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11. 发明授权

US08038982B2 EUO-structural-type zeolite containing the alkyl quinuclidinium structuring agent, process for preparation and use as catalyst 失效
标题翻译：含有烷基奎宁环结构剂的EUO结构型沸石，其制备方法和用作催化剂
公开(公告)号：US08038982B2
公开(公告)日：2011-10-18
申请号：US10579205
申请日：2004-11-09
申请人： Loic Rouleau , Sylvie Lacombe
发明人： Loic Rouleau , Sylvie Lacombe
IPC分类号： C01B39/04 , C07C5/27
CPC分类号： B01J29/7446 , B01J29/7023 , B01J2229/18 , C01B39/48 , C07C5/2775 , C07C9/14
摘要： An EUO-structural-type zeolite that comprises at least one element X that is selected from among silicon and germanium and at least one element T that is selected from among aluminum, iron, gallium, vanadium, zirconium, molybdenum, arsenic, antimony, chromium and manganese is described. It contains at least one alkyl quinuclidinium cation in its intracrystalline pores and has an N/X atomic ratio of more than 0.065, whereby N represents the nitrogen element. This invention also relates to a process for preparation of said zeolite and the use of the latter as an acidic solid in a process for conversion of hydrocarbon feedstocks.
摘要翻译：包含选自硅和锗中的至少一种元素X和选自铝，铁，镓，钒，锆，钼，砷，锑，铬中的至少一种元素T的EUO结构型沸石并描述了锰。它在其晶内孔中含有至少一个烷基奎宁环鎓阳离子，其N / X原子比大于0.065，由此N代表氮元素。本发明还涉及一种制备所述沸石的方法以及后者在烃原料转化方法中作为酸性固体的用途。

12. 发明授权

US07923398B2 Preparation of a porous composite material based on EU-1 zeolite and its implementation in the isomerization of C8 aromatics 有权
标题翻译：基于EU-1沸石的多孔复合材料的制备及其在C8芳烃异构化中的应用
公开(公告)号：US07923398B2
公开(公告)日：2011-04-12
申请号：US12203546
申请日：2008-09-03
申请人： Joël Patarin , Emmanuelle Guillon , Loic Rouleau , Simone Goergen
发明人： Joël Patarin , Emmanuelle Guillon , Loic Rouleau , Simone Goergen
IPC分类号： B01J29/06
CPC分类号： C01B39/48 , B01J29/7023 , B01J29/7446 , B01J2229/64 , C07C5/2775 , Y02P20/52 , C07C15/08
摘要： A preparation process is described for a porous composite material formed from an amorphous core based on at least one silicon oxide on which crystals of EU-1 zeolite are dispersed, said process comprising 1) the impregnation of a solid comprising a silicon oxide and an aluminum oxide with an aqueous solution comprising a hexamethonium cation, 2) the hydrothermal treatment, implemented in an autoclave of volume V (ml) under steam and at a temperature T comprised between 120 and 220° C., of said solid from stage 1), the quantity of water introduced beforehand into said autoclave being strictly greater than a volumetric quantity equal to V*[23.48*10−10*T3−48*10−8*T2+5*10−5*T−0.002] and less than or equal to 0.25*V, and is such that said solid is not in direct contact with it, 3) the drying then calcination of the solid from stage 2). The preparation a catalyst from said material for its use in the isomerization of C8 aromatics is also described.
摘要翻译：对于由非晶核构成的多孔复合材料的制备方法描述为基于其上分散有EU-1沸石晶体的至少一种氧化硅，所述方法包括：1）浸渍含有氧化硅和铝的固体氧化物与包含六甲基铵阳离子的水溶液，2）水蒸气处理，在蒸气和在120-220℃的温度T下在体积V（ml）的高压釜中实施，所述固体来自阶段1），预先引入所述高压釜的水的量严格地大于等于V * [23.48 * 10-10 * T3-48 * 10-8 * T2 + 5 * 10-5 * T-0.002]的体积，而小于或等于0.25 * V，并且使得所述固体不与其直接接触，3）干燥然后从阶段2）煅烧固体。还描述了从所述材料制备用于C8芳族化合物异构化的催化剂。

13. 发明申请

US20050250641A1 Heterogeneous adsorbent and the use for diffusional separation methods 失效
标题翻译：非均相吸附剂和扩散分离方法的应用
公开(公告)号：US20050250641A1
公开(公告)日：2005-11-10
申请号：US10522782
申请日：2003-07-11
申请人： Elsa Jolimaitre , Loic Rouleau , Olivier Ducreux
发明人： Elsa Jolimaitre , Loic Rouleau , Olivier Ducreux
IPC分类号： B01J20/18 , B01J20/28 , B01J20/32 , C10G25/00 , B01J29/06
CPC分类号： B01J20/28 , B01J20/28004 , B01J20/28019 , B01J20/28021 , B01J20/2808 , B01J20/28083 , B01J20/3007 , B01J20/3028 , B01J20/3042 , B01J20/3078 , B01J20/3085 , B01J20/3204 , B01J20/3223 , B01J20/3238 , B01J20/3293 , B01J20/3295 , C10G25/003
摘要： A non-homogeneous adsorbent is described, formed of a core and at least one continuous outer layer in which the core of said adsorbent has a volume adsorptive capacity representing at least 35% of the volume of the adsorbent and the outer layer has a diffusional selectivity greater than 5. The adsorbent is used in gas-separation processes or liquid-separation processes.
摘要翻译：描述了非均匀吸附剂，其由芯和至少一个连续的外层形成，其中所述吸附剂的芯具有代表吸附剂体积的至少35％的体积吸附能力，并且外层具有扩散选择性大于5.吸附剂用于气体分离过程或液体分离过程。

14. 发明授权

US08562940B2 Process for preparing an alumina with controlled mesoporosity 有权
标题翻译：制备具有受控中孔隙度的氧化铝的方法
公开(公告)号：US08562940B2
公开(公告)日：2013-10-22
申请号：US12978774
申请日：2010-12-27
申请人： Loic Rouleau , Sébastien Royer , Christine Lancelot , Franck Dumeignil , Edmond Payen , Pascal Blanchard
发明人： Loic Rouleau , Sébastien Royer , Christine Lancelot , Franck Dumeignil , Edmond Payen , Pascal Blanchard
IPC分类号： C01F7/00
CPC分类号： C01F7/36 , B01J29/0308 , B01J29/0333 , B01J35/1019 , B01J35/1042 , C01F7/441 , C01P2004/10 , C01P2006/12 , C01P2006/14 , C01P2006/16 , C04B35/111 , C04B38/00 , C04B38/0054 , C04B2111/0081 , C04B2235/3218
摘要： A process for preparing a mesoporous alumina is described, comprising the following steps: a) mixing, in aqueous solution, at least one source of aluminum constituted by an aluminum alkoxide, at least one cationic surfactant and at least one organic solvent selected from methanol and ethanol; b) hydrothermally treating the mixture formed in said step a); c) drying the solid formed in said step b); d) calcining the solid formed in said step c).
摘要翻译：描述了一种制备介孔氧化铝的方法，包括以下步骤：a）在水溶液中混合至少一种由烷氧基铝构成的铝源，至少一种阳离子表面活性剂和至少一种选自甲醇和乙醇; b）水热处理在所述步骤a）中形成的混合物; c）干燥所述步骤b）中形成的固体; d）煅烧在步骤c）中形成的固体。

15. 发明授权

US08399373B2 Zeolitic catalysts, their process for preparation and their applications 有权
标题翻译：沸石催化剂，其制备方法及其应用
公开(公告)号：US08399373B2
公开(公告)日：2013-03-19
申请号：US12541540
申请日：2009-08-14
申请人： Simone Goergen , Loic Rouleau , Emmanuelle Guillon , Florent Guillou , Laurent Simon , Christophe Bouchy , Joël Patarin
发明人： Simone Goergen , Loic Rouleau , Emmanuelle Guillon , Florent Guillou , Laurent Simon , Christophe Bouchy , Joël Patarin
IPC分类号： C07C5/22 , B01J29/06 , C10G47/02
CPC分类号： B01J29/06 , B01J29/084 , B01J29/166 , B01J29/40 , B01J29/70 , B01J29/7023 , B01J29/7446 , B01J35/002 , B01J35/10 , B01J35/1038 , B01J35/1066 , B01J2229/186 , B01J2229/64 , C10G47/16 , C10G49/08
摘要： The invention describes a porous composite material that comprises a porous substrate based on a refractory inorganic oxide in which said substrate has a zeolite crystal content that is less than 25% by mass, whereby said crystals are dispersed homogeneously in the pores of said substrate, and the distribution coefficient that is measured by Castaing microprobe is between 0.75 and 1.25, and in which the total pore volume of said substrate represents at least 40% of the initial total pore volume of the substrate, and the mean diameter of the pores represents at least 50% of the mean diameter of the pores of the initial substrate, its process for preparation and its use as catalyst in the hydrocarbon feedstock conversion reactions.
摘要翻译：本发明描述了一种多孔复合材料，其包括基于难熔无机氧化物的多孔基材，其中所述基材的沸石晶体含量小于25质量％，由此所述晶体均匀地分散在所述基材的孔中，以及由Castaing微探针测量的分布系数在0.75和1.25之间，其中所述基材的总孔体积占基材初始总孔体积的至少40％，孔的平均直径至少表示初始底物的孔的平均直径的50％，其制备方法及其作为烃原料转化反应中的催化剂。

16. 发明申请

US20120016170A1 PROCESS FOR PREPARING A CORE-LAYER MATERIAL HAVING GOOD MECHANICAL STRENGTH 审中-公开
标题翻译：制备具有良好机械强度的核心层材料的方法
公开(公告)号：US20120016170A1
公开(公告)日：2012-01-19
申请号：US13059666
申请日：2009-08-19
申请人： Samy Ould-Chikh , Antoine Fecant , Loic Rouleau , Lars Fischer , Mehrdji Hemati
发明人： Samy Ould-Chikh , Antoine Fecant , Loic Rouleau , Lars Fischer , Mehrdji Hemati
IPC分类号： C07C5/05 , B01J23/42 , B01J21/04 , B01J37/08 , B01J37/16 , B01J37/025 , B01J37/02
CPC分类号： B01J13/04
摘要： A process is described for preparing a spherical material comprising a porous core coated with a continuous and homogeneous porous layer, the degree of attrition of said material being less than 20%. Said preparation process comprises a) bringing a bed of spherical particles constituting the core of said material into contact with a suspension containing an inorganic binder in order to form a solid having a pre-layer around said core; b) bringing the solid derived from step a) into contact, in a stream of hot air, with a powder constituted by spherical particles of an inorganic oxide and a suspension containing an inorganic binder and an organic binder in order to form a solid the core of which is coated with at least one continuous and homogeneous porous layer, the ratio of the (mass of anhydrous inorganic binder/volume of powder particles) being in the range 0.05 to 1 g.mL−1; c) drying the solid derived from said step b); and d) calcining the solid derived from said step c).
摘要翻译：描述了一种用于制备球形材料的方法，该球形材料包括涂覆有连续且均匀的多孔层的多孔芯，所述材料的磨损程度小于20％。所述制备方法包括a）使构成所述材料的芯的球形颗粒床与含有无机粘合剂的悬浮液接触，以形成在所述芯周围具有预层的固体; b）使来自步骤a）的固体在热空气流中与由无机氧化物的球形颗粒和含有无机粘合剂和有机粘合剂的悬浮液构成的粉末接触以形成固体芯其中涂覆有至少一个连续且均匀的多孔层，（无水无机粘合剂的质量/粉末颗粒的体积）的比例在0.05-1g.mL-1的范围内; c）干燥衍生自所述步骤b）的固体; 和d）煅烧衍生自所述步骤c）的固体。

17. 发明授权

US06342200B1 Process for preparing a zeolite with structure type EUO 有权
标题翻译：制备结构型EUO的沸石的方法
公开(公告)号：US06342200B1
公开(公告)日：2002-01-29
申请号：US09432120
申请日：1999-11-02
申请人： Loic Rouleau , Sylvie Lacombe , Fabio Alario , Elisabeth Merlen , Frédéric Kolenda , Julia Magne-Drisch
发明人： Loic Rouleau , Sylvie Lacombe , Fabio Alario , Elisabeth Merlen , Frédéric Kolenda , Julia Magne-Drisch
IPC分类号： C01B3904
CPC分类号： B01J29/7023 , B01J20/18 , B01J29/04 , B01J2229/62 , C01B39/48 , C07C5/2708 , C07C2529/70 , C10G35/095 , C10G45/64 , Y02P20/588 , C07C15/067
摘要： The present invention concerns a process for preparing a zeolite with structure type EUO comprising at least one element X selected from silicon and germanium and at least one element T selected from iron, aluminium, gallium, boron, titanium, vanadium, zirconium, molybdenum, arsenic, antimony, chromium and manganese, characterized in that seeds of at least one zeolitic material are used comprising at least one element X′ selected from silicon and germanium and at least one element T′ selected from iron, aluminium, gallium, boron, titanium, vanadium, zirconium, molybdenum, arsenic, antimony, chromium and manganese with a ratio X′/T′ of less than 200, said seeds being different from the zeolite with structure type EUO being prepared. The present invention also concerns the use of the zeolite obtained as a catalyst in a process for converting hydrocarbon-containing feeds, as an adsorbent to control pollution and as a molecular sieve for separation, and more particularly as a catalyst in a process for isomerizing aromatic compounds containing 8 carbon atoms.
摘要翻译：本发明涉及一种制备具有结构型EUO的沸石的方法，该方法包括至少一种选自硅和锗的元素X和选自铁，铝，镓，硼，钛，钒，锆，钼，砷中的至少一种元素T ，锑，铬和锰，其特征在于使用至少一种沸石材料的种子，其包含至少一种选自硅和锗的元素X'和至少一种选自铁，铝，镓，硼，钛，钒，锆，钼，砷，锑，铬和锰，其比例X'/ T'小于200，所述种子与制备具有结构类型EUO的沸石不同。本发明还涉及在烃类进料转化方法中作为催化剂使用的沸石，作为用于控制污染的吸附剂和用于分离的分子筛，更特别地，作为用于异构化芳族化合物的方法中的催化剂含有8个碳原子的化合物。

18. 发明申请

US20090043145A1 Euo-structural-type zeolite containing the alkyl quinuclidinium structuring agent, process for preparation and use as catalyst 失效
标题翻译：含有烷基奎宁环结构剂的Eu-结构型沸石，其制备方法和用作催化剂
公开(公告)号：US20090043145A1
公开(公告)日：2009-02-12
申请号：US10579205
申请日：2004-11-09
申请人： Loic Rouleau , Sylvie Lacombe
发明人： Loic Rouleau , Sylvie Lacombe
IPC分类号： C07C5/13
CPC分类号： B01J29/7446 , B01J29/7023 , B01J2229/18 , C01B39/48 , C07C5/2775 , C07C9/14
摘要： An EUO-structural-type zeolite that comprises at least one element X that is selected from among silicon and germanium and at least one element T that is selected from among aluminum, iron, gallium, vanadium, zirconium, molybdenum, arsenic, antimony, chromium and manganese is described. It contains at least one alkyl quinuclidinium cation in its intracrystalline pores and has an N/X atomic ratio of more than 0.065, whereby N represents the nitrogen element. This invention also relates to a process for preparation of said zeolite and the use of the latter as an acidic solid in a process for conversion of hydrocarbon feedstocks.
摘要翻译：包含选自硅和锗中的至少一种元素X和选自铝，铁，镓，钒，锆，钼，砷，锑，铬中的至少一种元素T的EUO结构型沸石并描述了锰。它在其晶内孔中含有至少一个烷基奎宁环鎓阳离子，其N / X原子比大于0.065，由此N代表氮元素。本发明还涉及一种制备所述沸石的方法以及后者在烃原料转化方法中作为酸性固体的用途。

19. 发明授权

US6027707A NU-88 zeolite, a process for its preparation and catalytic applications thereof 失效
标题翻译： NU-88沸石，其制备方法和催化应用
公开(公告)号：US6027707A
公开(公告)日：2000-02-22
申请号：US916363
申请日：1997-08-22
申请人： John Leonello Casci , Sheena Maberly , Eric Benazzi , Loic Rouleau , Roland Patrick Henney
发明人： John Leonello Casci , Sheena Maberly , Eric Benazzi , Loic Rouleau , Roland Patrick Henney
IPC分类号： B01J29/78 , B01D53/86 , B01J29/04 , C01B39/08 , C01B39/48 , C07B61/00 , C07C2/12 , C07C5/02 , C07C5/13 , C07C5/22 , C07C5/27 , C07C5/32 , C07C5/41 , C07C6/02 , C07C6/12 , C07C9/02 , C07C11/02 , C07C15/02 , C10G11/05 , C10G35/095 , C10G45/64 , B01J29/068 , B01J29/072 , B01J29/076
CPC分类号： C10G45/64 , B01D53/8628 , B01J29/04 , C01B39/082 , C01B39/48 , C07C5/02 , C07C5/222 , C07C5/2708 , C07C5/2775 , C07C5/321 , C07C5/41 , C07C6/123 , C07C6/126 , C10G11/05 , C10G35/095 , C07C2529/70
摘要： The invention concerns NU-88 zeolite, characterized by:i) a chemical composition with the following formula, expressed in terms of the mole ratios of the oxides for the anhydrous state:100 XO.sub.2, mY.sub.2 O.sub.3, pR.sub.2/n Owherem is 10 or less;p is 20 or less;R represents one or more cations with valency n;X represents silicon and/or germanium;Y represents one or more of the following elements: aluminium, iron, gallium, boron, titanium, vanadium, zirconium, molybdenum, arsenic, antimony, chromium and manganese; andii) an X ray diffraction diagram, in its as synthesized state, which comprises the results shown in Table 1 of the description.The invention also concerns the preparation of the zeolite, any catalyst containing the zeolite and any catalytic process using such a catalyst.
摘要翻译：本发明涉及NU-88沸石，其特征在于：i）具有下式的化学组成，以无水状态的氧化物的摩尔比表示：100XO2，mY2O3，pR2 / nO，其中m为10或更小 ; p为20以下; R表示一个或多个价数为n的阳离子; X表示硅和/或锗; Y表示以下元素中的一种或多种：铝，铁，镓，硼，钛，钒，锆，钼，砷，锑，铬和锰; 和ii）其合成状态的X射线衍射图，其包含说明书的表1所示的结果。本发明还涉及沸石的制备，含有沸石的任何催化剂以及使用这种催化剂的任何催化方法。

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