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101. 发明授权

US3998873A Process for preparing one or more alkyl-2-methyl pentenoates by means of hydrogenation of one or more alkyl-2-methyl-3,4-pentadienoates 失效
标题翻译：通过氢化一种或多种烷基-2-甲基-3,4-二苯甲酸酯制备一种或多种烷基-2-甲基苯甲酸酯的方法
公开(公告)号：US3998873A
公开(公告)日：1976-12-21
申请号：US569853
申请日：1975-04-21
申请人： John B. Hall , Denis E. Hruza
发明人： John B. Hall , Denis E. Hruza
IPC分类号： C07C17/16 , C11B9/00 , C07C69/54
CPC分类号： C11B9/0019 , C07C17/16
摘要： A process for producing one or more alkyl-2-methyl pentenoates having the generic structure: ##STR1## comprising the steps of: I. Contacting with hydrogen gas one or more alkyl-2-methyl-3,4-pentadienoates having the structure: ##STR2## in the presence of a hydrogenation catalyst which may be either of: A. Raney Nickel;B. Palladium on carbon; orC. Palladium on calcium carbonateAt a temperature from about 10.degree. C up to about 100.degree. C, a hydrogen pressure from about 5 psig up to about 80 psig, the concentration of said catalyst based on the weight of the starting material, the alkyl-2-methyl-3,4-pentadienoate, being from about 0.1% up to about 10%;Ii. Recovering at least 60% by weight of one or more alkyl-2-methyl-cis-3-pentenoates having the structure: ##STR3## wherein R is alkyl having up to 6 carbon atoms; optionally III. Separating the ingredients of the resulting chemical composition to obtain ethyl-2-methyl-cis-3-pentenoate; and/or, optionally,Iv. Forming one or more carboxylic acids by means of admixing the resulting chemical composition with a basic hydrolysis agent which may be either an aqueous solution of alkali metal hydroxide, or an alcohol solution of an alkali metal hydroxide; and, optionally,V. Re-esterifying the resulting carboxylic acid(s) by reacting said carboxylic acid(s) with an esterifying agent such as an alkanol in the presence of a protonic acid catalyst.The products produced are useful in altering the organoleptic characteristics (aroma and/or taste) of foodstuffs, foodstuff flavors, chewing gum, medicinal products, tobaccos, flavoring compositions for tobaccos, perfumes, perfume compositions and perfumed articles such as soaps, colognes, cosmetic powders and detergent powders and liquids.

102. 发明授权

US5042714A Collapsible grocery container 失效
标题翻译：可折叠杂货容器
公开(公告)号：US5042714A
公开(公告)日：1991-08-27
申请号：US394890
申请日：1989-08-17
申请人： John B. Hall
发明人： John B. Hall
IPC分类号： B65D5/36
CPC分类号： B65D5/3621
摘要： A collapsible, grocery bag container made of lightweight plastic or cardboard which can be used by consumers to store groceries in the back of the car. The container can be readily converted from its stored, space saving position to its in-use position without having to be set up or needing to be manipulated by the consumer.
摘要翻译：一种可折叠的，由轻质塑料或纸板制成的杂货袋容器，可由消费者用来将杂货存放在汽车后部。容器可以容易地从其储存的节省空间的位置转换到其使用中的位置，而不必被设置或需要被消费者操纵。

103. 发明授权

US4632831A Uses of methyl phenyl pentanol derivatives in augmenting or enhancing the aroma or taste of consumable materials 失效
公开(公告)号：US4632831A
公开(公告)日：1986-12-30
申请号：US784057
申请日：1985-10-04
申请人： John B. Hall
发明人： John B. Hall
IPC分类号： C07C33/20 , C07C45/62 , C07C45/74 , C11B9/00 , A23L1/235
CPC分类号： C11B9/0061 , C07C33/20 , C07C45/62 , C07C45/74
摘要： Described are 2-methyl-4-phenyl-1-pentanol derivatives defined according to the structure: ##STR1## wherein R represents hydrogen or acetyl and uses thereof in augmenting or enhancing the aroma or taste of consumable materials including perfume compositions, colognes, perfumed articles, foodstuffs, chewing gums, medicinal products and chewing tobaccos.

104. 发明授权

US4627935A 2-isopropenyl-5-methylcyclopentanealkanols, esters thereof and organoleptic uses of same 失效
标题翻译： 2-异丙烯基-5-甲基环戊烷链烷醇，其酯及其感官用途
公开(公告)号：US4627935A
公开(公告)日：1986-12-09
申请号：US698862
申请日：1985-02-06
申请人： John B. Hall
发明人： John B. Hall
IPC分类号： C11B9/00 , C11D3/50 , A61K7/46 , C07C35/06
CPC分类号： C11B9/003 , C11D3/50
摘要： Described are the 2-isopropenyl-5-methylcyclopentanealkanols and esters thereof having the generic structure: ##STR1## wherein R.sub.1 represents hydrogen or C.sub.2 -C.sub.3 acyl and wherein n represents 0 or 1 and uses thereof in augmenting or enhancing the aroma of consumable materials including perfume compositions, colognes and perfumed articles such as solid or liquid anionic, cationic, nonionic or zwitterionic detergents, perfumed polymers, cosmetic compositions, fabric softener compositions, fabric softener articles and hair preparations.
摘要翻译：描述了具有以下通用结构的2-异丙烯基-5-甲基环戊烷醇及其酯：其中R 1表示氢或C 2 -C 3酰基，其中n表示0或1，并且其用于增强或增强消耗材料的香气，包括香水组合物，古龙水和香料制品如固体或液体阴离子，阳离子，非离子或两性离子洗涤剂，加香聚合物，化妆品组合物，织物柔软剂组合物，织物柔软剂制品和毛发制品。

105. 发明授权

US4576740A Tertiary pentamethylindanol derivatives and organoleptic uses thereof 失效
标题翻译：叔五甲基茚醇衍生物及其感官用途
公开(公告)号：US4576740A
公开(公告)日：1986-03-18
申请号：US671329
申请日：1984-11-14
申请人： John B. Hall , Takao Yoshida
发明人： John B. Hall , Takao Yoshida
IPC分类号： A24B15/34 , C07C35/23 , C07C35/32 , C11B9/00 , C11D3/50 , A61K7/46
CPC分类号： C11D3/50 , A24B15/345 , C07C35/23 , C07C35/32 , C11B9/0049
摘要： Described are tertiary pentamethylindanol derivatives defined according to the structure: ##STR1## wherein the dashed line represents a carbon-carbon single bond or a carbon-carbon double bond and uses thereof in augmenting or enhancing the aroma or taste of consumable materials selected from the group consisting of perfume compositions, colognes, perfumed articles, foodstuffs, smoking tobaccos and smoking tobacco compositions.
摘要翻译：描述了根据以下结构定义的叔五甲基茚醇衍生物：其中虚线表示碳 - 碳单键或碳 - 碳双键，并且其用于增强或增强选自组中的可消耗材料的香气或味道由香水组合物，古龙水，香料制品，食品，烟草烟草和烟草组合物组成。

106. 发明授权

US4576186A Use of pentamethylindanol derivatives in augmenting or enhancing the aroma or taste of smoking tobacco compositions or smoking tobacco articles 失效
标题翻译：五甲基茚满醇衍生物在增加或增强吸烟烟草组合物或烟草制品的香味或味道方面的应用
公开(公告)号：US4576186A
公开(公告)日：1986-03-18
申请号：US671331
申请日：1984-11-14
申请人： John B. Hall , Takao Yoshida
发明人： John B. Hall , Takao Yoshida
IPC分类号： A24B15/34 , C07C35/23 , C07C35/32 , C11B9/00 , C11D3/50 , A24B15/30
CPC分类号： C11D3/50 , A24B15/345 , C07C35/23 , C07C35/32 , C11B9/0049
摘要： Described are tertiary pentamethylindanol derivatives defined according to the structure: ##STR1## wherein the dashed line represents a carbon-carbon single or a carbon-carbon double bond and uses thereof in augmenting or enhancing the aroma or taste of smoking tobaccos or smoking tobacco compositions.
摘要翻译：描述了根据以下结构定义的叔五甲基茚醇衍生物：其中虚线表示碳 - 碳单碳或碳 - 碳双键，并且其用于增强或增强吸烟烟草或烟草烟草组合物的香味或味道。

107. 发明授权

US4560499A Isosolanone and solanone intermediates and organoleptic uses 失效
标题翻译： Isosolanone和solanone中间体和感官用途
公开(公告)号：US4560499A
公开(公告)日：1985-12-24
申请号：US609349
申请日：1984-06-22
申请人： John B. Hall , James M. Sanders , James N. Siano
发明人： John B. Hall , James M. Sanders , James N. Siano
IPC分类号： A24B15/32 , C07C29/40 , C07C33/02 , C07C45/54 , C07C45/67 , C07C45/75 , C07C49/203 , C11D3/50 , C11B9/00
CPC分类号： C11D3/50 , A24B15/32 , C07C29/40 , C07C33/02 , C07C45/54 , C07C45/67 , C07C45/75 , C07C49/203 , C07C67/03
摘要： Described is a novel genus of compounds defined according to the structure: ##STR1## wherein Z represents hydrogen, MgX and the moiety having the structure: ##STR2## and X represents chloro, bromo or iodo; as well as the novel compounds defined according to the structures: ##STR3## and mixtures of same shown according to the structure: ##STR4## wherein the wavy lines indicate both cis and trans juxtaposition of the hydrogen and methallyl moieties about the carbon-carbon double bond; uses of same as intermediates in a process for producing isosolanone which is a mixture of compounds having the structures: ##STR5## or shown by the single structure: ##STR6## and solanone which is a mixture of compounds having the structures: ##STR7## or shown by the structure: ##STR8## wherein the wavy lines are indicative of a cis or trans juxtaposition of the hydrogen or 2-propenyl moieties about the double bond; and organoleptic uses of the compounds having the structures: ##STR9##
摘要翻译：描述了根据以下结构定义的化合物的新颖属性：其中Z表示氢，MgX和具有以下结构的部分：其中X表示氯，溴或碘; 以及根据以下结构定义的新颖化合物：根据以下结构显示的相同的结构：其中波浪线表示氢和甲代烯丙基部分在碳 - 碳双键上的顺式和反式并置键; 在作为制备具有以下结构的化合物的混合物的方法中使用与中间体的相同的化合物：具有以下结构的化合物：或者由单一结构显示：作为化合物的混合物，其具有以下结构：或由以下结构示出：其中波浪线表示在双键上的氢或2-丙烯基部分的顺式或反式并置; 和具有以下结构的化合物的感官用途：

108. 发明授权

US4449007A Process for preparing 1(4-pentonoyl)-3,3-dimethylcyclohexane and intermediates used in a said process 失效
标题翻译：制备1（4-戊烯酰基）-3,3-二甲基环己烷的方法和用于所述方法的中间体
公开(公告)号：US4449007A
公开(公告)日：1984-05-15
申请号：US441221
申请日：1982-11-12
申请人： John B. Hall , Mark A. Sprecker
发明人： John B. Hall , Mark A. Sprecker
IPC分类号： C07C45/45 , C07C49/175 , C07C49/185 , C07C49/255 , C07C49/258 , C07C49/303 , C07C49/355 , C07C49/557 , C07C49/583 , C07C51/02 , C07C59/80 , C07C69/716 , C07C403/00 , C11B9/00 , C07C45/67
CPC分类号： C11B9/0034 , C07C403/16 , C07C45/455 , C07C49/303 , C07C49/355 , C07C49/557 , C07C49/583 , C07C51/02 , C07C59/80 , C07C2101/14
摘要： A process comprising the steps of reacting 1-acetyl-3,3-dimethylcyclohexane with an alkyl acetate, thereby forming a diketone having the structure: ##STR1## reacting the said diketone with an allyl halide to form a substituted diketone having the structure: ##STR2## which is transformed into the compound having the structure: ##STR3## by means of a retro-Claisen reaction. Also described is the use in augmenting or enhancing the aroma of perfume compositions, colognes or perfumed articles of the compound having the structure: ##STR4##
摘要翻译：一种方法包括以下步骤：使1-乙酰基-3,3-二甲基环己烷与乙酸烷基酯反应，从而形成具有以下结构的二酮：将所述二酮与烯丙基卤反应形成具有以下结构的取代二酮： IMAGE“，其通过复古克莱森反应转化为具有以下结构的化合物：。还描述了用于增强或增强具有以下结构的化合物的香料组合物，古龙水或香料制品的香味：

109. 发明授权

US4275251A Substituted tricyclodecane derivatives, processes for producing same and organoleptic uses thereof 失效
标题翻译：取代的三环癸烷衍生物，其制备方法和感官用途
公开(公告)号：US4275251A
公开(公告)日：1981-06-23
申请号：US144898
申请日：1980-04-29
申请人： Mark A. Sprecker , John B. Hall
发明人： Mark A. Sprecker , John B. Hall
IPC分类号： C07C69/03 , A23L27/20 , A24B3/12 , A24B15/34 , A61K8/34 , A61K8/35 , A61K8/37 , A61Q13/00 , C07C27/00 , C07C29/09 , C07C29/10 , C07C29/17 , C07C29/70 , C07C35/37 , C07C35/46 , C07C41/00 , C07C41/06 , C07C43/188 , C07C45/00 , C07C45/29 , C07C49/643 , C07C67/00 , C07C67/04 , C11B9/00 , C07C35/22
CPC分类号： C07C29/172 , A24B15/345 , C07C29/095 , C07C29/17 , C07C29/70 , C07C35/37 , C07C35/46 , C07C45/29 , C07C49/643 , C11B9/0042 , C07C2103/68
摘要： Described are substituted tricyclodecane derivatives having the generic structure: ##STR1## wherein Y is a moiety having a structure selected from the group consisting of: ##STR2## wherein one of the dashed lines represents a carbon-carbon single bond and the other of the dashed lines represents a carbon-carbon double bond; wherein R.sub.1 and R.sub.2 represent hydrogen or methyl with the proviso that one of R.sub.1 and R.sub.2 is hydrogen and the other of R.sub.1 and R.sub.2 is methyl; wherein R.sub.3 is hydrogen, C.sub.1 -C.sub.3 acyl, C.sub.3 or C.sub.4 alkyl or C.sub.3 or C.sub.4 alkenyl; wherein R.sub.4, R.sub.5 and R.sub.6 represent hydrogen or methyl with the additional proviso that one of R.sub.4, R.sub.5 and R.sub.6 is methyl and the other two of R.sub.4, R.sub.5 and R.sub.6 is hydrogen. Also described are processes for preparing such substituted tricyclodecane derivatives and processes for using the above defined substituted tricyclodecane derivatives for their organoleptic properties and compositions containing said substituted tricyclodecane derivatives including perfumes, perfumed articles, such as solid or liquid anionic, cationic, nonionic and zwitterionic detergents, fabric softeners and cosmetic powders; foodstuffs, chewing gums, toothpastes, medicinal products and chewing tobaccos; smoking tobacco compositions and smoking tobacco flavoring compositions and smoking tobacco articles containing such smoking tobacco compositions.
摘要翻译：描述了具有以下通用结构的取代的三环癸烷衍生物：其中Y是具有选自以下的结构的部分：其中一条虚线表示碳 - 碳单键，另一条为虚线线代表碳 - 碳双键; 其中R1和R2表示氢或甲基，条件是R1和R2之一是氢，R1和R2中的另一个是甲基; 其中R3是氢，C1-C3酰基，C3或C4烷基或C3或C4链烯基; 其中R4，R5和R6代表氢或甲基，另外条件是R4，R5和R6之一是甲基，R4，R5和R6中的另外两个是氢。还描述了制备这种取代的三环癸烷衍生物的方法和使用上述定义的取代的三环癸烷衍生物的感官特性的方法和含有所述取代的三环癸烷衍生物的组合物，包括香料，加香制品如固体或液体阴离子，阳离子，非离子和两性离子洗涤剂，织物柔软剂和化妆粉; 食品，口香糖，牙膏，药用产品和咀嚼烟草; 吸烟烟草组合物和吸烟烟草调味组合物和含有烟草烟草组合物的烟草制品。

110. 发明授权

US4234518A Ketones and organoleptic uses thereof 失效
标题翻译：酮和感官用途
公开(公告)号：US4234518A
公开(公告)日：1980-11-18
申请号：US46390
申请日：1979-06-07
申请人： Takao Yoshida , John B. Hall
发明人： Takao Yoshida , John B. Hall
IPC分类号： C07C45/74 , C07C49/20 , C11B9/00 , C07C45/00
CPC分类号： C11B9/0034 , C07C403/16 , C07C45/74 , C07C2101/16
摘要： Described is a process for the production of alpha, beta unsaturated ketones by reaction of an aldehyde with a ketone in the presence of a catalyst consisting essentially of either zinc acetate or zinc acetate dihydrate. The ketones obtained are suitable and some cases as solvents and in some cases as intermediates for the production of valuable odorants, dyes, plastics and especially nature-identical substances and are also useful as odorants per se.
摘要翻译：描述的是通过在主要由乙酸锌或乙酸锌二水合物组成的催化剂的存在下，通过醛与酮的反应制备α，β不饱和酮的方法。获得的酮是合适的，有些情况是溶剂，在某些情况下作为生产有价值气味剂，染料，塑料，特别是自然相同物质的中间体，也可用作气味剂本身。

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