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91. 发明授权

US4518752A Process for polyolefins production 失效
标题翻译：聚烯烃生产工艺
公开(公告)号：US4518752A
公开(公告)日：1985-05-21
申请号：US551516
申请日：1983-11-15
申请人： Nobuyuki Kuroda , Toru Nakamura , Yutaka Shikatani , Kazuo Matsuura
发明人： Nobuyuki Kuroda , Toru Nakamura , Yutaka Shikatani , Kazuo Matsuura
IPC分类号： C08F4/00 , C08F4/10 , C08F4/14 , C08F4/16 , C08F4/60 , C08F4/62 , C08F10/00 , C08F4/02
CPC分类号： C08F10/00 , Y10S526/901 , Y10S526/906
摘要： A process for the homopolymerization or copolymerization of olefins is disclosed, which is carried out in the presence of an improved catalyst comprising a solid catalyst component and an organometal compound, said solid catalyst component being obtained by the reaction of: (a) a magnesium halide, (b) a compound represented by the formula: Me(OR).sub.n X.sub.z-n where Me is any of the Group I-VIII elements of the Periodic Table, excluding Al, Si, Ti and V, R is a hydrocarbon residual group having 1-24 carbon atoms, X is a halogen atom, z represents the valence of Me and n is 0
摘要翻译：公开了一种烯烃均聚或共聚合的方法，该方法在包含固体催化剂组分和有机金属化合物的改进催化剂存在下进行，所述固体催化剂组分通过以下反应获得：（a）卤化镁，（b）由Me（OR）n X z-n表示的化合物，其中Me是元素周期表中的I-VIII族元素中的任何一种，不包括Al，Si，Ti和V，R是具有 1-24个碳原子，X是卤素原子，z代表Me的价数，n是0

92. 发明授权

US4427771A Assay method for amylase activity and method of producing maltose dehydrogenase for use therein 失效
标题翻译：淀粉酶活性的测定方法和生产用于其中的麦芽糖脱氢酶的方法
公开(公告)号：US4427771A
公开(公告)日：1984-01-24
申请号：US311263
申请日：1981-10-14
申请人： Hideo Misaki , Eiji Muramatsu , Hidehiko Ishikawa , Kazuo Matsuura
发明人： Hideo Misaki , Eiji Muramatsu , Hidehiko Ishikawa , Kazuo Matsuura
IPC分类号： C12N9/04 , C12Q1/40 , C12N1/20 , C12Q1/32 , C12R1/11
CPC分类号： C12N9/0006 , C12Q1/40 , G01N2400/18 , Y10S435/837
摘要： An assay method for amylase activity in a biological specimen such as serum, saliva or urine. The enzyme amylase in the specimen is used to decompose a substrate which is a glucose polymer having a modified reducing terminal glucose residue or a cyclic glucose polymer. A component of the decomposed substrate is measured as an indication of amylase activity in the specimen. The residue may be amylose, amylopectin, starch, starch hydrolyzate, an etherified reducing terminal, an esterified reducing terminal, gluconolactone or a gluconic acid residue or its derivative. Decomposed substrate assay may be effected by contacting the same with maltose dehydrogenase and NAD or NADP, whereupon the assay is performed by measuring the amount of reduced NAD or reduced NADP, by reacting the same with reduced-form hydrogen transport colorimetric reaction reagent. This reagent may be a tetrazolium salt and diaphorase, or tetrazolium salt and phenazinemethosulfate. To remove pre-existing glucose and maltose present in the specimen, the specimen may be pretreated with alpha-glucosidase or kinase in the presence of Mg.sup.++ and ATP, the kinase being for example hexokinase. The preferred maltose dehydrogenase is produced by culturing Bacillus megaterium B-0779 FERM-P No. 5662.
摘要翻译：生物样品如血清，唾液或尿液中淀粉酶活性的测定方法。试样中的酶淀粉酶用于分解具有修饰的还原性末端葡萄糖残基或环状葡萄糖聚合物的葡萄糖聚合物的底物。测量分解的底物的组分作为样品中淀粉酶活性的指示。残基可以是直链淀粉，支链淀粉，淀粉，淀粉水解物，醚化还原末端，酯化还原末端，葡萄糖酸内酯或葡萄糖酸残基或其衍生物。分解的底物测定可以通过使其与麦芽糖脱氢酶和NAD或NADP接触来实现，因此通过使其与还原形式的氢转运比色反应试剂反应来测量还原的NAD或还原的NADP的量来进行测定。该试剂可以是四唑盐和心律黄素，或四唑鎓盐和吩嗪甲硫酸盐。为了除去样品中存在的现有葡萄糖和麦芽糖，可以在Mg ++和ATP存在下用α-葡糖苷酶或激酶预处理样品，所述激酶例如己糖激酶。优选的麦芽糖脱氢酶是通过培养巨大芽孢杆菌B-0779 FERM-P No.5662产生的。

93. 发明授权

US4384088A Process for preparing polyolefins 失效
标题翻译：聚烯烃的制备方法
公开(公告)号：US4384088A
公开(公告)日：1983-05-17
申请号：US913507
申请日：1978-06-07
申请人： Mitsuo Matsuno , Etsuo Kawamata , Nobuyuki Kuroda , Kazuo Matsuura , Mitsuji Miyoshi
发明人： Mitsuo Matsuno , Etsuo Kawamata , Nobuyuki Kuroda , Kazuo Matsuura , Mitsuji Miyoshi
IPC分类号： C08F4/62 , C08F4/64 , C08F10/00 , C08F4/02 , C08F10/02
CPC分类号： C08F10/00 , Y10S526/906
摘要： According to this invention, there is provided a process for preparing polyolefins wherein olefins are polymerized or copolymerized using as catalyst a solid component and an organometallic compound, characterized in that said solid component is a substance obtained by the copulverization of:(1) a reaction product resulting from a heat reaction of magnesium oxide and aluminum trichloride,(2) a titanium compound and/or a vanadium compound, and(3) if desired, an organic halide.
摘要翻译：根据本发明，提供了一种制备聚烯烃的方法，其中使用固体组分和有机金属化合物作为催化剂将烯烃聚合或共聚，其特征在于所述固体组分是通过共沉淀获得的物质：（1）反应由氧化镁和三氯化铝的热反应产生的产物，（2）钛化合物和/或钒化合物，和（3）如果需要，有机卤化物。

94. 发明授权

US4346173A Process for the production of acyl-Coenzyme A oxidase 失效
标题翻译：制备酰基辅酶A氧化酶的方法
公开(公告)号：US4346173A
公开(公告)日：1982-08-24
申请号：US201123
申请日：1980-10-27
申请人： Shigeru Ikuta , Shigeyuki Imamura , Hidehiko Ishikawa , Kazuo Matsuura , Masaki Takada , Hideo Misaki
发明人： Shigeru Ikuta , Shigeyuki Imamura , Hidehiko Ishikawa , Kazuo Matsuura , Masaki Takada , Hideo Misaki
IPC分类号： C12N9/02
CPC分类号： C12Y103/03006 , C12N9/001 , C12R1/06 , C12R1/645 , C12R1/66 , C12R1/865 , Y10S435/83 , Y10S435/911 , Y10S435/913 , Y10S435/942
摘要： A process for the production of acyl-Coenzyme A oxidase, comprises culturing an acyl-Coenzyme A-oxidase-producing microorganism belonging to genus Macrophomina, genus Cladosporium, genus Aspergillus, genus Monascus, genus Saccharomyces or genus Arthrobacter in a nutrient medium, and isolating the thus-formed acyl-CoA oxidase therefrom. The preferred species of microorganism are Macrophomina phaseoli ATCC 14383, Cladosporium resinae IFO 6367, Aspergillus candidus M-4815 FERM-P No. 5226, Monascus sp. M-4800 FERM-P No. 5225, Saccharomyces cerevisiae Y 0036 FERM-P No. 5174, and Arthrobacter sp. B-720 FERM-P No. 5224, respectively.
摘要翻译：一种制备酰基辅酶A氧化酶的方法，包括在营养培养基中培养属于巨噬细胞，枝孢霉属，曲霉属，红曲霉属，酿酒酵母属或节杆菌属的酰基辅酶A氧化酶微生物，由此形成的酰基辅酶A氧化酶。微生物的优选种类是Macrophomina phaseoli ATCC 14383，Cladosporium resinae IFO 6367，Aspergillus candidus M-4815 FERM-P No.5226，Monascus sp。 M-4800 FERM-P No.5225，酿酒酵母Y 0036 FERM-P No.5174和节杆菌属（Arthrobacter sp。 B-720 FERM-P No. 5224。

95. 发明授权

US4324876A Process for the production of polyolefins 失效
标题翻译：生产聚烯烃的方法
公开(公告)号：US4324876A
公开(公告)日：1982-04-13
申请号：US209318
申请日：1980-11-24
申请人： Kazuo Matsuura , Takeichi Shiraishi , Etsuo Kawamata , Nobuyuki Kuroda , Mitsuji Miyoshi
发明人： Kazuo Matsuura , Takeichi Shiraishi , Etsuo Kawamata , Nobuyuki Kuroda , Mitsuji Miyoshi
IPC分类号： C08F4/00 , C08F4/50 , C08F4/60 , C08F4/64 , C08F10/00 , C08F4/02
CPC分类号： C08F10/00
摘要： A process for the homopolymerization or copolymerization of olefins is disclosed. The process is carried out in the presence of a catalyst system comprising the combination of an organometallic compound with a component resulting from the mutual contact of (i) an inorganic magnesium compound of a spherical shape having an average particle size of from 1 to 100 microns; (ii) a compound represented by the formula AlX.sub.3.OR'R" (where X represents a halogen atom, and R' and R" represent a hydrocarbon residual group having 1 to 20 carbon atoms; and (iii) a titanium compound represented by the formula Ti(OR).sub.4 (where R represents a hydrocarbon residual group having 1 to 20 carbon atoms). The resulting polymers are provided with a spherical particle shape.
摘要翻译：公开了一种烯烃均聚或共聚合的方法。该方法在催化剂体系的存在下进行，所述催化剂体系包含有机金属化合物与由（i）平均粒度为1至100微米的球形的无机镁化合物的相互接触所形成的组分的组合 ; （ii）由式AlX3.OR'R“表示的化合物（其中X表示卤素原子，R'和R”表示碳原子数为1〜20的烃残基;（iii）钛化合物由式Ti（OR）4（其中R表示具有1至20个碳原子的烃残基）表示，所得聚合物具有球形颗粒形状。

96. 发明授权

US4315999A Process for preparing polyolefins 失效
标题翻译：聚烯烃的制备方法
公开(公告)号：US4315999A
公开(公告)日：1982-02-16
申请号：US189823
申请日：1980-09-23
申请人： Kazuo Matsuura , Takeichi Shiraishi , Etsuo Kawamata , Nobuyuki Kuroda , Mituji Miyoshi
发明人： Kazuo Matsuura , Takeichi Shiraishi , Etsuo Kawamata , Nobuyuki Kuroda , Mituji Miyoshi
IPC分类号： C08F4/02 , C08F4/65 , C08F4/76 , C08F10/00
CPC分类号： C08F10/00 , C08F4/022 , C08F2410/04 , Y10S526/906
摘要： An olefin is polymerized using a catalyst obtained by contacting (1) at least one of silicon or aluminum dioxide, (2) a compound of the formula ROH wherein R is a hydrocarbon radical having 1 to 20 carbon atoms, and (3) a substance obtained by supporting a titanium or a vanadium compound on a magnesium or manganese halide.
摘要翻译：使用通过使（1）硅或二氧化铝中的至少一种与（2）式ROH的化合物（其中R是具有1至20个碳原子的烃基）的化合物和（3）物质通过在镁或锰卤化物上负载钛或钒化合物获得。

97. 发明授权

US4288579A Process for preparing polyolefins 失效
标题翻译：聚烯烃的制备方法
公开(公告)号：US4288579A
公开(公告)日：1981-09-08
申请号：US102646
申请日：1979-12-12
申请人： Mitsuji Miyoshi , Yoshio Tajima , Kazuo Matsuura , Nobuyuki Kuroda , Mitsuo Matsuno
发明人： Mitsuji Miyoshi , Yoshio Tajima , Kazuo Matsuura , Nobuyuki Kuroda , Mitsuo Matsuno
IPC分类号： C08F4/00 , C08F4/60 , C08F4/64 , C08F10/00 , C08F4/02 , C08F10/06
CPC分类号： C08F10/00 , Y10S526/906
摘要： According to this invention there is provided a process for polymerizing or copolymerizing olefins using a catalyst consisting of:[A]a solid component obtained by contacting(1) a reaction product resulting from heat reaction of a magnesium oxide and an aluminum trihalide with(2) a titanium halide and/or an addition product of a titanium halide and an aromatic carboxylic acid ester, and[B]an organometallic compound and/or an addition product of an organometallic compound and an aromatic carboxylic acid ester,or alternatively, using a catalyst consisting of acid components [A] and [B] plus [C] an aromatic carboxylic acid ester.
摘要翻译：根据本发明，提供了一种使用由以下组成的催化剂聚合或共聚烯烃的方法：[A]通过使（1）由氧化镁和三卤化铝的热反应得到的反应产物与（2））卤化钛和/或卤化钛和芳族羧酸酯的加成产物，和[B]有机金属化合物和/或有机金属化合物和芳族羧酸酯的加成产物，或者使用由酸组分[A]和[B] + [C]芳族羧酸酯组成的催化剂。

98. 发明授权

US4275161A Process for the manufacture of L-.alpha.-glycerophosphate oxidase 失效
标题翻译：制备L-α-甘油磷酸氧化酶的方法
公开(公告)号：US4275161A
公开(公告)日：1981-06-23
申请号：US59583
申请日：1979-07-20
申请人： Hideo Misaki , Yoshifumi Horiuchi , Kazuo Matsuura , Saburo Harada
发明人： Hideo Misaki , Yoshifumi Horiuchi , Kazuo Matsuura , Saburo Harada
IPC分类号： C12N9/04 , C12Q1/26 , C12Q1/32 , C12R1/01
CPC分类号： C12N9/0006 , C12Q1/26 , C12Q1/32 , Y10S435/822
摘要： L-.alpha.-glycerophosphate oxidase can be produced by culturing Aerococcus viridans IFO-12219 or Aerococcus viridans IFO-12317. It is useful for analysis for L-.alpha.-glycerophosphate, because it catalyzes the reaction of L-.alpha.-glycerophosphate and oxygen to form dihydroxyacetone phosphate and hydrogen peroxide.
摘要翻译： L-阿糖甘油磷酸氧化酶可以通过培养绿脓杆菌IFO-12219或野生型球菌IFO-12317来产生。它可用于分析L-α-甘油磷酸酯，因为它催化L-α-甘油磷酸酯和氧气反应形成磷酸二羟基丙酮和过氧化氢。

99. 发明授权

US4093789A Process for preparing polyolefins 失效
标题翻译：聚烯烃的制备方法
公开(公告)号：US4093789A
公开(公告)日：1978-06-06
申请号：US705607
申请日：1976-07-15
申请人： Nobuyuki Kuroda , Toru Nakamura , Takeichi Shiraishi , Kazuo Matsuura , Mituji Miyoshi
发明人： Nobuyuki Kuroda , Toru Nakamura , Takeichi Shiraishi , Kazuo Matsuura , Mituji Miyoshi
IPC分类号： C08F4/00 , C08F4/02 , C08F4/60 , C08F4/64 , C08F10/00 , C08F10/02
CPC分类号： C08F10/00 , C08F4/022 , Y10S526/903 , Y10S526/906
摘要： According to the present invention, there is provided a process for preparing polyolefins by polymerizing or copolymerizing olefins in the presence of a catalyst consisting of a solid component and an organometallic compound component, characterized in that said solid component is obtained by copulverizing(1) a magnesium halide and/or a manganese halide,(2) an aromatic hydrocarbon,(3) a tetravalent titanium compound, and(4) a trivalent titanium compoundAnd in that said organometallic compound component is a mixture of(5) a trialkylaluminum and(6) a compound represented by the general formula AlR.sub.n X.sub.3-n wherein R is alkyl having 1 to 10 carbon atoms and may be the same or different, X is halogen and O
摘要翻译：根据本发明，提供一种通过在由固体成分和有机金属化合物成分组成的催化剂存在下聚合或共聚烯烃制备聚烯烃的方法，其特征在于所述固体组分通过共混（1）A （2）芳族碳氢化合物，（3）四价钛化合物，和（4）多价钛化合物，以及所述有机元素化合物组分是（5）三烯丙基铝和（ 6）由通式AlRnX 3-n表示的化合物，其中R是具有1至10个碳原子的烷基并且可以相同或不同，X是卤素且O

100. 发明授权

US4083802A Polymerization of olefins and catalysts therefor 失效
标题翻译：烯烃和其催化剂的聚合
公开(公告)号：US4083802A
公开(公告)日：1978-04-11
申请号：US706589
申请日：1976-07-19
申请人： Kazuo Matsuura , Nobuyuki Kuroda , Takeichi Shiraishi , Mitsuji Miyoshi
发明人： Kazuo Matsuura , Nobuyuki Kuroda , Takeichi Shiraishi , Mitsuji Miyoshi
IPC分类号： C08F4/02 , C08F10/00 , C08F4/64
CPC分类号： C08F4/022 , C08F10/00
摘要： A process for the production of polyolefins is disclosed, which is carried out in the presence of catalysts prepared according to the invention. The catalysts comprise a carrier resulting from the reaction of anhydrous magnesium halide, silicon tetrachloride and a compound represented by the general formulaROHwhere R is a hydrocarbon group of 1 to 20 carbon atoms, and a transition metal compound supported on said carrier. Such catalysts are activated by an organometal compound of a metal of the Groups I to IV of the Periodic Table when in use.
摘要翻译：公开了一种生产聚烯烃的方法，其在根据本发明制备的催化剂的存在下进行。催化剂包含由无水卤化镁，四氯化硅和通式ROH表示的化合物（其中R是1至20个碳原子的烃基）和负载在所述载体上的过渡金属化合物反应而产生的载体。这种催化剂在使用时由元素周期表第I至IV族金属的有机金属化合物活化。

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