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11. 发明授权

US06811596B1 Phase change inks with improved image permanence 失效
标题翻译：相变油墨具有改善的图像持久性
公开(公告)号：US06811596B1
公开(公告)日：2004-11-02
申请号：US10436177
申请日：2003-05-12
申请人： Christine E. Bedford , Marcel P. Breton , H. Bruce Goodbrand
发明人： Christine E. Bedford , Marcel P. Breton , H. Bruce Goodbrand
IPC分类号： C09D1100
CPC分类号： C09D11/34
摘要： Phase change inks comprising colorant, a phase change ink carrier, and an antioxidant or UV stabilizer of the formula wherein R1, R2, R3, R4, R5, R6, R7, R8, and R9 each, independently of the others, is hydrogen, hydroxy, amino, alkyl, aryl, arylaikyl, alkylaryl, alkoxy, aryloxy, arylalkyloxy, alkylaryloxy, halogen, cyano, aldehyde, ketone, ester, amide, sulfide, sulfoxide, nitrile, sulfone, acyl, or carboxylic acid, provided that at least one of R1, R2, R3, R4, R5, R6, R7, R8, and R9 is alkyl having at least about 8 carbon atoms, alkoxy having at least about 8 carbon atoms, aryl having at least about 6 carbon atoms, aryloxy having at least about 6 carbon atoms, arylalkyl having at least about 7 carbon atoms, arylalkyloxy having at least about 7 carbon atoms, alkylaryl having at least about 7 carbon atoms, or alkylaryloxy having at least about 7 carbon atoms.
摘要翻译：包含着色剂，相变油墨载体，以及R 1，R 2，R 3，R 4，R 5，R 6，R 7，R 8和R 9中的R 1，R 2，R 3，R 8和R 9的抗氧化剂或UV稳定剂的相变油墨，各自独立地为氢，羟基，氨基，烷基，芳基，芳基烷基，烷基芳基，烷氧基，芳氧基，芳烷氧基，烷基芳氧基，卤素，氰基，醛，酮，酯，酰胺，硫醚，亚砜，腈，砜，酰基或羧酸，条件是至少一个的R 1，R 2，R 3，R 4，R 5，R 6，R 7，R 8和R 9是具有至少约8个碳原子的烷基，具有至少约8个碳原子的烷氧基，具有至少约6个碳原子的芳基，至少约6个碳原子，具有至少大约7个碳原子的芳基烷基，具有至少大约7个碳原子的芳基烷氧基，具有至少约7个碳原子的烷基芳基，或至少约7个碳原子的烷基芳氧基。

12. 发明授权

US07347892B2 Phase change inks containing modified pigment particles 失效
标题翻译：含改性颜料颗粒的相变油墨
公开(公告)号：US07347892B2
公开(公告)日：2008-03-25
申请号：US10918808
申请日：2004-08-13
申请人： Christine E Bedford , Marcel P Breton
发明人： Christine E Bedford , Marcel P Breton
IPC分类号： C09D11/02
CPC分类号： C09D11/34
摘要： Disclosed is a phase change ink composition comprising (a) an ink carrier comprising (1) a polyalkylene wax and (2) a component selected from the group consisting of (A) amides, (B) esters, (C) ester-amides, (D) urethanes, (E) ureas, (F) urethane-ureas, and (G) mixtures thereof, and (b) pigment particles having hydrophobic functional groups covalently bonded to the surfaces thereof, said ink composition having a melting point no lower than about 40° C., said ink composition having a melting point no higher than about 160° C.
摘要翻译：公开了一种相变油墨组合物，其包含（a）油墨载体，其包含（1）聚亚烷基蜡和（2）选自（A）酰胺，（B）酯，（C）酯 - 酰胺，（D）聚氨酯，（E）脲，（F）氨基甲酸酯脲和（G）它们的混合物，和（b）具有与其表面共价结合的疏水官能团的颜料颗粒，所述油墨组合物的熔点不低所述油墨组合物的熔点不高于约160℃。

13. 发明申请

US20070119340A1 Ink carriers containing nanoparticles, phase change inks including same and methods for making same 有权
标题翻译：含有纳米颗粒的油墨载体，包含其的相变油墨及其制备方法
公开(公告)号：US20070119340A1
公开(公告)日：2007-05-31
申请号：US11291540
申请日：2005-11-30
申请人： Marcel P. Breton , Adela Goredema , Christine E. Bedford , Christopher Wagner , Sandra Gardner , Nan-Xing Hu , Bruce Goodbrand
发明人： Marcel P. Breton , Adela Goredema , Christine E. Bedford , Christopher Wagner , Sandra Gardner , Nan-Xing Hu , Bruce Goodbrand
IPC分类号： C09D11/02
CPC分类号： C09D11/34
摘要： Disclosed is an ink carrier and a method for forming same, and a phase change ink including same. The ink carrier comprises a colloidal dispersion of at least one of silica nanoparticles and metal oxide nanoparticles. The ink carrier can also include a low melting wax, and a gelling agent. The ink carrier exhibits a substantially uniform distribution of the nanoparticles so that they are discretely distributed therewithin, and are substantially resistant to the aggregation of the nanoparticles distributed therewithin.
摘要翻译：公开了一种油墨载体及其形成方法，以及包含它的相变油墨。油墨载体包括二氧化硅纳米颗粒和金属氧化物纳米颗粒中的至少一种的胶体分散体。油墨载体还可以包括低熔点蜡和胶凝剂。油墨载体表现出基本均匀的纳米颗粒分布，使得它们在其中离散分布，并且基本上抵抗分布在其中的纳米颗粒的聚集。

14. 发明授权

US07220300B2 Phase change inks containing bis(urea-urethane) compounds 有权
标题翻译：含有双（脲 - 氨基甲酸酯）化合物的相变油墨
公开(公告)号：US07220300B2
公开(公告)日：2007-05-22
申请号：US11004333
申请日：2004-12-04
申请人： Adela Goredema , Rina Carlini , Christine E. Bedford , Marcel P. Breton
发明人： Adela Goredema , Rina Carlini , Christine E. Bedford , Marcel P. Breton
IPC分类号： C09D11/02
CPC分类号： C08G18/2825 , C08G18/3228 , C08G18/324 , C08G18/6715 , C08G18/73 , C09D11/34
摘要： Disclosed is a phase change ink composition comprising a phase change ink carrier and a bis(urea-urethane) compound of the formula wherein R1 and R1′ each, independently of the other, is an alkyl group, an aryl group, an arylalkyl group, or an alkylaryl group, R2 and R2′ each, independently of the other, is an alkylene group, an arylene group, an arlyalkylene group, or an alkylarylene group, R3 is an alkylene group, an arylene group, an arylalkylene group, or an alkylarylene group, and R4 and R5 each independently of the other, is a hydrogen atom or an alkyl group.
摘要翻译：公开了一种相变油墨组合物，其包含相变油墨载体和下式的双（脲 - 氨基甲酸酯）化合物，其中R 1和R 2各自独立地为另一个是烷基，芳基，芳基烷基或烷基芳基，R 2和R 2各自独立地是一个亚烷基，亚芳基，芳亚烷基或烷基亚芳基，R 3是亚烷基，亚芳基，芳基亚烷基或烷基亚芳基，R 4， / SUB和R 5各自独立地是氢原子或烷基。

15. 发明授权

US07202883B2 Heterogeneous reactive ink composition 有权
标题翻译：非均相反应性油墨组成
公开(公告)号：US07202883B2
公开(公告)日：2007-04-10
申请号：US11008628
申请日：2004-12-10
申请人： Marcel P. Breton , Guerino G. Sacripante , Christine E. Bedford
发明人： Marcel P. Breton , Guerino G. Sacripante , Christine E. Bedford
IPC分类号： G01D11/00
CPC分类号： C09D133/068 , C08L67/00 , C09D11/30 , C08L2666/02 , C08L2666/18
摘要： An ink composition includes a colorant, a reactive polymer latex such as an epoxy copolymer latex, an optional dissipatable polymer, a dispersant such as a sulfonated polyester, and a liquid vehicle such as water. The ink composition is a stable liquid at ambient temperature, but becomes a gel upon heating or removal of part of the liquid vehicle.
摘要翻译：油墨组合物包括着色剂，反应性聚合物胶乳如环氧共聚物胶乳，任选的可分散聚合物，分散剂如磺化聚酯，以及液体载体如水。油墨组合物在环境温度下是稳定的液体，但在加热或除去部分液体载体时变成凝胶。

16. 发明授权

US06878198B1 Phase change inks and process for the preparation thereof 有权
标题翻译：相变油墨及其制备方法
公开(公告)号：US06878198B1
公开(公告)日：2005-04-12
申请号：US10722164
申请日：2003-11-25
申请人： Stephan V. Drappel , Marcel P. Breton , James D. Mayo , Raymond W. Wong , Christine E. Bedford , Danielle C. Boils-Boissier , Sandra J. Gardner , Paul F. Smith
发明人： Stephan V. Drappel , Marcel P. Breton , James D. Mayo , Raymond W. Wong , Christine E. Bedford , Danielle C. Boils-Boissier , Sandra J. Gardner , Paul F. Smith
IPC分类号： C09D11/00
CPC分类号： C09D11/34
摘要： Phase change ink compositions comprising (a) an ink carrier comprising a monoamide and a tetra-amide, and (b) pigment particles having oxygen-containing functional groups on the surfaces thereof. Also, processes for preparing a phase change ink which comprise (a) melting a tetra-amide which is solid at about 25° C.; (b) admixing with the molten tetra-amide pigment particles having oxygen-containing functional groups on the surfaces thereof; (c) maintaining the mixture of pigment and tetra-amide at a temperature of at least about 100° C. and at a temperature of no more than about 200° C. for a period sufficient to enable the molten tetra-amide to wet the pigment particle surfaces; (d) subsequent to wetting of the pigment particle surfaces with the molten tetra-amide, adding to the mixture a monoamide; (e) subsequent to addition of the monoamide, subjecting the resulting mixture to high shear mixing; and (f) subsequent to subjecting the mixture to high shear mixing, optionally adding to the mixture additional ink ingredients.
摘要翻译：相变油墨组合物，其包含（a）包含单酰胺和四酰胺的油墨载体，和（b）在其表面上具有含氧官能团的颜料颗粒。另外，制备相变油墨的方法包括（a）在约25℃熔化固体的四酰胺; （b）与表面具有含氧官能团的熔融四酰胺颜料颗粒混合; （c）将颜料和四酰胺的混合物在至少约100℃的温度和不超过约200℃的温度下保持足以使熔融的四酰胺湿润的时间颜料颗粒表面; （d）在用四酰胺熔融物润湿颜料颗粒表面之后，向混合物中加入单酰胺; （e）在加入单酰胺后，将所得混合物进行高剪切混合; 和（f）在混合物进行高剪切混合之后，任选地向混合物中加入另外的油墨成分。

17. 发明授权

US06583234B2 Process for preparing waterfastness additive 失效
标题翻译：防水添加剂的制备方法
公开(公告)号：US06583234B2
公开(公告)日：2003-06-24
申请号：US09915430
申请日：2001-07-26
申请人： Sheau V. Kao , Daniel A. Foucher , Mohammad J. Hossain , Christine E. Bedford , George Liebermann
发明人： Sheau V. Kao , Daniel A. Foucher , Mohammad J. Hossain , Christine E. Bedford , George Liebermann
IPC分类号： C08F204
CPC分类号： C08F26/04
摘要： Disclosed is a process which comprises (a) reacting allyl bromide with diethyl amine in a molar ratio of at least about 1 mole of allyl bromide per about 1.15 moles of diethyl amine and in a molar ratio of no more than about 1 mole of allyl bromide per about 2 moles of diethyl amine, thereby generating allyl diethyl amine in a monomer reaction mixture; (b) subsequently filtering the monomer reaction mixture to remove impurities; (c) subsequently reacting the allyl diethyl amine with allyl bromide, thereby generating solid diallyl diethyl ammonium bromide; (d) subsequently isolating the solid diallyl diethyl ammonium bromide; (e) subsequently dissolving the diallyl diethyl ammonium bromide in a solvent and adding thereto a polymerization initiator to form a polymerization reaction mixture; (f) subsequently heating the polymerization reaction mixture in a vessel equipped with a reflux condenser to a temperature of from about 90 to about 100° C., thereby generating poly(diallyl diethyl ammonium bromide); and (g) subsequently optionally isolating the poly(diallyl diethyl ammonium bromide) from the polymerization reaction mixture.
摘要翻译：公开了一种方法，其包括（a）烯丙基溴与二乙基胺的摩尔比为至少约1摩尔烯丙基溴/约1.15摩尔二乙胺和摩尔比不超过约1摩尔烯丙基溴每2摩尔二乙胺，从而在单体反应混合物中产生烯丙基二乙胺; （b）随后过滤单体反应混合物以除去杂质; （c）随后使烯丙基二乙胺与烯丙基溴反应，从而产生固体二烯丙基二乙基溴化铵; （d）随后分离固体二烯丙基二乙基溴化铵; （e）随后将二烯丙基二甲基溴化铵溶解在溶剂中并加入聚合引发剂以形成聚合反应混合物; （f）随后将装有回流冷凝器的容器中的聚合反应混合物加热至约90至约100℃的温度，从而产生聚（二烯丙基二乙基溴化铵）; 和（g）随后任选地从聚合反应混合物中分离聚（二烯丙基二乙基溴化铵）。

18. 发明授权

US07655084B2 Carbon black inks and method for making same 失效
标题翻译：炭黑油墨及其制造方法
公开(公告)号：US07655084B2
公开(公告)日：2010-02-02
申请号：US11301732
申请日：2005-12-12
申请人： Raymond W. Wong , Marcel P. Breton , Christine E. Bedford , Adela Goredema , Caroline Turek
发明人： Raymond W. Wong , Marcel P. Breton , Christine E. Bedford , Adela Goredema , Caroline Turek
IPC分类号： C09D11/00
CPC分类号： C09D11/34
摘要： Disclosed is a phase change carbon black ink composition comprising 1) a low polarity ink carrier comprising (A) a low polarity wax, optionally (B) an ester-terminated polyamide, (2) a dispersant, and (3) a carbon black colorant. The ink can be resistant to substantial aggregation and settling of the carbon black colorant in the melt and up to about the jetting temperature of the ink even when exposed to freeze thaw cycles.
摘要翻译：公开了一种相变炭黑油墨组合物，其包含1）低极性油墨载体，其包含（A）低极性蜡，任选地（B）酯封端的聚酰胺，（2）分散剂，和（3）炭黑着色剂。油墨可以抵抗熔体中炭黑着色剂的大量聚集和沉降，并且甚至在暴露于冻融循环时高达油墨的喷射温度。

19. 发明授权

US07563314B2 Ink carriers containing nanoparticles, phase change inks including same and methods for making same 有权
标题翻译：含有纳米颗粒的油墨载体，包含其的相变油墨及其制备方法
公开(公告)号：US07563314B2
公开(公告)日：2009-07-21
申请号：US11291540
申请日：2005-11-30
申请人： Marcel P. Breton , Adela Goredema , Christine E. Bedford , Christopher Wagner , Sandra Gardner , Nan-Xing Hu , Bruce Goodbrand
发明人： Marcel P. Breton , Adela Goredema , Christine E. Bedford , Christopher Wagner , Sandra Gardner , Nan-Xing Hu , Bruce Goodbrand
IPC分类号： C09D11/00
CPC分类号： C09D11/34
摘要： Disclosed is an ink carrier and a method for forming same, and a phase change ink including same. The ink carrier comprises a colloidal dispersion of at least one of silica nanoparticles and metal oxide nanoparticles. The ink carrier can also include a low melting wax, and a gelling agent. The ink carrier exhibits a substantially uniform distribution of the nanoparticles so that they are discretely distributed therewithin, and are substantially resistant to the aggregation of the nanoparticles distributed therewithin.
摘要翻译：公开了一种油墨载体及其形成方法，以及包含它的相变油墨。油墨载体包括二氧化硅纳米颗粒和金属氧化物纳米颗粒中的至少一种的胶体分散体。油墨载体还可以包括低熔点蜡和胶凝剂。油墨载体表现出基本均匀的纳米颗粒分布，使得它们在其中离散分布，并且基本上抵抗分布在其中的纳米颗粒的聚集。

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