骤：a）连续合并到分散器中，并在乳化剂和稳定剂量的表面活性剂存在下，连续相液体流具有流量R1和具有流量R2的分散相液体流; 和b）将合并的流与足够量的剪切混合，并使R2：R1充分恒定，以形成高内相比乳液，而不会内相逐步分配到外相中; 其中R2：R1包含一个范围，其下限限定在高内相比乳液的体积平均粒径开始显示与R2:R1的反相关性的点，其中其上限范围小于R2：R1，其中发生高内相比乳液的相转化。可以使用本发明的方法制备单分散亚微米颗粒。可以从这些高内相比乳液制备有用的胶乳。

13. 发明授权

US5578674A High-strength films of block copolymer latices 失效
标题翻译：高强度嵌段共聚物胶片
公开(公告)号：US5578674A
公开(公告)日：1996-11-26
申请号：US469184
申请日：1995-06-05
申请人： David R. Speth , Brian W. Walther , Ronald R. Pelletier
发明人： David R. Speth , Brian W. Walther , Ronald R. Pelletier
IPC分类号： B29C41/00 , B29C71/02 , B29D7/01 , C08J3/03 , C08J5/18 , C08L53/02 , B29D7/00 , C08K5/01 , C08L53/00
CPC分类号： C08J5/18 , B29C41/003 , B29D7/01 , C08J3/03 , C08L53/02 , C08L53/025 , B29C71/02 , B29K2009/06 , B29K2096/04 , B29K2105/0064 , C08J2353/02
摘要： What is claimed is a coherent, elastomeric, solid, free-standing film comprising an organic phase comprising: (a) one or more block copolymer(s) corresponding to the formula:A--B--X.sub.m --(B--A).sub.nwherein each A is a polymer block consisting essentially of a monovinylidene aromatic monomer, each B is a polymer block consisting essentially of a conjugated diene and, optionally, a monovinylidene aromatic monomer, X is the remnant of a multifunctional coupling agent, m is 0 or 1, and n is an integer from 1 to 5, each monovinylidene aromatic monomer block having a weight average molecular weight from about 8,000 to about 15,000 Daltons, each conjugated diene block having a weight average molecular weight from about 30,000 to about 200,000 Daltons, and (b) optionally, an extender which is compatible with the B block; wherein the A block comprises 5 to 25 percent by weight of the organic phase and exhibits an effective phase volume in the organic phase from about 5 to about 20 percent and the amount of extender present is sufficient to achieve the desired effective phase volume of the A block, wherein the film is annealed and demonstrates a tensile strength of 11.0 MPa or greater.
摘要翻译：所要求保护的是一种包含有机相的相干，弹性体，固体，自立膜，其包含：（a）一个或多个相应于下式的嵌段共聚物：AB-Xm-（BA）n，其中每个A是聚合物基本上由单亚乙烯基芳族单体组成的嵌段，每个B是基本上由共轭二烯和任选的单亚乙烯基芳族单体组成的聚合物嵌段，X是多官能偶联剂的残余物，m是0或1，n是 1至5的整数，每个单亚乙烯基芳族单体嵌段具有约8,000至约15,000道尔顿的重均分子量，每个共轭二烯嵌段的重均分子量为约30,000至约200,000道尔顿，和（b）任选地，与B块兼容的扩展器; 其中A嵌段占有机相的5〜25重量％，有机相的有效相体积约为5〜20％，而且存在的增量剂的量足以达到所需有效相体积的A 块，其中所述膜退火并显示出11.0MPa或更大的拉伸强度。

14. 发明授权

US5100938A Bituminous compositions and methods of application to surfaces 失效
标题翻译：沥青组合物和应用于表面的方法
公开(公告)号：US5100938A
公开(公告)日：1992-03-31
申请号：US647955
申请日：1991-01-30
申请人： John F. Vitkuske , Lu H. Tung , Ronald R. Pelletier , Ronald E. Snyder , William A. Gros
发明人： John F. Vitkuske , Lu H. Tung , Ronald R. Pelletier , Ronald E. Snyder , William A. Gros
IPC分类号： C08L95/00
CPC分类号： C08L95/005
摘要： Disclosed are bituminous blends having improved toughness and elasticity. The blends contain an emulsion of a bituminous binder and an emulsion of a tapered block copolymer formed from a monovinyl aromatic compound and a conjugated diene. Suitable tapered block copolymers include a tapered A-B-A type block copolymer of the A-t-B-t-A configuration, particularly those having an isolated monovinyl aromatic compound content of about 20 to about 90 weight percent, and tapered A-B-A type block copolymers of the A-B-t-A configuration having an isolated styrene content of about 20 to about 90 weight percent of the total monovinyl aromatic compound in the tapered block copolymer. Also disclosed is a method of applying the blends to various surfaces.
摘要翻译：公开了具有改进的韧性和弹性的沥青混合物。共混物含有沥青粘合剂的乳液和由单乙烯基芳族化合物和共轭二烯形成的锥形嵌段共聚物的乳液。合适的锥形嵌段共聚物包括AtBtA构型的锥形ABA型嵌段共聚物，特别是具有约20至约90重量％的单一乙烯基芳族化合物含量的渐缩ABA型嵌段共聚物，以及具有分离的苯乙烯含量的ABtA构型的锥形ABA型嵌段共聚物在锥形嵌段共聚物中约20至约90重量％的总单乙烯基芳族化合物。还公开了将共混物施加到各种表面的方法。

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