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11. 发明授权

US4957994A Epoxy resins containing imido rings, production process thereof and epoxy resin compositions containing the same 失效
标题翻译：含有亚氨基环的环氧树脂及其制备方法和含有它的环氧树脂组合物
公开(公告)号：US4957994A
公开(公告)日：1990-09-18
申请号：US393798
申请日：1989-08-15
申请人： Tatsuhiro Urakami , Yoshimitsu Tanabe , Keizaburo Yamaguchi , Akihiro Yamaguchi
发明人： Tatsuhiro Urakami , Yoshimitsu Tanabe , Keizaburo Yamaguchi , Akihiro Yamaguchi
IPC分类号： C08G59/06 , C08G59/26
CPC分类号： C08G59/26 , C08G59/063
摘要： An opoxy resin is obtained by reacting an epihalohydrin with an imido-ring-containing diphenol represented by the following formula (I): ##STR1## wherein R represents an aliphatic group having at least two carbon atoms, an alicyclic group, a monocyclic aryl group, a fused polycyclic aromatic group, or a non-fused polycyclic aromatic group formed of aromatic groups coupled together directly or via a linking member and the two hydroxyl groups are each bonded to a meta position or the para position. In the epoxy resin, at least 50% of the hdroxyl groups of molecules of the diphenol have been opoxidized.

12. 发明授权

US5710334A Aromatic dinitro and diamino intermediates 失效
标题翻译：芳香二硝基和二氨基中间体
公开(公告)号：US5710334A
公开(公告)日：1998-01-20
申请号：US453073
申请日：1995-05-26
申请人： Yuko Ishihara , Mitsunori Matsuo , Keizaburo Yamaguchi , Akihiro Yamaguchi
发明人： Yuko Ishihara , Mitsunori Matsuo , Keizaburo Yamaguchi , Akihiro Yamaguchi
IPC分类号： C07C201/12 , C07C205/45 , C07C221/00 , C07C225/22 , C08G73/10 , C08G73/12 , C08J5/18 , C08L79/08 , C07C217/84 , C07C217/90
CPC分类号： C08G73/10 , C08G73/1007 , C08G73/1014 , C08G73/1017 , C08G73/1067 , Y10T428/31504 , Y10T428/31721
摘要： This invention relates to a novel thermoplastic and amorphous polyimide which is readily soluble in organic solvent, a novel aromatic diamino compound used for the polyimide, a preparation process thereof, a polyimide-based resin composition comprising the thermoplastic polyimide and a fibrous reinforcement, a process for preparing the resin composition, an injection molded article of the resin composition, a polyimide-based composite obtained by molding the above soluble and thermoplastic polyimide in combination with a fibrous reinforcement, and a fibrous reinforcement having a surface modified with the above polyimide. The polyimide comprise a requisite structural unit having one or more recurring structural units of the formula: ##STR1## wherein m and n are individually an integer of 0 or 1, and R is ##STR2## The polyimide of the invention is essentially amorphous, excellent in melt flow stability in the decreased temperature as compared with conventionally known polyimide and has greatly improved processability. The polyimide of the invention obtained by using a novel aromatic diamino compound as a monomer can control various properties such as melt flow ability and solubility in solvents by side chains and not by principal chain of polyimide. Thus, excellent melt flow property and solubility in solvents can be obtained while maintaining high heat resistance and adhesive property which are derived from benzophenone structure of the diamino compound of the the invention.
摘要翻译：本发明涉及易溶于有机溶剂的新型热塑性和无定形聚酰亚胺，用于聚酰亚胺的新型芳族二氨基化合物及其制备方法，包含热塑性聚酰亚胺和纤维增强剂的聚酰亚胺基树脂组合物，用于制备树脂组合物的树脂组合物的注塑制品，通过将上述可溶性和热塑性聚酰亚胺与纤维增强剂组合成型而获得的聚酰亚胺类复合材料和具有用上述聚酰亚胺改性的表面的纤维增强剂。聚酰亚胺包含必需的结构单元，其具有一个或多个下式的重复结构单元：其中m和n分别为0或1的整数，且R为“无定形”，优异的与传统已知的聚酰亚胺相比在降低的温度下的熔体流动稳定性，并且具有极大的改进的加工性能。通过使用新颖的芳族二氨基化合物作为单体获得的本发明的聚酰亚胺可以通过侧链而不是聚酰亚胺的主链来控制各种性能如熔体流动性和在溶剂中的溶解度。因此，在保持由本发明的二氨基化合物的二苯甲酮结构得到的高耐热性和粘合性的同时，可以获得优异的熔体流动性和溶剂中的溶解性。

13. 发明授权

US5145949A Production process for making aromatic amine resins 失效
标题翻译：制备芳香胺树脂的生产工艺
公开(公告)号：US5145949A
公开(公告)日：1992-09-08
申请号：US823478
申请日：1992-01-22
申请人： Keizaburo Yamaguchi , Yoshimitsu Tanabe , Tatsuhiro Urakami , Akihiro Yamaguchi , Norimasa Yamaya , Masahiro Ohta
发明人： Keizaburo Yamaguchi , Yoshimitsu Tanabe , Tatsuhiro Urakami , Akihiro Yamaguchi , Norimasa Yamaya , Masahiro Ohta
IPC分类号： C07C211/50 , C08G73/12
CPC分类号： C08G73/121 , C07C211/50
摘要： Disclosed herein is an aromatic amine resin formed of a mixture of aromatic amine compounds represented by the following general formula (a): ##STR1## wherein A means a phenylene, alkyl-substituted phenylene, diphenylene, diphenyl ether or naphthylenyl group, R.sup.1 denotes a halogen atom or a hydroxyl, C.sub.1-4 alkoxy or C.sub.1-5 alkyl group, l stands for 1 or 2, m is an integer of 0-3, when m is 2 or 3, R.sup.1 s may be the same or different and two of R.sup.1 s may join together into a 5- to 6-membered alicyclic moiety which may optionally contain one or more side chains, and n stands for an integer of 0-300.
摘要翻译：本文公开了由以下通式（a）表示的芳族胺化合物的混合物形成的芳香族胺树脂：其中A表示亚苯基，烷基取代的亚苯基，二亚苯基，二苯基醚或萘基， R1表示卤素原子或羟基，C1-4烷氧基或C1-5烷基，l表示1或2，m表示0-3的整数，当m为2或3时，R 1可以相同或不同并且R 1中的两个可以连接在一起可以任选地含有一个或多个侧链的5-至6-元脂环部分，n表示0-300的整数。

14. 发明授权

US5079331A Heat-resistant epoxy resin composition based on 2-(4-hydroxyphenyl)-2-(4-maleimidophenyl)propane 失效
标题翻译：基于2-（4-羟基苯基）-2-（4-马来酰亚胺基苯基）丙烷的耐热环氧树脂组合物
公开(公告)号：US5079331A
公开(公告)日：1992-01-07
申请号：US527267
申请日：1990-05-23
申请人： Mikio Kitahara , Koichi Machida , Takayuki Kubo , Motoyuki Torikai , Koutarou Asahina , Yoshimitsu Tanabe , Keizaburo Yamaguchi , Akihiro Yamaguchi
发明人： Mikio Kitahara , Koichi Machida , Takayuki Kubo , Motoyuki Torikai , Koutarou Asahina , Yoshimitsu Tanabe , Keizaburo Yamaguchi , Akihiro Yamaguchi
IPC分类号： H01L23/29 , C07D207/44 , C07D207/452 , C08G59/40 , C08K5/3415 , H01L23/31
CPC分类号： C07D207/452 , C08K5/3415
摘要： Heat-resistant epoxy resin composition obtained by incorporation of 2-(4-hydroxyphenyl)-2-(4-maleimidophenyl)propane in a resin composition consisting esssentially of epoxy resin and an epoxy hardener is disclosed.
摘要翻译：公开了通过在由环氧树脂和环氧固化剂组成的树脂组合物中引入2-（4-羟基苯基）-2-（4-马来酰亚胺基苯基）丙烷获得的耐热环氧树脂组合物。

15. 发明授权

US4952648A Production process of multivalent metal-modified salicylic acid/styrene resin, color-developing agent using the resin and suited for use in pressure-sensitive copying paper sheet and pressure-sensitive copying paper unit employing the agent 失效
标题翻译：多价金属改性水杨酸/苯乙烯树脂的制造方法，使用该树脂的显色剂，适用于压敏复印纸和使用该试剂的压敏复印纸单元
公开(公告)号：US4952648A
公开(公告)日：1990-08-28
申请号：US228235
申请日：1988-08-04
申请人： Keizaburo Yamaguchi , Yoshimitsu Tanabe , Akihiro Yamaguchi
发明人： Keizaburo Yamaguchi , Yoshimitsu Tanabe , Akihiro Yamaguchi
IPC分类号： B41M5/155 , C08G61/02
CPC分类号： B41M5/155 , C08G61/02
摘要： Disclosed herein are novel multivalent metal-modified salicyclic acid resins useful as color-developing agents for pressure-sensitive copying paper. They can each be produced by causing a salicyclic acid ester and a styrene derivative to undergo a Friedel-Crafts reaction in the presence of a strong acid catalyst, hydrolyzing the resulting salicylic acid ester resin, and then reacting the thus-obtained salicyclic acid resin with a multivalent metal salt.

16. 发明授权

US4803258A Thermoplastic aromatic polyether-pyridine and process for preparing same 失效
标题翻译：热塑性芳族聚醚 - 吡啶及其制备方法
公开(公告)号：US4803258A
公开(公告)日：1989-02-07
申请号：US76873
申请日：1987-07-23
申请人： Keizaburo Yamaguchi , Hideaki Oikawa , Kenichi Sugimoto , Masahiro Ohta , Akihiro Yamaguchi
发明人： Keizaburo Yamaguchi , Hideaki Oikawa , Kenichi Sugimoto , Masahiro Ohta , Akihiro Yamaguchi
IPC分类号： C07D213/64 , C08G65/40 , C08G75/23
CPC分类号： C08G65/4006 , C07D213/64 , C08G65/4037 , C08G75/23
摘要： Disclosed are thermoplastic aromatic polyetherpyridines composed of repeating structural units each containing one or more pyridine rings. These polymers are prepared by reacting a 2,6-dihalogenopyridine with one or two dihydroxy compounds or by reacting a bis(6-chloro-2-pyridyloxy) compound with a dihydroxy compound. The polymers thus obtained have an excellent combination of heat resistance, moldability and other properties, and hence are useful in a wide variety of applications.

17. 发明授权

US4453009A Process for producing fluorobenzophenone derivatives 失效
标题翻译：氟代二苯甲酮衍生物的制备方法
公开(公告)号：US4453009A
公开(公告)日：1984-06-05
申请号：US433438
申请日：1982-10-08
申请人： Akihiro Yamaguchi , Keizaburo Yamaguchi , Kenichi Sugimoto , Yoshimitsu Tanabe
发明人： Akihiro Yamaguchi , Keizaburo Yamaguchi , Kenichi Sugimoto , Yoshimitsu Tanabe
IPC分类号： C07C45/63 , C07C49/80 , C07C49/813 , C07C49/84
CPC分类号： C07C201/12
摘要： 4-Fluorobenzophenone derivatives of 4,4'-difluorobenzophenone are produced by effecting a halogen-fluorine exchanging reaction between the corresponding 4-halogenobenzophenone derivatives or 4,4'-dihalogenobenzophenone and an alkali fluoride.The reaction is carried out by heating in an organic solvent. After distilling off the solvent from the reaction product mixture, the end product is isolated by extracting with a solvent. Alternatively the end product is isolated by distillation.
摘要翻译：通过在相应的4-卤代二苯甲酮衍生物或4,4'-二卤代二苯甲酮与碱金属氟化物之间进行卤素 - 氟交换反应来制备4,4'-二氟二苯甲酮的4-氟二苯甲酮衍生物。反应通过在有机溶剂中加热进行。从反应产物混合物中蒸除溶剂后，通过用溶剂萃取分离终产物。或者，最终产物通过蒸馏分离。

18. 发明授权

US5674953A Method of preventing scale adhesion to surfaces of polymerization tank with phenol-aldehyde coating 失效
标题翻译：用酚醛涂料防止聚合槽表面附着垢的方法
公开(公告)号：US5674953A
公开(公告)日：1997-10-07
申请号：US466522
申请日：1995-06-06
申请人： Seiichi Masuko , Ichisaburo Nakamura , Keiichi Fukuda , Yasuyuki Hatakeyama , Akihiro Yamaguchi , Keizaburo Yamaguchi
发明人： Seiichi Masuko , Ichisaburo Nakamura , Keiichi Fukuda , Yasuyuki Hatakeyama , Akihiro Yamaguchi , Keizaburo Yamaguchi
IPC分类号： C08F2/00 , C08F14/06 , C08F2/20 , C08F2/02
CPC分类号： C08F14/06 , C08F2/004
摘要： In a novel method of homo- or copolymerization of vinyl chloride, a specified coating agent is applied on the surfaces of the portions which will become into contact with the vinyl chloride monomer during the polymerization process. The coating agent is in a form of an aqueous solution of a modified condensation product of phenol and aldehyde, the pH of the solution being adjusted in a range that the product is dissolved at an ambient temperature upon coating of the solution and separates out of the solution upon being heated on the surfaces. The wall surface of the polymerization tank and the like is then coated with a thin film of the coating agent having a uniform thickness and being strongly adhered to the wall surface, thereby providing an excellent effect of preventing adhesion of the product polymer to the wall surface.
摘要翻译：在氯乙烯均聚或共聚的新方法中，在聚合过程中将在与氯乙烯单体接触的部分的表面上施加特定的涂布剂。涂层剂是苯酚和醛的改性缩合产物的水溶液形式，溶液的pH值在产物在环境温度下溶解的范围内被调节，并在分离出在表面上加热时的溶液。然后将聚合槽等的壁面用均匀厚度的涂布剂的薄膜涂布并牢固地附着在壁面上，从而提供优异的防止产品聚合物粘合到壁面上的效果。

19. 发明授权

US5631377A Polyimide intermediates 失效
标题翻译：聚酰亚胺中间体
公开(公告)号：US5631377A
公开(公告)日：1997-05-20
申请号：US450150
申请日：1995-05-26
申请人： Mitsunori Matsuo , Tsutomu Ishida , Akio Karasawa , Keizaburo Yamaguchi , Akihiro Yamaguchi
发明人： Mitsunori Matsuo , Tsutomu Ishida , Akio Karasawa , Keizaburo Yamaguchi , Akihiro Yamaguchi
IPC分类号： C08G73/10 , C08L79/08 , C07C255/60 , C07D213/38
CPC分类号： C08G73/1085 , C08G73/10 , C08G73/1039 , C08G73/105 , C08G73/1053 , C08G73/1071 , C08L79/08
摘要： This invention relates to a novel polyimide or polyimide copolymer having excellent heat resistance and greatly improved processability, and has a novel aromatic diamino compound used for the polyimide, a preparation process thereof, a polyimide-based resin composition comprising the polyimide or polyimide copolymer and a fibrous reinforcement, a process for preparing the resin composition, an injection molded article of the resin composition.The polyimide comprise a requisite structural unit having one or more recurring structural units of the formula: ##STR1## wherein L is an oxygen atom, carbonyl, isopropylidene or hexafluoroisopropylidene, and X is ##STR2## , and Ar is a tetravalent radical having 6 to 27 carbon atoms and being selected from the group consisting of a monoaromatic radical, condensed polyaromatic radical and noncondensed polyaromatic radical having aromatic radicals connected to each other with a direct bond or a bridge member.The polyimide or polyimide copolymer is outstanding in melt-flow stability, and has greatly improved processability and excellent heat resistance. Consequently, the polyimide or polyimide copolymer can be applied to structural materials, and electic . electronic appliances.
摘要翻译：本发明涉及耐热性优异且加工性极佳的新型聚酰亚胺或聚酰亚胺共聚物，具有用于聚酰亚胺的新型芳族二氨基化合物及其制备方法，包含聚酰亚胺或聚酰亚胺共聚物的聚酰亚胺系树脂组合物和纤维增强材料，树脂组合物的制备方法，树脂组合物的注塑制品。聚酰亚胺包含具有一个或多个下式的重复结构单元的必需结构单元：其中L是氧原子，羰基，异亚丙基或六氟异亚丙基，X是X，且Ar是选自具有6至27个碳原子的四价基团，并且选自具有芳族基团的单芳族基团，缩合多芳族基团和具有直接键合的桥连构件彼此连接的非缩合多芳族基团。聚酰亚胺或聚酰亚胺共聚物在熔体流动稳定性方面是突出的，并且具有极大的改进的加工性和优异的耐热性。因此，聚酰亚胺或聚酰亚胺共聚物可以应用于结构材料和电极。电子电器。

20. 发明授权

US5410084A Aromatic diamine and polyimide, and preparation process of same 失效
标题翻译：芳香二胺和聚酰亚胺，其制备方法相同
公开(公告)号：US5410084A
公开(公告)日：1995-04-25
申请号：US253267
申请日：1994-06-02
申请人： Mitsunori Matsuo , Tsutomu Ishida , Keizaburo Yamaguchi , Akihiro Yamaguchi
发明人： Mitsunori Matsuo , Tsutomu Ishida , Keizaburo Yamaguchi , Akihiro Yamaguchi
IPC分类号： C07C217/90 , C08G73/10 , H05K1/00 , H05K1/03
CPC分类号： C08G73/105 , C07C217/90 , C08G73/10 , C08G73/1014 , C08G73/1017 , H05K1/0346 , H05K3/4676
摘要： A polyimide comprising a requisite structural unit having one or more recurring structural units of the formula: ##STR1## such as the structural units of the formula ##STR2## Further, the present invention relates to a novel aromatic diamine which has a perfluoro radical and can be used as a raw material monomer of the polyimide, and a process for preparing the same.The polyimide can have an extremely low dielectric constant and is colorless, transparent and excellent in processability and heat resistance.
摘要翻译：一种聚酰亚胺，其包含具有一个或多个下式的重复结构单元的必需结构单元：例如下式的结构单元。此外，本发明涉及一种新型芳族二胺，其具有全氟自由基，并且可以用作聚酰亚胺的原料单体及其制备方法。聚酰亚胺可以具有极低的介电常数，并且是无色透明且加工性和耐热性优异的。

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