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11. 发明授权

US3424770A Process for the addition of bisulfite to compounds containing double bonds 失效
标题翻译：将双酚A添加到含有双重化合物的化合物的方法
公开(公告)号：US3424770A
公开(公告)日：1969-01-28
申请号：US3424770D
申请日：1965-02-09
申请人： HENKEL & CIE GMBH
发明人： STEIN WERNER , KITTL HANS
IPC分类号： C07B45/02 , C07C303/20 , C07C303/32 , C07C143/02
CPC分类号： C07B45/02 , C07C303/20 , C07C303/32

12. 发明授权

US3897469A Process for the production of di- and polyhydroxycarboxylic acids 失效
标题翻译：生产二羟基羧酸和多羟基羧酸的方法
公开(公告)号：US3897469A
公开(公告)日：1975-07-29
申请号：US41365373
申请日：1973-11-07
申请人： HENKEL & CIE GMBH
发明人： STEIN WERNER , OSBERGHAUS RAINER
IPC分类号： C07C59/00 , C07C51/00 , C07C51/347 , C07C59/10 , C07C59/105 , C07C67/00 , C08H17/36
CPC分类号： C07C59/105
摘要： The invention provides an improved process for the manufacture of higher-molecular weight di- and/or polyhydroxycarboxylic acids by the hydrolysis of epoxidized mono- or polyunsaturated carboxylic acids utilizing aqueous solutions of salts of aliphatic carboxylic acids as catalysts at temperatures of over 100*C.
摘要翻译：本发明提供了一种用于通过在超过100℃的温度下利用脂族羧酸盐作为催化剂的水溶液水解环氧化单或多不饱和羧酸来制备高分子量二 - 和/或多羟基羧酸的改进方法。

13. 发明授权

US3703469A Low-foaming rinsing,washing and cleaning compositions 失效
公开(公告)号：US3703469A
公开(公告)日：1972-11-21
申请号：US3703469D
申请日：1970-12-09
申请人： HENKEL & CIE GMBH
发明人： STEIN WERNER , FLORY KLAUS
IPC分类号： B01D19/04 , C11D3/00 , C11D3/20 , C11D
CPC分类号： C11D3/0026 , B01D19/0404 , C11D1/04 , C11D3/2096 , B01D19/0436 , B01D19/0495
摘要： LOW-FOAMING RINSING, WASHING AND CLEANING COMPOSITIONS COMPRISING (A) FROM 90% TO 99.9% BY WEIGHT OF AT LEAST ONE COMPOUND HAVING A CLEANING OR COMPLEXING ACTION, AND (B) FROM 0.1% TO 10% BY WEIGHT OF AT LEAST ONE FOAM-INHIBITING COMPOUND OF THE FORMULA I

2-(R1-C(-R2)=),3-R2,3-R4,4-(O=)OXETANE

AND ITS SAPONIFICATION PRODUCT OF THE FORMULA II

R1-CH(-R3)-CO-C(-R4)(-R2)-COO-X

WHEREIN R1 AND R2 REPRESENT HYDROCARBON RADICALS WITH 8 TO 30 CARBON ATOMS AND R3 AND R4 REPRESENT HYDROGEN OR HYDROCARBON RADICALS WITH 1 TO 30 CARBON ATOMS, AND X REPRESENTS A CATION.

14. 发明授权

US3637864A Bis-(hydroxyalkyl)-sulfides and preparation thereof 失效
标题翻译： BIS-（羟基丁基） - 磺化物及其制备方法
公开(公告)号：US3637864A
公开(公告)日：1972-01-25
申请号：US3637864D
申请日：1969-04-22
申请人： HENKEL & CIE GMBH
发明人： UMBACH WILFRIED , MEHREN RAINER , STEIN WERNER
IPC分类号： C08K5/00 , A01N31/02 , B01J21/00 , B01J31/00 , C07B61/00 , C07C67/00 , C07C313/00 , C07C319/14 , C07C323/12 , C08K5/37 , C07C149/18
CPC分类号： C07C323/00 , Y10S516/02
摘要： A PROCESS FOR THE PREPARATION OF BIS-(HYDROXYALKYL)SULFIDES WHICH COMPRISES THE STEPS OF REACTING AN EPOXIDE SELECTED FROM THE GROUP CONSISTING OF MONO-VICINAL-EPOXYEPOXIDE COMPOUNDS AND POLY-VICINAL-EPOXY EPOXIDE COMPOUNDS WITH SUBSTANTIALLY THE STOICHIOMETRIC AMOUNT OF HYDROGEN SULFIDE, IN THE ABSENCE OF SOLVENTS AT A TEMPERATURE OF BETWEEN ABOUT 40*C. AND 200*C. AND NORMAL PRESSURES IN THE PRESENCE OF FROM ABOUT 0.01% TO 10% BY WEIGHT, BASED ON SAID EPOXIDE, OF A STRONGLY BASIC CATALYST, AND RECOVERING SAID BIS(HYDROXYALKYL)-SULFIDES. BIS-(HYDROXYALKYL)-SULFIDES OF THE FORMULA

(R1-CH(-OH)-CH(-R2)-)2-S

WHEREIN R1 IS A MEMBER HAVING FROM 1 TO 22 CARBON ATOMS SELECTED FROM THE GROUP CONSISTING OF ALKYL AND ALKYLOL, R2 IS A MEMBER SELECTED FROM THE GROUP CONSISTING OF HYDROGEN, ALKYL HAVING FROM 1 TO 21 CARBON ATOMS AND ALKYLOL HAVING FROM 1 TO 21 CARBON ATOMS WITH THE PROVISO THAT THE SUM OF THE CARBON ATOMS IN R1 AND R2 IS BETWEEN 6 AND 22 ARE DISCLOSED. THE COMPOUNDS ARE USEFUL AS ANTIOXIDANTS, INSECTICIDES, FUNGICIDES AND INTERMEDIATES.

15. 发明授权

US3585225A Process for the continuous preparation of addition products of propylene oxide to carboxylic acids 失效
标题翻译：丙烯氧化物向羧酸的连续制备的方法
公开(公告)号：US3585225A
公开(公告)日：1971-06-15
申请号：US3585225D
申请日：1967-07-14
申请人： HENKEL & CIE GMBH
发明人： STEIN WERNER , UMBACH WILFRIED
IPC分类号： C11C3/00 , C11C3/10
CPC分类号： C11C3/003
摘要： THIS INVENTION RELATES TO AN IMPROVED PROCESS FOR THE CONTINUOUS PRODUCTION OF ADDITION PRODUCTS OF PROPYLENE OXIDE WITH ORGANIC CARBOXYLIC ACIDS WHICH COMPRISES IN COMBINATION (A) CONTINUOUSLY PASSING A MIXTURE OF AN ORGANIC COMPOUND SELECTED FROM THE GROUP CONSISTING OF ORGANIC CARBOXYLIC ACIDS FREE FROM REACTIVE HYDROGEN ATOMS OTHER THAN THE CARBOXYL HYDROGEN ATOM AND ADDITION PRODUCTS OF PROPYLENE OXIDE THEREOF, WITH PROPYLENE OXIDE IN A MOLAR RATIO OF 1:1 TO 1:6 IN THE PRESENCE OF FROM 0.05% TO 1.5% BY WEIGHT OF ALKALI METAL, BASED ON SAID ORGANIC COMPOUND, OF AN ALKALI METAL PROPYLOXYLATION CATALYST, THROUGH A JACKETED REACTOR HAVING A SMALL CROSS-SECTION COMPARED TO ITS LENGTH, UNDER A PRESSURE AT WHICH THE REACTION MIXTURE IS LIQUID, (B) HEATING SAID MIXTURE WHILE PASSING THROUGH SAID JACKETED REACTOR TO ATTAIN A MAXIMUM TEMPERATURE OF BETWEEN ABOUT 230*C. AND 390*C., (C) MAINTAINING SAID MIXTURE IN SAID JACKETED REACTOR FOR ABOUT 10 TO 150 SECONDS, WHEREBY AN ADDITION PRODUCT IS FORMED, (D) IMMEDIATELY COOLING SAID ADDITION PRODUCT TO A TEMPERATURE BELOW 180*C. AFTER SAID ADDITION PRODUCT LEAVES SAID JACKETED REACTOR, AND (E) RECOVERING SAID ADDITION PRODUCT. MORE PARTICULARLY, THE INVENTION RELATES TO THE PREPARATION OF PRODUCTS WITH A HIGH CONTENT OF PROPYLENEGLYCOL-1,2 CARBOXYLIC MONOESTERS IN HIGH VOLUME-TIME-YIELDS.

16. 发明授权

US3523100A Novel compositions for polyurethane coatings 失效
标题翻译：聚氨酯涂料的新型组合物
公开(公告)号：US3523100A
公开(公告)日：1970-08-04
申请号：US3523100D
申请日：1967-10-12
申请人： HENKEL & CIE GMBH
发明人： STEIN WERNER , BARNSTORF JOACHIM , PLOOG UWE
IPC分类号： C08G18/30 , C08G18/48 , C08G18/64 , C08G22/04 , C08G22/08
CPC分类号： C08G18/30 , C08G18/4879 , C08G18/4887 , C08G18/64

17. 发明授权

US3485856A Process for the production of light colored surface active esters of sulfo-fatty acids and salts thereof 失效
标题翻译：生产含硫脂肪酸及其盐的活性酯的光色表面活性剂的制备方法
公开(公告)号：US3485856A
公开(公告)日：1969-12-23
申请号：US3485856D
申请日：1964-03-06
申请人： HENKEL & CIE GMBH
发明人： WULFF CARL , STEIN WERNER , KOCH OTTO , WEISS HERBERT
IPC分类号： C07C303/42 , C07C309/17 , C07C143/90
CPC分类号： C07C309/00

18. 发明授权

US3862204A Hydroxycarboxylic acid nitriles and process 失效
标题翻译：羟基羧酸类硝酸盐和方法
公开(公告)号：US3862204A
公开(公告)日：1975-01-21
申请号：US40623373
申请日：1973-10-15
申请人： HENKEL & CIE GMBH
发明人： UMBACH WILFRIED , MEHREN RAINER , STEIN WERNER
IPC分类号： C07C121/02
CPC分类号： C07C255/00
摘要： 3-HYDROXY-1-CARBOXYLIC ACID NITRILES HAVING MORE THAN 5 CARBON ATOMS AND A PROCESS FOR PRODUCING THEM, COMPRISING REACTING A VICINAL EPOXIDE HAVING MORE THAN 4 CARBON ATOMS WITH HYDROCYANIC ACID IN THE LIQUID PHASE AT A TEMPERATURE OF FROM -20* TO 120*C in the presence of a compound selected from the group consisting of compounds forming cyanide ions, strong bases and mixtures thereof.
摘要翻译：具有5个碳原子的3-羟基-1-羧酸硝酸盐及其制备方法，包括在-20℃至120℃的温度范围内将具有多于4个碳氢化合物的氢氧化物在液相中反应的环氧化物在选自由形成氰化物离子的化合物，强碱和其混合物组成的组的存在下存在。

19. 发明授权

US3662004A Process for producing hydroxyalkyl mercaptans 失效
标题翻译：生产羟基甘油酯的方法
公开(公告)号：US3662004A
公开(公告)日：1972-05-09
申请号：US3662004D
申请日：1969-10-02
申请人： HENKEL & CIE GMBH
发明人： UMBACH WILFRIED , MEHREN RAINER , STEIN WERNER
IPC分类号： C08K5/37 , C07C149/18
CPC分类号： C07C323/00 , C08K5/37 , Y10S516/01 , C08L21/00
摘要： PROCESSES OF REACTING HYDROGEN SULFIDE WITH A MONO OR POLY, TERMINAL OR NON-TERMINAL, ALIPHATIC OR CYCLOALIPHATIC EPOXIDES HAVING MORE THAN 3 CARBON ATOMS IN THE PRESENCE OF 0.01% TO 10% BY WEIGHT OF A STRONGLY BASIC CATALYST IN THE TEMPERATURE RANGE OF FROM -20*C. TO 200*C. AT NORMAL TO ELEVATED PRESSURES IN ORDER TO OBTAIN A HYDROXYALKYL MERCAPTAN CONTAINING MORE THAN 3 CARBON ATOMS. THE NOVEL PRODUCTS ARE HIGHER MOLECULAR WEIGHT HYDROXYALKYL MERCAPTANS OF THE FORMULA

R1-C(-R2)(-OH)-CH(-R3)-SH

WHEREIN R1 IS A MEMBER SELECTED FROM THE GROUP CONSISTING OF ALKYL HAVING FROM 1 TO 22 CARBON ATOMS, ALKYLOL HAVING FROM 1 TO 22 CARBON ATOMS, ALKOXYALKYL HAVING FROM 2 TO 22 CARBON ATOMS, HALOALKYL HAVING FROM 1 TO 22 CARBON ATOMS, CYCLOALKYLALKYL HAVING FROM 6 TO 22 CARBON ATOMS AND ALKENYL HAVING FROM 3 TO 22 CARBON, R2 AND R3 ARE MEMBERS SELECTED FROM THE GROUP CONSISTING OF HYDROGEN AND R1 AND, WHEN TAKEN TOGETHER, ALKYLENE HAVING FROM 3 TO 4 CARBON ATOMS, WITH THE PROVISO THAT THE SUM OF THE CARBON ATOMS IN R1, R2 AND R3 IS FROM 6 TO 22. THE NOVEL HYDROXYALKYL MERCAPTANS ARE USEFUL AS INSECTICIDES AND FUNGICIDES, EMULSIFIERS AND INTERMEDIATES IN CHEMICAL SYNTHESIS.

20. 发明授权

US3662003A Polyalkyleneglycol ethers of bis-(hydroxyalkyl)-sulfides 失效
标题翻译：双（双羟基烷基）-SULFIDES的聚亚烷基二醇
公开(公告)号：US3662003A
公开(公告)日：1972-05-09
申请号：US3662003D
申请日：1969-10-02
申请人： HENKEL & CIE GMBH
发明人： UMBACH WILFRIED , MEHREN RAINER , STEIN WERNER , GOTT ERNST
IPC分类号： B01F17/42 , C07C67/00 , C07C313/00 , C07C319/20 , C07C323/12 , C08G65/28 , C08G65/34 , C08G75/12 , C11D1/00 , C11D1/72 , C07C149/18
CPC分类号： C11D1/002 , C07C323/00 , C08G65/34 , Y10S516/02
摘要：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

(AO)M-H

R1-C(-R2)(-O-(AO)N-H)-CH(-R2)-S-CH(-R2)-C(-R3)(-R1)-O-

POLYALKYLENEGLYCOL ETHERS OF BIS(HYDROIXYALKYL)-SULFIDES HAVING THE FORMULA

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