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111. 发明授权

US06585941B2 Apparatus and process for filling and emptying a vessel charged with flammable and aggressive gas 失效
标题翻译：用于填充和排空装有易燃和侵蚀性气体的容器的装置和方法
公开(公告)号：US06585941B2
公开(公告)日：2003-07-01
申请号：US09373724
申请日：1999-08-13
申请人： Lothar Zehe , Mieczyslaw Kuzma , Hartwig Rauleder
发明人： Lothar Zehe , Mieczyslaw Kuzma , Hartwig Rauleder
IPC分类号： B01J808
CPC分类号： C01B33/1071 , B01J8/003 , B01J8/0035 , B01J8/125 , B01J2208/00212 , B01J2208/00752 , B01J2219/00033 , B01J2219/00245 , B65G53/4691 , C01B3/06 , Y02E60/36 , Y10T137/3127 , Y10T137/4259 , Y10T137/88054
摘要： An apparatus safely fills and empties a pressurized vessel charged with flammable and/or reactive gas. The apparatus features an upper flap combination, an intermediate lock vessel having a flushing apparatus, and a lower flap combination. The present invention also relates to a pressurized reactor which is charged with flammable and/or reactive gas and is equipped with a filling lock apparatus and an emptying lock apparatus for the simultaneous preparation of tetrachlorosilane, trichlorosilane and hydrogen. In addition, the present invention relates to a special process for filling and emptying such a reactor.
摘要翻译：装置安全地填充和排空装有可燃和/或反应气体的加压容器。该装置具有上部翼片组合，具有冲洗装置的中间锁定容器和下部翼片组合。本发明还涉及一种带有易燃和/或反应性气体的加压反应器，并且配备有用于同时制备四氯硅烷，三氯硅烷和氢气的填充锁定装置和排空锁定装置。此外，本发明涉及一种用于填充和排空这种反应器的特殊方法。

112. 发明授权

US06294682B1 Alkoxides with alkaline earths and titanium, zirconium and/or hafnium, their production and use 失效
标题翻译：碱土金属和钛，锆和/或铪，其生产和使用
公开(公告)号：US06294682B1
公开(公告)日：2001-09-25
申请号：US09077671
申请日：2000-06-19
申请人： Hartwig Rauleder , Burkhard Standke , Michael Horn , Hans-Joachim Kotzsch , Hans-Gunther Srebny
发明人： Hartwig Rauleder , Burkhard Standke , Michael Horn , Hans-Joachim Kotzsch , Hans-Gunther Srebny
IPC分类号： C07F1900
CPC分类号： D21H25/18 , C07F7/003 , C08F10/00 , C08F4/6548
摘要： The invention concerns solutions of alkoxides containing titanium and/or zirconium and/or hafnium and magnesium and/or calcium and/or strontium and/or barium of general formula (I): [MII(OR)2-y(OR1)y]n.[MIV(OR1)4-z(OR)2], in which: MII means magnesium and/or calcium and/or strontium and/or barium; MIV titanium and/or zirconium and/or hafnium; R is an alkyl group with 1 to 18 carbon atoms; R1 is an alkyl group with 1 to 18 carbon atoms, y has a value of between 0 to 2; z has a value of 0 and 4; and n is a number between 0.001 and 3, with the exception that n cannot be 1 when y is 2 and z is 0, or when y is 0 and z is 4. The invention further concerns the production of these alkoxides and their use.
摘要翻译：本发明涉及含有钛和/或铪和/或铪以及通式（I）的镁和/或钙和/或锶和/或钡的醇盐的溶液：[MII（OR）2-y（OR 1）y] n。[MIV（OR1）4-z（OR）2]，其中：MII表示镁和/或钙和/或锶和/或钡; MIV钛和/或锆和/或铪; R是具有1至18个碳原子的烷基; R1是具有1至18个碳原子的烷基，y具有在0至2之间的值; z的值为0和4; 并且n是0.001至3之间的数字，除了当y为2且z为0时，或当y为0且z为4时，n不能为1时。本发明还涉及这些醇盐的生产及其用途。

113. 发明授权

US5210334A Process for the preparation of alkaline earth metal alkylates having a spherical particle form 失效
标题翻译：制备具有球形颗粒形式的碱金属金属烷基化物的方法
公开(公告)号：US5210334A
公开(公告)日：1993-05-11
申请号：US807271
申请日：1991-12-13
申请人： Burkhart Standke , Hartwig Rauleder , Harald-Jurgen Biangardi , Hans-Joachim Kotzsch
发明人： Burkhart Standke , Hartwig Rauleder , Harald-Jurgen Biangardi , Hans-Joachim Kotzsch
IPC分类号： C07C29/70 , C07C29/68 , C07C31/30 , C08F4/02 , C08F10/00
CPC分类号： C07C29/68 , C08F10/00
摘要： Alkaline earth metal alkylates having a spherical particle habit are prepared by dissolving an alkaline earth metal alkylate in a solvent, adding a second solvent which dissolves the alkaline earth metal alkylate only with difficulty or does not dissolve it at all, but which is homogeneously miscible with the solution of the alkaline earth metal alkylate in the first solvent, removing the first solvent and then removing the second solvent. The particle size can be controlled by means of the shear gradient during the precipitation or by the use of emulsion stabilizers. Emulsion stabilization leads to particles in the size range 0.5 to 20 .mu.m with a particularly narrow particle size distribution. Catalysts for polyolefin synthesis can be prepared on the basis of magnesium alkylates prepared by the process according to the invention. The polymer is advantageous with respect to particle habit and particle size distribution, compared with the prior art. A narrower particle size distribution, and thus a reduction in undesired oversize and undersized particles, and a smoother surface structure are achieved.
摘要翻译：通过将碱土金属烷基化物溶解在溶剂中来制备具有球形颗粒习惯的碱土金属烷基化物，仅添加溶解碱土金属烷基化物的第二溶剂难以完全溶解，或者完全不溶解，但是均匀混溶将碱土金属烷基化物溶于第一溶剂中，除去第一溶剂，然后除去第二溶剂。可以通过沉淀过程中的剪切梯度或使用乳液稳定剂来控制粒度。乳液稳定化导致尺寸范围为0.5至20μm的颗粒，具有特别窄的粒度分布。用于聚烯烃合成的催化剂可以基于通过根据本发明的方法制备的烷基烷基镁来制备。与现有技术相比，聚合物在颗粒习性和粒度分布方面是有利的。实现了较窄的粒度分布，从而减少了不想要的过大尺寸和尺寸过小的颗粒，并且实现了更平滑的表面结构。

114. 发明授权

US5053560A Method for the continuous production of potassium tert-butoxide 失效
标题翻译：连续生产叔丁醇钾的方法
公开(公告)号：US5053560A
公开(公告)日：1991-10-01
申请号：US363292
申请日：1989-06-07
申请人： Rheinhard Matthes , Hartwig Rauleder , Hans-Joachim Vahlensieck
发明人： Rheinhard Matthes , Hartwig Rauleder , Hans-Joachim Vahlensieck
IPC分类号： C07C27/00 , C07C29/70 , C07C31/30 , C07C67/00
CPC分类号： C07C29/70
摘要： A method for the continuous production of anhydrous potassium tert-butoxide in a packed distillation column, wherein aqueous potash lye is fed with excess tert-butyl alcohol to the top of the column. Water formed in the reaction as well as water brought in with the reactants is distilled out at the top using methylcyclohexane or n-heptane as withdrawing agent. The amount of the withdrawing agent and of the tert-butanol must be selected such that above the column boiler a content between 0.2 and 2 wt.-% of the withdrawing agent is present in the gas mixture, while the gas mixture in the middle of the column has either between 32 and 34 wt.-% of methylcyclohexane or 36 to 38 wt.-% of n-heptane. The water together with the withdrawing agent and tert-butanol is withdrawn from the top of the column and then condensed. The organic phase of the condensate is fed back to the column.
摘要翻译：在填充蒸馏塔中连续生产无水叔丁醇钾的方法，其中将钾盐水溶液加入到塔顶部的过量叔丁醇。在反应中形成的水以及与反应物一起引入的水在顶部使用甲基环己烷或正庚烷作为萃取剂被蒸馏出来。取出剂和叔丁醇的量必须选择为使得在塔式锅炉以上，在气体混合物中存在取出剂的0.2至2重量％的含量，而在中间的气体混合物该柱具有32至34重量％的甲基环己烷或36至38重量％的正庚烷。将水与萃取剂和叔丁醇一起从塔顶排出，然后冷凝。将冷凝物的有机相反馈回塔中。

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