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101. 发明申请

US20050004386A1 Organosilicon compounds 有权
标题翻译：有机硅化合物
公开(公告)号：US20050004386A1
公开(公告)日：2005-01-06
申请号：US10902572
申请日：2004-07-30
申请人： Ulrich Deschler , Roland Krafczyk , Hans-Detlef Luginsland , Karsten Korth , Ingo Kiefer , Michael Horn
发明人： Ulrich Deschler , Roland Krafczyk , Hans-Detlef Luginsland , Karsten Korth , Ingo Kiefer , Michael Horn
IPC分类号： C07B61/00 , C07F7/18 , C08K5/5419 , C08L21/00
CPC分类号： C08K5/544 , C07F7/1804 , C08K5/548 , C08L21/00
摘要： Organosilicon compounds of the general formula I and/or II are produced by reacting silanes of the general formula III with alcohols of the general formula R′—OH, with elimination of R—OH, wherein R—OH may be continuously separated from the reaction mixture by distillation. The organosilicon compounds may be used in rubber mixtures. Compounds, such as rubbers, produced using such organosilicon compounds.
摘要翻译：通式I和/或II的有机硅化合物是通过使通式III的硅烷与通式R'-OH的醇反应，同时除去R-OH，其中R-OH可与反应物连续分离通过蒸馏混合。有机硅化合物可用于橡胶混合物中。使用这种有机硅化合物制备的化合物，例如橡胶。

102. 发明授权

US06767982B2 Continuous manufacturing process for organoalkoxysiloxanes 有权
标题翻译：有机烷氧基硅氧烷的连续制造工艺
公开(公告)号：US06767982B2
公开(公告)日：2004-07-27
申请号：US09987267
申请日：2001-11-14
申请人： Burkhard Standke , Michael Horn
发明人： Burkhard Standke , Michael Horn
IPC分类号： C08G7706
CPC分类号： C08G77/18 , C07F7/0872 , C08G77/06 , C09D4/00 , C09D183/04 , C08G77/04
摘要： A mixture of organoalkoxysiloxanes of formula I: wherein R and R″ are identical or different and are methyl, ethyl, vinyl, n-propyl, i-propyl, &ggr;-chloropropyl, n-butyl, i-butyl, n-pentyl, i-pentyl, n-hexyl, i-hexyl, n-heptyl, i-heptyl, n-octyl, i-octyl, hexadecyl, octadecyl or alkoxy, R′ represents methyl or ethyl, n and m are identical or different and each is 0 or an integer ranging from 1 to 20, on the condition that (n+m)≧2, is prepared by: reacting in a first stage the constituents of (i) an organotrichlorosilane or a mixture of organotrichlorosilanes or a mixture of at least one organotrichlorosilane and tetrachlorosilane, (ii) water and (iii) alcohol, combined in a molar ratio (i):(ii):(iii) of 1:(0.59 to 0.95):(0.5 to 100), at a temperature of 0 to 150° C., which produces hydrogen chloride as a product which is removed from the system and the crude organoalkoxysiloxane product is transferred proportionately to the reaction distillation column of a subsequent second stage after an average dwell time of 0.5 to 180 minutes; and conducting reaction and distillation in the reaction distillation column in a second stage in which volatile constituents are withdrawn from the top of the column and the organoalkoxysiloxane product is withdrawn as a bottom product, wherein the reaction-distillation column is operated at a bottom temperature of 50 to 200° C.
摘要翻译：式I的有机烷氧基硅氧烷的混合物：其中R和R“相同或不同，是甲基，乙基，乙烯基，正丙基，异丙基，γ-氯丙基，正丁基，异丁基，正戊基，正戊基，正己基，异己基，正庚基，异庚基，正辛基，异辛基，十六烷基，十八烷基或烷氧基，R'表示甲基或乙基，n和m相同或不同，在（n + m）> = 2的条件下，为0或1〜20的整数，通过以下步骤制备：在第一阶段中使（i）有机三氯硅烷或有机三氯硅烷的混合物的组分或至少一种有机三氯硅烷和四氯硅烷，（ii）以1：（0.59至0.95）：（0.5至100）的摩尔比（i）：（ii）：（iii）组合的水和（iii）醇，温度为0至150℃，其产生作为从系统中除去的产物的氯化氢，粗有机烷氧基硅氧烷产物按比例转移到随后的第二阶段的反应蒸馏塔af 平均停留时间为0.5至180分钟; 在反应蒸馏塔中的第二阶段进行反应和蒸馏，其中挥发性成分从塔顶排出，有机烷氧基硅氧烷产物作为底部产物排出，其中反应蒸馏塔在底部温度为50℃ 至200℃

103. 发明授权

US06713186B1 Fluoroalkyl-functional organosiloxane-containing compositions based on alcohol, a process for their preparation and their use 失效
标题翻译：基于醇的含氟烷基官能的有机硅氧烷的组合物，其制备方法及其用途
公开(公告)号：US06713186B1
公开(公告)日：2004-03-30
申请号：US09685341
申请日：2000-10-11
申请人： Peter Jenkner , Albert-Johannes Frings , Michael Horn , Eckhard Just , Jaroslaw Monkiewicz , Burkhard Standke
发明人： Peter Jenkner , Albert-Johannes Frings , Michael Horn , Eckhard Just , Jaroslaw Monkiewicz , Burkhard Standke
IPC分类号： B32B1500
CPC分类号： C09K3/18 , C03C25/40 , C08G77/24 , C09D183/08 , D06M13/513 , D06M15/657 , D21H19/32 , D21H21/16 , Y10T428/31663
摘要： An alcoholic fluoroalkyl-functional group containing organosiloxane based composition prepared is prepared by the controlled hydrolysis of at least one fluoroalkyl-functional group containing organosilane of formula I: R1—Y—(CH2)2SiHx(R2)y(OR)3−x−y (I), in which R1 is a mono, oligo- or perfluorinated alkyl group having 1-9 C atoms or a mono-, oligo- or perfluorinated aryl group, Y is a CH2, O or S group, R2 and R are each independently a linear, branched or cyclic alkyl group having 1-8 C atoms or an aryl group and x=0, 1 or 2 and y=0, 1 or 2, where (x+y)≦2, at a temperature in the range of 0-120° C. over a period of 0.5-24 hours and with thorough mixing in an w alcoholic medium which contains water and a weak mono- or polybasic acid or a weak base or a weak mono- or polybasic acid and a weak base or an acid or basic salt, the water employed and the alkoxysilane employed being in a molar ratio of 2-500:1.
摘要翻译：制备的含有机硅氧烷的组合物的含氟烷基官能团的组合物是通过控制水解至少一个含有氟代烷基官能团的式I有机硅烷来制备的：其中R 1是具有1-羟基的单，低聚或全氟化的烷基， 9个C原子或单，低聚或全氟化芳基，Y为CH 2，O或S基团，R 2和R 3各自独立地为具有1-8个C原子的直链，支链或环状烷基或芳基和x = 0,1或2，y = 0,1或2，其中（x + y）<= 2，在0〜120℃的温度下，在0.5-24小时内并且在含有水和弱单或多元酸或弱碱或弱单或多元酸和弱碱或酸或碱性盐的w-醇介质中充分混合，使用的水和使用的烷氧基硅烷摩尔比为2-500:1。

104. 发明授权

US06534667B1 Water-based composition of amino-functional silicon compounds 有权
标题翻译：氨基官能硅化合物的水基组成
公开(公告)号：US06534667B1
公开(公告)日：2003-03-18
申请号：US09514356
申请日：2000-02-28
申请人： Burkhard Standke , Roland Edelmann , Albert-Johannes Frings , Michael Horn , Peter Jenkner , Ralf Laven , Helmut Mack , Jaroslaw Monkiewicz , Günter Switalla
发明人： Burkhard Standke , Roland Edelmann , Albert-Johannes Frings , Michael Horn , Peter Jenkner , Ralf Laven , Helmut Mack , Jaroslaw Monkiewicz , Günter Switalla
IPC分类号： C07F708
CPC分类号： C08K5/544 , C08K5/549 , C09D183/08 , C23C2222/20 , C08L83/08 , C08L2666/34
摘要： A composition which comprises a mixture of water-soluble, amino-functional silicon compounds which are essentially free from alkoxy groups, water, optionally a content of alcohol and optionally a content of acid, the composition comprising silicon compounds of the general formula I: NH2[CH2)2NH]x(CH2)3SiO1.5 (I) in which x is 0, 1 or 2, and of the general formula II: (SiO1.5(CH2)3[NH(CH2)2]yNH[(CH2)2NH]x(CH2)3Si)1.5 (II) in which y and z are 0, 1 or 2 and are identical or different. The compositions are obtainable by mixing corresponding aminoalkoxy silanes, hydrolyzing the mixture and removing the hydrolysis alcohol formed as a result. The invention furthermore relates to a process for the preparation of the compositions and to their use in a wide variety of applications.
摘要翻译：包含基本上不含烷氧基的水溶性，氨基官能的硅化合物的混合物的组合物，水，任选的醇含量和任选的酸的含量，所述组合物包含通式I的硅化合物：在其中x为0,1或2，通式II：其中y和z为0,1或2并且相同或不同。组合物可通过混合相应的氨基烷氧基硅烷，水解混合物并除去水解因此形成酒精。本发明还涉及制备组合物的方法及其在各种应用中的用途。

105. 发明授权

US06403228B1 Functional organylorganyloxysilanes on a carrier in cable compounds 失效
标题翻译：电缆化合物中载体上的功能性有机酰基氧基硅烷
公开(公告)号：US06403228B1
公开(公告)日：2002-06-11
申请号：US09604273
申请日：2000-06-26
申请人： Helmut Mack , Ralf Laven , Peter Jenkner , Roland Edelmann , Dieter Barfurth , Albert-Johannes Frings , Burkhard Standke , Jaroslaw Monkiewicz , Michael Horn
发明人： Helmut Mack , Ralf Laven , Peter Jenkner , Roland Edelmann , Dieter Barfurth , Albert-Johannes Frings , Burkhard Standke , Jaroslaw Monkiewicz , Michael Horn
IPC分类号： B32B904
CPC分类号： H01B3/44 , Y10T428/31663 , Y10T428/31801 , Y10T428/31855
摘要： The invention relates to the use of (1) a liquid functional organylorganyloxysilane bound to a carrier, or of a liquid (co)condensate derived from a functional organylorganyloxysilane and bound to a carrier for preparing cable compounds which comprise (2) a thermoplastic base polymer having polar functional groups and (3) a reinforcing or extending mineral filler.
摘要翻译：本发明涉及（1）与载体或衍生自功能性有机酰基氧基硅烷的液体（共）缩合物结合并结合到用于制备电缆化合物的载体的液体功能性有机羧基氧基硅烷的用途，其包含（2）热塑性基础聚合物具有极性官能团和（3）增强或延伸的矿物填料。

106. 发明授权

US06398917B1 Apparatus for the purification of commercially available diphenyl-p-phenylenediamine (DPPD) 失效
标题翻译：用于纯化市售二苯基对苯二胺（DPPD）的设备
公开(公告)号：US06398917B1
公开(公告)日：2002-06-04
申请号：US09480481
申请日：2000-01-11
申请人： Albert-Johannes Frings , Michael Horn , Peter Jenker , Jaroslaw Monkiewicz , Hans-Guenther Srebny , Burkhard Standke , Bertram Trautvetter
发明人： Albert-Johannes Frings , Michael Horn , Peter Jenker , Jaroslaw Monkiewicz , Hans-Guenther Srebny , Burkhard Standke , Bertram Trautvetter
IPC分类号： B01D300
CPC分类号： C07C211/55 , B01D11/028 , B01D11/0288 , C07C209/84 , Y10S203/17
摘要： An apparatus for the purification of crude N,N′-diphenyl-p-phenylenediamine (DPPD) in which there is an extraction unit containing a liquid permeable container and an adsorption layer downstream of the container, a solvent evaporator downstream of the adsorption layer, a filter unit, a line for returning the filtrate to the solvent evaporator, and a condenser for returning solvent to the extraction unit.
摘要翻译：用于净化粗N，N'-二苯基对苯二胺（DPPD）的装置，其中存在含有液体可渗透容器的萃取单元和容器下游的吸附层，在吸附层下游的溶剂蒸发器，过滤器单元，将滤液返回到溶剂蒸发器的管线和用于将溶剂返回到萃取单元的冷凝器。

107. 发明授权

US06228936B1 Fluoroalkyl-functional organopolysiloxane-containing compositions 失效
标题翻译：含氟烷基官能的含有机聚硅氧烷的组合物
公开(公告)号：US06228936B1
公开(公告)日：2001-05-08
申请号：US09228641
申请日：1999-01-12
申请人： Burkhard Standke , Roland Edelmann , Albert-Johannes Frings , Ralf Laven , Michael Horn , Peter Jenkner , Helmut Mack , Jaroslaw Monkiewicz
发明人： Burkhard Standke , Roland Edelmann , Albert-Johannes Frings , Ralf Laven , Michael Horn , Peter Jenkner , Helmut Mack , Jaroslaw Monkiewicz
IPC分类号： C08L8308
CPC分类号： C14C9/00 , C03C17/30 , C03C25/40 , C04B41/4961 , C08G77/22 , C08G77/24 , C08G77/26 , C09D183/08 , C09K3/18 , C23C30/00 , C23C2222/20 , D06M15/657 , D06M2101/06 , D06M2200/11 , D06M2200/12 , Y10T428/31663
摘要： The present invention provides an aqueous alcoholic fluoroalkyl functional group containing organopolysiloxane composition, which includes organopolysiloxanes of formula I: RO{Si(A)(CH3)z(OR)1−zO}a{Si(B)(R2)y(OR)1−yO}b{Si(C)(CH3)O}c{Si(D)(OR)O}dR.(HX)e (I) wherein A, B, C, D, R, R2, X, z, y, a, b, c, d and e are defined in the claims. The present invention also provides methods for making the fluoroalkyl functional group containing organopolysiloxane composition as well as methods of using same.
摘要翻译：本发明提供含有有机聚硅氧烷组合物的含水醇的氟代烷基官能团，其包括式I的有机聚硅氧烷：其中A，B，C，D，R，R 2，X，z，y，a，b，c，d和e是在权利要求中限定。本发明还提供了制备含氟烷基官能团的有机聚硅氧烷组合物的方法以及使用它们的方法。

108. 发明授权

US06177584B1 Process for neutralizing and reducing residual halogen contents in alkoxysilanes or alkoxysilane-based compositions 失效
标题翻译：在烷氧基硅烷或烷氧基硅烷类组合物中中和还原残留卤素含量的方法
公开(公告)号：US06177584B1
公开(公告)日：2001-01-23
申请号：US09427118
申请日：1999-10-26
申请人： Peter Loewenberg , Frank Kropfgans , Ralf Laven , Roland Edelmann , Albert-Johannes Frings , Michael Horn , Peter Jenkner , Helmut Mack , Jaroslaw Monkiewicz , Burkhard Standke
发明人： Peter Loewenberg , Frank Kropfgans , Ralf Laven , Roland Edelmann , Albert-Johannes Frings , Michael Horn , Peter Jenkner , Helmut Mack , Jaroslaw Monkiewicz , Burkhard Standke
IPC分类号： C07F708
CPC分类号： C07F7/20 , C07F7/1804
摘要： The present invention relates to a process for neutralizing and reducing the residual halogen content in alkoxysilanes and alkoxysilane-based compositions, which includes treating an alkoxysilane having a residual content of acidic halide, or a corresponding alkoxysilane-based composition, with metallic magnesium in the presence of an alcohol and separating off the resulting solids.
摘要翻译：本发明涉及中和和还原烷氧基硅烷和烷氧基硅烷类组合物中的残留卤素含量的方法，其包括在存在下用金属镁处理具有酸性卤化物残余量的烷氧基硅烷或相应的烷氧基硅烷基组合物的醇并分离出所得固体。

109. 发明授权

US6054601A Fluoroalkyl-functional organopolysiloxane-containing compositions based on water, a process for their preparation and their use 失效
标题翻译：基于水的含氟烷基官能的有机聚硅氧烷的组合物，其制备方法及其应用
公开(公告)号：US6054601A
公开(公告)日：2000-04-25
申请号：US93681
申请日：1998-06-09
申请人： Burkhard Standke , Roland Edelmann , Albert-Johannes Frings , Michael Horn , Peter Jenkner , Ralf Laven , Helmut Mack , Jaroslaw Monkiewicz
发明人： Burkhard Standke , Roland Edelmann , Albert-Johannes Frings , Michael Horn , Peter Jenkner , Ralf Laven , Helmut Mack , Jaroslaw Monkiewicz
IPC分类号： C08L83/08 , B27K3/15 , C03C17/30 , C04B41/49 , C04B41/64 , C04B41/84 , C08G77/24 , C08G77/26 , C09D183/08 , C09K3/18 , C23C30/00 , D06M15/643 , D06M15/657 , D21H17/59 , D21H21/16 , C07F7/08
CPC分类号： C04B41/009 , C03C17/30 , C04B41/4961 , C04B41/64 , C04B41/84 , C08G77/24 , C08G77/26 , C09D183/08 , C09K3/18 , C23C30/00 , D06M15/6436 , D06M15/657 , D21H17/59 , B05D1/18 , B05D2201/00 , B05D2202/00 , B05D2203/20 , B05D2203/22 , B05D2203/24 , B05D2203/30 , B05D2203/35 , B05D5/08 , B05D5/083 , C04B2111/1012 , C04B2111/203 , C04B2111/27 , C23C2222/20 , D06M2101/06 , D21H21/16 , Y10T428/24355 , Y10T428/24372 , Y10T428/2438 , Y10T428/24388 , Y10T428/24405 , Y10T428/24994 , Y10T428/249946 , Y10T428/249947 , Y10T428/249974 , Y10T428/8305
摘要： Organopolysiloxane containing compositions are prepared by mixing an organopolysiloxane containing an aminoalkyl group, an organopolysiloxane containing a fluoroalkyl group, and optionally, organopolysiloxanes containing alkyl groups, together with water, or a water/acid mixture, or a water/acid/alcohol mixture, where the mixture is adjusted to have a pH in the range of 1-8, then removing the alcohol already present or formed during reaction.
摘要翻译：含有机聚硅氧烷的组合物通过将含有氨基烷基的有机聚硅氧烷，含氟烷基的有机聚硅氧烷和任选的含有烷基的有机聚硅氧烷，水或水/酸混合物或水/酸/醇混合物混合而制备，其中将混合物调节至pH在1-8范围内，然后除去反应中已经存在或形成的醇。

110. 发明授权

US6020448A N-[.omega.-(methyl),.omega.-(silyl)] alkyl-N-organocarboxamides, oligomeric and polycondensed Si-containing compounds thereof, processes for their preparation, and their use 失效
标题翻译： N-（ω-（甲基），ω-（甲硅烷基）]烷基-N-有机碳酰胺，其低聚和缩聚的含Si化合物，其制备方法及其用途
公开(公告)号：US6020448A
公开(公告)日：2000-02-01
申请号：US98530
申请日：1998-06-17
申请人： Peter Jenkner , Albert Frings , Michael Horn , Jaroslaw Monkiewicz , Burkhard Standke
发明人： Peter Jenkner , Albert Frings , Michael Horn , Jaroslaw Monkiewicz , Burkhard Standke
IPC分类号： C07F7/18 , C08G77/26 , C09D183/08 , C09J183/08 , C08G77/04
CPC分类号： C08G77/26 , C07F7/1836
摘要： N-[.omega.-(methyl),.omega.-(silyl)]alkyl-N-organocarboxamides, oligomeric and polycondensed Si-containing compounds thereof, or mixtures of the corresponding monomeric, oligomeric and polycondensed Si-containing compounds. These materials are useful as, for example, adhesion promoters and for coating surfaces.
摘要翻译： N-（ω-（甲基），ω-（甲硅烷基）]烷基-N-有机碳酰胺，其低聚和缩聚的含Si化合物，或相应的单体，低聚和缩聚的含Si化合物的混合物。这些材料可用作例如粘合促进剂和涂层表面。

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