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11. 发明申请

WO2011036293A2 COMPOSITION OF A FLUORINATED ORGANIC CARBONATE AND A LEWIS ACID 审中-公开
标题翻译：氟化有机碳酸酯和乳酸的组成
公开(公告)号：WO2011036293A2
公开(公告)日：2011-03-31
申请号：PCT/EP2010/064269
申请日：2010-09-27
申请人： SOLVAY SA , OLSCHIMKE, Jens , BOMKAMP, Martin , GROSSMANN, Andreas
发明人： OLSCHIMKE, Jens , BOMKAMP, Martin , GROSSMANN, Andreas
IPC分类号： C07D317/36 , C07D317/42
CPC分类号： C07D317/36 , C07D317/42
摘要： The present invention provides inter alia a method for handling fluorinated organic carbonates such that degradation reactions are minimized or even completely suppressed and hence initial purity of fluorinated organic carbonatesis essentially maintained during handling. The invention further provides compositions comprising a fluorinated organic carbonate with improved stability against degradation reactions. The compositions comprise equal to or less than 500 ppm of a Lewis acid.
摘要翻译：本发明尤其提供一种处理氟化有机碳酸酯的方法，使得降解反应最小化或甚至完全抑制，因此氟化有机碳酸酯的初始纯度在处理过程中基本保持。本发明进一步提供包含具有改进的降解反应稳定性的氟化有机碳酸酯的组合物。组合物包含等于或小于500ppm的路易斯酸。

12. 发明申请

WO2010136506A1 PROCESS FOR THE PREPARATION OF 4-FLUORO-4-R-5-R'-1,3-DIOXOLANE-2-ONES 审中-公开
标题翻译：制备4-氟-4-R-5-R'-1,3-二氧杂环己烷-2-酮的方法
公开(公告)号：WO2010136506A1
公开(公告)日：2010-12-02
申请号：PCT/EP2010/057281
申请日：2010-05-26
申请人： SOLVAY FLUOR GMBH , BOMKAMP, Martin , OLSCHIMKE, Jens , BROSCH, Carsten , GROSSMANN, Andreas
发明人： BOMKAMP, Martin , OLSCHIMKE, Jens , BROSCH, Carsten , GROSSMANN, Andreas
IPC分类号： C07D317/42 , C07C69/96 , C07C68/02 , H01M10/36
CPC分类号： H01M10/0525 , C07C68/02 , C07C69/96 , C07D317/42 , H01M10/0567 , H01M10/0568 , H01M10/0569
摘要： The present invention concerns 4-fluoro-4-R-5-R'-1,3-dioxolane-2-ones, wherein R is an alkyl group and R' is H or a C1 to C3 alkyl group, their manufacture, solvent mixtures for lithium ion batteries containing them and conductive salt solutions for lithium ion batteries, e.g. solutions containing LiPF 6 .
摘要翻译：本发明涉及4-氟-4-R-5-R'-1,3-二氧戊环-2-酮，其中R是烷基，R'是H或C1-C3烷基，它们的制备，溶剂含锂离子电池的混合物和锂离子电池的导电盐溶液，例如含LiPF6的溶液。

13. 发明申请

WO2009118368A1 PREPARATION OF FLUORINATED ORGANIC CARBONATES DEPLETED IN HF USING A SPECIFIC ABSORBENT 审中-公开
标题翻译：使用特定吸收剂在HF中制备氟化有机碳酸盐
公开(公告)号：WO2009118368A1
公开(公告)日：2009-10-01
申请号：PCT/EP2009/053559
申请日：2009-03-26
申请人： SOLVAY FLUOR GMBH , OLSCHIMKE, Jens , GROSSMANN, Andreas , EICHHOLZ, Kerstin , PALSHERM, Stefan , BÖSE, Olaf
发明人： OLSCHIMKE, Jens , GROSSMANN, Andreas , EICHHOLZ, Kerstin , PALSHERM, Stefan , BÖSE, Olaf
IPC分类号： C07D317/42 , C07D317/36 , C07C68/08
CPC分类号： C07D317/36 , C07C68/08 , C07D317/42 , C07C69/96
摘要： The content of hydrogen fluorides in fluorosubstituted organic carbonates can be reduced by contact with SiO 2 containing agents, especially silica gel. The process is especially suitable to reduce the hydrogen fluoride content in fluoroethylene carbonate which after further purification can be applied as solvent or solvent additive in lithium ion batteries.
摘要翻译：通过与含SiO 2的试剂，特别是硅胶接触可以降低含氟取代有机碳酸酯中氟化氢的含量。该方法特别适用于降低氟代亚乙基碳酸酯中的氟化氢含量，其进一步纯化可用作锂离子电池中的溶剂或溶剂添加剂。

14. 发明申请

WO2011036293A3 PROCESS FOR THE MANUFACTURE OF TRIFLUOROETHLYLENE CARBONATE AND TETRAFLUOROETHYLENE CARBONATE 审中-公开
标题翻译：碳酸三氟乙烯和碳酸四亚乙基碳酸酯的制备方法
公开(公告)号：WO2011036293A3
公开(公告)日：2011-05-19
申请号：PCT/EP2010064269
申请日：2010-09-27
申请人： SOLVAY , OLSCHIMKE JENS , BOMKAMP MARTIN , GROSSMANN ANDREAS
发明人： OLSCHIMKE JENS , BOMKAMP MARTIN , GROSSMANN ANDREAS
IPC分类号： C07D317/36 , C07D317/42
CPC分类号： C07D317/36 , C07D317/42
摘要： The present invention provides inter alia a method for handling fluorinated organic carbonates such that degradation reactions are minimized or even completely suppressed and hence initial purity of fluorinated organic carbonatesis essentially maintained during handling. The invention further provides compositions comprising a fluorinated organic carbonate with improved stability against degradation reactions. The compositions comprise equal to or less than 500 ppm of a Lewis acid.
摘要翻译：本发明尤其提供一种处理氟化有机碳酸酯的方法，使得降解反应最小化或甚至完全抑制，因此氟化有机碳酸酯的初始纯度在处理过程中基本维持。本发明进一步提供包含具有改进的降解反应稳定性的氟化有机碳酸酯的组合物。组合物包含等于或小于500ppm的路易斯酸。

15. 发明申请

WO2011051275A1 LITHIUM SULFUR BATTERY 审中-公开
标题翻译：锂硫电池
公开(公告)号：WO2011051275A1
公开(公告)日：2011-05-05
申请号：PCT/EP2010/066143
申请日：2010-10-26
申请人： SOLVAY FLUOR GmbH , OLSCHIMKE, Jens , BOMKAMP, Martin , EICHER, Johannes
发明人： OLSCHIMKE, Jens , BOMKAMP, Martin , EICHER, Johannes
IPC分类号： H01M12/08 , H01M10/052 , H01M10/0569 , H01M10/0568 , H01M10/05
CPC分类号： H01M12/08 , H01M4/134 , H01M4/38 , H01M4/381 , H01M4/382 , H01M10/05 , H01M10/052 , H01M10/0568 , H01M10/0569 , H01M2300/0025 , H01M2300/0068 , Y02E60/128 , Y02T10/7011
摘要： A lithium sulfur battery comprising at least one fluorosubstituted compound is described. Preferred fluorosubstituted compounds which are predominantly solvents are notably selected from the group consisting of fluorosubstituted carboxylic acid esters, fluorosubstituted carboxylic acid amides, fluorosubstituted fluorinated ethers, fluorosubstituted carbamates, fluorosubstituted cyclic carbonates, and fluorosubstituted acyclic carbonates fluorosubstituted ethers, perfluoroalkyl phosphoranes, fluorosubstituted phosphites, fluorosubstituted phosphates, fluorosubstituted phosphonates and fluorosubstituted heterocycles. Monofluoroethylene carbonate, cis-difluoroethylene carbonate, trans- difluoroethylene carbonate, 4,4- difluoroethylene carbonate, trifluoroethylene carbonate, tetrafluoroethylene carbonate, 4-fluoro-4-methyl-l,3-dioxolane-2-one, 4-fluoro-4-ethyl- 1,3-dioxolane-2-one, 2,2,2-trifluoroethyl-methyl carbonate, 2,2,2-trifluoroethyl-fluoromethyl carbonate are preferred. The solvent my further comprise non-fluorinated solvents, e.g. ethylene carbonate, a dialkyl carbonate or propylene carbonate. The invention also concerns the use of fluorinated compounds as additive for such batteries and specific electrolyte solutions.
摘要翻译：描述了包含至少一种氟取代的化合物的锂硫电池。主要是溶剂的优选氟取代的化合物特别选自氟取代的羧酸酯，氟取代的羧酸酰胺，氟取代的氟代醚，氟取代的氨基甲酸酯，氟取代的环状碳酸酯和氟取代的无环碳酸酯氟取代的醚，全氟烷基磷，氟取代的亚磷酸酯，氟取代的磷酸酯，氟取代的膦酸酯和氟取代的杂环。单氟代碳酸亚乙酯，顺式二氟亚乙基碳酸酯，反式二氟亚乙基碳酸酯，4,4-二氟亚乙基碳酸酯，三氟乙烯碳酸酯，四氟乙烯碳酸酯，4-氟-4-甲基-1,3-二氧戊环-2-酮，4-氟-4- 乙基-1,3-二氧戊环-2-酮，2,2,2-三氟乙基 - 甲基碳酸酯，2,2,2-三氟乙基 - 氟甲基碳酸酯。溶剂我还包括非氟化溶剂，例如碳酸亚乙酯，碳酸二烷基酯或碳酸亚丙酯。本发明还涉及氟化化合物作为这种电池和特定电解质溶液的添加剂的用途。

16. 发明申请

WO2011036283A2 MANUFACTURE OF DIFLUOROETHYLENE CARBONATE, TRIFLUOROETHYLENE CARBONATE AND TETRAFLUOROETHYLENE CARBONATE 审中-公开
标题翻译：碳酸二甲酯，三氟乙烯碳酸酯和四氟乙烯碳酸酯的制备
公开(公告)号：WO2011036283A2
公开(公告)日：2011-03-31
申请号：PCT/EP2010/064221
申请日：2010-09-27
申请人： SOLVAY FLUOR GmbH , OLSCHIMKE, Jens , SEFFER, Dirk , BOMKAMP, Martin
发明人： OLSCHIMKE, Jens , SEFFER, Dirk , BOMKAMP, Martin
IPC分类号： C07D317/36 , C07D317/42
CPC分类号： C07D317/36 , C07D317/42
摘要： Difluoroethylene carbonate, trifluoroethylene and tetrafluoroethylene carbonate are produced by the reaction between elemental fluorine and ethylene carbonate or fluorinated ethylene carbonates with a lower degree of fluorination.
摘要翻译：二氟乙烯碳酸酯，三氟乙烯和四氟乙烯碳酸酯通过元素氟和碳酸亚乙酯之间的反应或具有较低氟化度的氟化亚乙基碳酸酯的反应来制备。

17. 发明申请

WO2011020830A1 PROCESS FOR THE DESTILLATIVE PURIFICATION OF FLUOROETHYLENE CARBONATE 审中-公开
标题翻译：氟代乙烯碳酸酯的目的化学纯化方法
公开(公告)号：WO2011020830A1
公开(公告)日：2011-02-24
申请号：PCT/EP2010/061973
申请日：2010-08-17
申请人： SOLVAY FLUOR GMBH , LAMBERT, Alain , SOMMER, Christoph , KRUEGER, Harald , OLSCHIMKE, Jens
发明人： LAMBERT, Alain , SOMMER, Christoph , KRUEGER, Harald , OLSCHIMKE, Jens
IPC分类号： C07D317/42
CPC分类号： C07D317/42
摘要： Process for the destillative purification of fluoroethylene carbonate Crude fluoroethylene carbonate obtained by the fluorination of ethylene carbonate and elemental fluorine containing not more than 5 % by weight of HF is purified by at least two subsequent distillation steps. The bulk of HF can be removed, if desired,in a preliminary HF removal step, e.g. by stripping,before performing the distillation. Further,if desired, a second HF removal step can be performed by contacting the crude mixture or the distillate obtained after the first distillation step with an adsorbent for HF, e.g. silica gel. The distillation can be performed batch wise. It is preferred to perform it continuously. It yields purified fluoroethylene carbonate with an HF content of equal to or less than 30 ppm. The purified fluoroethylene carbonate can be applied as solvent additive for lithium ion batteries.
摘要翻译：氟代碳酸亚乙酯的游离纯化方法通过氟化碳酸亚乙酯和含有不超过5重量％HF的元素氟获得的粗氟代碳酸亚乙酯通过至少两个随后的蒸馏步骤纯化。如果需要，可以在初步HF去除步骤中除去大部分HF。通过汽提，然后进行蒸馏。此外，如果需要，可以通过使在第一蒸馏步骤后获得的粗混合物或蒸馏物与HF的吸附剂接触来进行第二HF去除步骤，例如。硅胶。蒸馏可以分批进行。优选连续执行。产生HF含量等于或小于30ppm的纯化氟代碳酸亚乙酯。纯化的碳酸亚乙酯可用作锂离子电池的溶剂添加剂。

18. 发明申请

WO2006045518A1 VERFAHREN ZUR GASTRENNUNG 审中-公开
标题翻译：工艺气体分离
公开(公告)号：WO2006045518A1
公开(公告)日：2006-05-04
申请号：PCT/EP2005/011267
申请日：2005-10-20
申请人： SOLVAY FLUOR GMBH , OLSCHIMKE, Jens , BRAUKMÜLLER, Saskia , BROSCH, Carsten
发明人： OLSCHIMKE, Jens , BRAUKMÜLLER, Saskia , BROSCH, Carsten
IPC分类号： C01B7/07 , C01B7/09 , B01D53/14 , C01B7/19 , C07C51/64 , C07D233/54
CPC分类号： C01B7/0737 , B01D53/1456 , B01D53/1493 , B01D2257/2042 , B01D2257/2045 , C01B7/0731 , C01B7/093 , C01B7/195 , C07C51/47 , C07D233/64 , C07C53/48 , C07C53/46 , C07C53/40
摘要： Gasgemische, die HF, HCI oder HBr und andere Bestandteile enthalten, insbesondere solche Gasgemische, die Carbonsäurefluoride, C(0)F 2 oder Phosphorpentafluorid sowie HCI und gegebenenfalls HF enthalten, können mittels ionischer Flüssigkeiten aufgetrennt werden.
摘要翻译：含有HF，HCl或HBr和其它成分的气体混合物，特别是含有羧酸氟化物的那些气体混合物，C（O）R _{2 或五氟化磷和HCl和任选的HF，可以通过离子液体的方法分离。}

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