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1. 发明授权

US06180175B2 Coating composition 失效
标题翻译：涂料组成
公开(公告)号：US06180175B2
公开(公告)日：2001-01-30
申请号：US09177082
申请日：1998-10-23
申请人： Masaaki Saika , Yoshiyuki Yukawa , Motoshi Yabuta , Seiji Wada , Kohsuke Noura , Yasumasa Okumura
发明人： Masaaki Saika , Yoshiyuki Yukawa , Motoshi Yabuta , Seiji Wada , Kohsuke Noura , Yasumasa Okumura
IPC分类号： B05D302
CPC分类号： B05D7/532 , C08G18/4063 , C08G18/6295 , C08G18/73 , C08G18/771 , C09D175/04
摘要： There is disclosed a novel organic solvent type coating composition capable of making the solid content concentration at the time of coating to higher than 70% by weight, without lowering the properties, which urethane type coating materials have, such as acid resistance, scratch resistance, finishing appearance etc. The composition comprises (A) a vinyl type polymer having both hydroxyl groups and alkoxysilyl groups in the molecule and having a number-average molecular weight in a range of 2,000 to 10,000; (B) a polyol compound having a number-average molecular weight of less than 1,000 and having a hydroxyl value in a range of 120 to 1,000 mgKOH/g; (C) a polyisocyanate compound having a number-average molecular weight of less than 2,000; and (D) a silanol group forming catalyst.
摘要翻译：公开了一种新型的有机溶剂型涂料组合物，其能够使涂布时的固体成分浓度高于70重量％，而不降低聚氨酯类涂料具有的耐酸性，耐刮擦性，整理外观等。该组合物包含（A）分子中具有羟基和烷氧基甲硅烷基的乙烯基类聚合物，数均分子量在2,000〜10,000的范围内; （B）数均分子量小于1000且羟基值在120〜1000mgKOH / g范围内的多元醇化合物; （C）数均分子量小于2,000的多异氰酸酯化合物; 和（D）形成硅烷醇基团的催化剂。

2. 发明授权

US6045870A High solid coating composition and method for forming topcoat using same 失效
标题翻译：高固体涂料组合物和使用其形成面漆的方法
公开(公告)号：US6045870A
公开(公告)日：2000-04-04
申请号：US145427
申请日：1998-09-01
申请人： Kohsuke Noura , Yoshiyuki Yukawa , Masaaki Saika , Motoshi Yabuta , Yasumasa Okumura
发明人： Kohsuke Noura , Yoshiyuki Yukawa , Masaaki Saika , Motoshi Yabuta , Yasumasa Okumura
IPC分类号： C09D143/04 , C09D201/08 , B05D3/02
CPC分类号： C09D201/08 , C09D143/04 , C08L2205/18
摘要： An organic solvent-based heat-curable high solid coating composition comprising:(A) a carboxyl-containing compound having an acid value of 50 to 500 mg KOH/g wherein 20 mol % or more of the carboxyl groups are silylated carboxyl groups,(B) at least one epoxide selected from (B-1) an epoxy-, hydroxyl- and hydrolyzable alkoxysilyl-containing vinyl polymer, (B-2) the vinyl polymer (B-1) wherein 20 mol % or more of the hydroxyl groups are silylated hydroxyl groups, and (B-3) an epoxy compound having a number average molecular weight less than 1,000, and(C) a crosslinked particulate polymer,the composition having a solid content of 65 wt. % or more; and a method for forming a topcoat using the composition. The composition of the invention has a sufficiently high solid content, is capable of forming a coating film with high resistance to acids and the like, and is excellent in low-temperature curability, storage stability and recoat adhesion.
摘要翻译：一种有机溶剂型可热固化高固体涂料组合物，其包含：（A）酸值为50〜500mgKOH / g的含羧基化合物，其中20摩尔％以上的羧基为甲硅烷基化羧基（ B）至少一种选自（B-1）环氧基，羟基和可水解的含烷氧基甲硅烷基的乙烯基聚合物的环氧化物，（B-2）乙烯基聚合物（B-1），其中20mol％或更多的羟基是（甲基）丙烯酸羟基，和（B-3）数均分子量小于1000的环氧化合物，和（C）交联的颗粒聚合物，该组合物的固含量为65重量％％或者更多; 以及使用该组合物形成面漆的方法。本发明的组合物具有足够高的固体含量，能够形成具有高耐酸性等的涂膜，并且具有优异的低温固化性，储存稳定性和重涂性。

3. 发明授权

US06319557B1 Coating composition and method for application thereof 失效
标题翻译：涂料组合物及其应用方法
公开(公告)号：US06319557B1
公开(公告)日：2001-11-20
申请号：US09437145
申请日：1999-11-10
申请人： Satoshi Ikushima , Seiji Wada , Yasumasa Okumura , Haruhiko Aida , Motoshi Yabuta , Yoshiyuki Yukawa , Ken-ichi Hasada
发明人： Satoshi Ikushima , Seiji Wada , Yasumasa Okumura , Haruhiko Aida , Motoshi Yabuta , Yoshiyuki Yukawa , Ken-ichi Hasada
IPC分类号： B05D302
CPC分类号： C08L63/00 , C08G59/24 , C08L27/12 , C08L33/068 , C08L33/16 , C09D133/068 , C09D163/00 , Y10T428/31692 , Y10T428/31699 , C08L2666/04 , C08L2666/06 , C08L2666/14 , C08L2666/54
摘要： The present invention provides a thermosetting organic solvent type coating capable of forming a cured coating film having a TUKON hardness at 20° C. of 15 or more and the minimum value of dynamic modulus E′ at a frequency of 110 Hz in the temperature range of 150-200° C., of 1×109 dyn/cm or more. The cured film formed from the coating, as compared with the cured films formed from conventional organic solvent type coatings used as a top coat for automobile (e.g. an organic solvent type coating containing, as main components, a hydroxyl group-containing acrylic resin and a melamine resin, or a carboxylic-epoxy type coating), is at least equivalent in weatherabiIity, finish appearance, acid resistance, etc. and superior in stain resistance.
摘要翻译：本发明提供一种热固性有机溶剂型涂料，其能够在20℃下形成具有15℃以上的TUKON硬度的固化涂膜，在110Hz的温度范围内形成频率为110Hz的动态模量E'的最小值 150-200℃，1×10 9 dyn / cm以上。与由用作汽车面漆的常规有机溶剂型涂料形成的固化膜（例如含有含羟基的丙烯酸树脂的主要成分的有机溶剂型涂料）相比，由涂层形成的固化膜三聚氰胺树脂或羧基环氧型涂料）在耐候性，外观，耐酸性等方面至少相当，耐污染性优异。

4. 发明授权

US06262147B1 Coating composition and method for application thereof 失效
标题翻译：涂料组合物及其应用方法
公开(公告)号：US06262147B1
公开(公告)日：2001-07-17
申请号：US09384299
申请日：1999-08-26
申请人： Satoshi Ikushima , Seiji Wada , Yasumasa Okumura , Haruhiko Aida , Motoshi Yabuta , Yoshiyuki Yukawa , Ken-ichi Hasada
发明人： Satoshi Ikushima , Seiji Wada , Yasumasa Okumura , Haruhiko Aida , Motoshi Yabuta , Yoshiyuki Yukawa , Ken-ichi Hasada
IPC分类号： C08L6300
CPC分类号： C08L63/00 , C08G59/24 , C08L27/12 , C08L33/068 , C08L33/16 , C09D133/068 , C09D163/00 , Y10S525/922 , C08L2666/04 , C08L2666/06 , C08L2666/14 , C08L2666/54
摘要： The present invention provides a thermosetting organic solvent type coating capable of forming a cured coating film having a TUKON hardness at 20° C. of 15 or more and the minimum value of dynamic modulus E′ at a frequency of 110 Hz in the temperature range of 150-200° C., of 1×109 dyn/cm2 or more. The cured film formed from the coating, as compared with the cured films formed from conventional organic solvent type coatings used as a top coat for automobile (e.g. an organic solvent type coating containing, as main components, a hydroxyl group-containing acrylic resin and a melamine resin, or a carboxylic-epoxy type coating), is at least equivalent in weatherability, finish appearance, acid resistance, etc. and superior in stain resistance.
摘要翻译：本发明提供一种热固性有机溶剂型涂料，其能够在20℃下形成具有15℃以上的TUKON硬度的固化涂膜，在110Hz的温度范围内形成频率为110Hz的动态模量E'的最小值 150-200℃，1×10 9 dyn / cm 2以上。与由用作汽车面漆的常规有机溶剂型涂料形成的固化膜（例如含有含羟基的丙烯酸树脂的主要成分的有机溶剂型涂料）相比，由涂层形成的固化膜三聚氰胺树脂或羧基环氧型涂料）在耐候性，外观，耐酸性等方面至少相当，并且耐污染性优异。

5. 发明授权

US6015848A Coating composition and method for application thereof 失效
标题翻译：涂料组合物及其应用方法
公开(公告)号：US6015848A
公开(公告)日：2000-01-18
申请号：US985907
申请日：1997-12-05
申请人： Satoshi Ikushima , Seiji Wada , Yasumasa Okumura , Haruhiko Aida , Motoshi Yabuta , Yoshiyuki Yukawa , Ken-ichi Hasada
发明人： Satoshi Ikushima , Seiji Wada , Yasumasa Okumura , Haruhiko Aida , Motoshi Yabuta , Yoshiyuki Yukawa , Ken-ichi Hasada
IPC分类号： C08G59/24 , C08L27/12 , C08L33/06 , C08L33/16 , C08L63/00 , C08L63/02 , C09D133/06 , C09D163/00 , C08J3/28 , C08L83/04
CPC分类号： C08L63/00 , C08G59/24 , C09D133/068 , C09D163/00 , C08L27/12 , C08L33/068 , C08L33/16 , Y10S525/922
摘要： The present invention provides a thermosetting organic solvent type coating capable of forming a cured coating film having a TUKON hardness at 20.degree. C. of 15 or more and the minimum value of dynamic modulus E' at a frequency of 110 Hz in the temperature range of 150-200.degree. C., of 1.times.1O.sup.9 dyn/cm.sup.2 or more. The cured film formed from the coating, as compared with the cured films formed from conventional organic solvent type coatings used as a top coat for automobile (e.g. an organic solvent type coating containing, as main components, a hydroxyl group-containing acrylic resin and a melamine resin, or a carboxylic-epoxy type coating), is at least equivalent in weatherability, finish appearance, acid resistance, etc. and superior in stain resistance.
摘要翻译：本发明提供一种热固性有机溶剂型涂料，其能够在20℃下的TUKON硬度形成15或更高的固化涂膜，并且在110℃的频率下在110Hz的频率下形成动态模量E'的最小值 150-200℃，为1×10 9 dyn / cm 2以上。与由用作汽车面漆的常规有机溶剂型涂料形成的固化膜（例如含有含羟基的丙烯酸树脂的主要成分的有机溶剂型涂料）相比，由涂层形成的固化膜三聚氰胺树脂或羧基环氧型涂料）在耐候性，外观，耐酸性等方面至少相当，并且耐污染性优异。

6. 发明授权

US5296551A Self-crosslinking resin 失效
标题翻译：自交联树脂
公开(公告)号：US5296551A
公开(公告)日：1994-03-22
申请号：US97236
申请日：1993-07-27
申请人： Yoshiyuki Yukawa , Motoshi Yabuta , Akimasa Nakahata , Kazunori Mayumi
发明人： Yoshiyuki Yukawa , Motoshi Yabuta , Akimasa Nakahata , Kazunori Mayumi
IPC分类号： C08G18/10 , C08G18/42 , C08G18/72 , C08G18/80 , C08G18/81 , C09D175/00 , C09D175/06 , C08G81/02
CPC分类号： C08G18/728 , C08G18/10 , C08G18/42
摘要： The present invention provides(1) a self-crosslinking resin (I) having a blocked isocyanate group and a hydroxyl group in the molecule and characterized in that the resin is prepared from a vinyl polymer (A) having at least two free isocyanate groups in the molecule and a polyester resin (B) having at least two hydroxyl groups in the molecule by reacting some of the hydroxyl groups of the resin (B) with some of the free isocyanate groups of the polymer (A), and subsequently reacting a blocking agent with all the remaining free isocyanate groups, and(2) a self-crosslinking resin (II) having a blocked isocyanate group and a hydroxyl group in the molecule and characterized in that the resin is prepared from a vinyl polymer (C) having a free isocyanate group and a blocked isocyanate group in the molecule and the polyester resin (B) having at least two hydroxyl groups in the molecule by reacting some of the hydroxyl groups of the resin (B) with all the free isocyanate groups of the polymer (C).
摘要翻译：本发明提供（1）在分子中具有封端异氰酸酯基和羟基的自交联树脂（I），其特征在于，所述树脂由具有至少两个游离异氰酸酯基的乙烯基聚合物（A）所述分子和通过使所述树脂（B）的一些羟基与所述聚合物（A）的一些游离异氰酸酯基团反应而在所述分子中具有至少两个羟基的聚酯树脂（B）反应，具有所有剩余的游离异氰酸酯基团的试剂，和（2）在分子中具有封端的异氰酸酯基和羟基的自交联树脂（II），其特征在于，树脂由乙烯基聚合物（C）制备，游离异氰酸酯基和分子内的封端异氰酸酯基和分子中具有至少两个羟基的聚酯树脂（B），其中树脂（B）的一些羟基与聚合物的所有游离异氰酸酯基反应 r（C）。

7. 发明授权

US5124399A Process for preparation of self-curing resin 失效
标题翻译：自固化树脂的制备方法
公开(公告)号：US5124399A
公开(公告)日：1992-06-23
申请号：US709460
申请日：1991-06-03
申请人： Motoshi Yabuta , Yasushi Nakao , Yoshiyuki Yukawa
发明人： Motoshi Yabuta , Yasushi Nakao , Yoshiyuki Yukawa
IPC分类号： C08G18/83 , C08G18/08 , C08G18/32 , C08G18/72 , C08G18/80
CPC分类号： C08G18/728 , C08G18/0814 , C08G18/3271 , C08G18/8041 , C08G18/8061 , C08G18/8077
摘要： The present invention provides a process for preparing a self-curing resin having a blocked isocyanate group and a hydroxyl group in the molecule from a polymer 500 to 50000 in number average molecular weight and having a tertiary amino group and/or a quaternary ammonium group, and at least two isocyanate groups in the molecule, the process comprising the steps of partly blocking the isocyanate groups in the skeleton of the polymer, and reacting the remaining unblocked isocyanate groups with an alkanolamine to introduce hydroxyl groups into the polymer.
摘要翻译：本发明提供一种在数均分子量为500〜50000的分子内具有封端异氰酸酯基和羟基的自固化树脂的制备方法，其具有叔氨基和/或季铵基，和至少两个异氰酸酯基团，该方法包括以下步骤：部分地封闭聚合物骨架中的异氰酸酯基团，并使剩余的未封端的异氰酸酯基团与链烷醇胺反应，以将羟基引入聚合物中。

8. 发明授权

US5587426A Process for preparing self-crosslinking resin 失效
标题翻译：自交联树脂的制备方法
公开(公告)号：US5587426A
公开(公告)日：1996-12-24
申请号：US024774
申请日：1993-03-02
申请人： Yoshiyuki Yukawa , Motoshi Yabuta , Akimasa Nakahata , Yoh Sugimura
发明人： Yoshiyuki Yukawa , Motoshi Yabuta , Akimasa Nakahata , Yoh Sugimura
IPC分类号： C08G18/10 , C08G18/62 , C08G18/70 , C08G18/72 , C08G18/80 , C08G81/02
CPC分类号： C08G18/8061 , C08G18/10 , C08G18/6229 , C08G18/6254 , C08G18/728
摘要： The present invention provides:(1) a self-crosslinking resin (I) having a blocked isocyanate group and a hydroxyl group in the molecule and characterized in that the resin is prepared from a vinyl polymer (A) having at least two free isocyanate groups in the molecule and an acrylic resin (B) having at least two hydroxyl groups in the molecule by reacting some of the hydroxyl groups of the resin (B) with some of the free isocyanate groups of the polymer (A), and subsequently reacting a blocking agent with all the remaining free isocyanate groups, and(2) a self-crosslinking resin (II) having a blocked isocyanate group and a hydroxyl group in the molecule and characterized in that the resin is prepared from a vinyl polymer (C) having a free isocyanate group and a blocked isocyanate group in the molecule and the acrylic resin (B) having at least two hydroxyl groups in the molecule by reacting some of the hydroxyl groups of the resin (B) with all the free isocyanate groups of the polymer (C).
摘要翻译：本发明提供：（1）分子中具有封端异氰酸酯基和羟基的自交联树脂（I），其特征在于，所述树脂由具有至少两个游离异氰酸酯基的乙烯基聚合物（A）在分子中具有至少两个羟基的丙烯酸树脂（B），其中树脂（B）的一些羟基与聚合物（A）的一些游离异氰酸酯基团反应，然后使具有所有剩余的游离异氰酸酯基团的封端剂，和（2）分子中具有封端的异氰酸酯基和羟基的自交联树脂（II），其特征在于，树脂由具有通过使树脂（B）的一些羟基与聚合物中的所有游离异氰酸酯基团反应，分子中的游离异氰酸酯基和封端的异氰酸酯基和分子中具有至少两个羟基的丙烯酸树脂（B）（C）。

9. 发明授权

US5274045A Self-crosslinkable resin 失效
标题翻译：自交联树脂
公开(公告)号：US5274045A
公开(公告)日：1993-12-28
申请号：US842565
申请日：1992-02-27
申请人： Yoshiyuki Yukawa , Motoshi Yabuta , Yasushi Nakao
发明人： Yoshiyuki Yukawa , Motoshi Yabuta , Yasushi Nakao
IPC分类号： C08G18/67 , C08F290/06 , C08F290/14 , C08G18/72 , C08G18/80 , C09D175/04 , C09D175/14 , C09J175/00 , C09J175/04
CPC分类号： C08F290/147 , C08G18/728
摘要： A self-crosslinkable resin useful as, for example, adhesive compositions and coating compositions. The resin contains complementary reactive groups, that is, a blocked isocyanate group and a hydroxyl group, in the same molecule. The resin is prepared by reacting a hydroxy-containing vinyl monomer with some isocyanate groups on the skeleton of a vinyl polymer having at least two isocyanate groups in the molecule so to introduce a polymerizable double bond into the polymer, and subsequently completely blocking the isocyanate group(s) remaining on the polymer skeleton with a blocking agent, or vice versa. Thereafter an unsaturated monomer component consisting essentially of a hydroxyl-containing vinyl monomer is polymerized with the polymerizable double bond introduced.

10. 发明授权

US5780113A Method for formation of coating film 失效
标题翻译：涂膜形成方法
公开(公告)号：US5780113A
公开(公告)日：1998-07-14
申请号：US833118
申请日：1997-04-04
申请人： Yutaka Masuda , Akimasa Nakahata , Yoshiyuki Yukawa , Motoshi Yabuta
发明人： Yutaka Masuda , Akimasa Nakahata , Yoshiyuki Yukawa , Motoshi Yabuta
IPC分类号： B05D5/06 , B05D7/00 , B05D7/14
CPC分类号： B05D7/57 , B05D5/068
摘要： The present invention provides a method for forming a multi-layer coating film by applying a clear coating (B) on the film of a leafing type aluminum flake-containing metallic coating (A), which method comprises forming a film of the metallic coating (A), curing the film, applying thereon a composition (C) containing a polymer formed from an unsaturated monomer having a phosphoric acid group represented by --O--PO(OH)(R.sub.1) (wherein R.sub.1 is a hydroxyl group, a phenyl group or a C.sub.1-20 alkyl group) and a hydroxyl group-containing unsaturated monomer, and then applying the clear coating (B) on the film of the composition (C). The method can form a multi-layer coating film improved in interlayer adhesivity between the metallic coating film and the clear coating film, without reducing the excellent effects and metallic feeling provided by a metallic coating film containing leafing type aluminum flake.
摘要翻译：本发明提供了一种通过在含叶片状的含铝薄片的金属涂层（A）的薄膜上涂布透明涂层（B）来形成多层涂膜的方法，该方法包括形成金属涂层的膜 A），固化该膜，在其上涂覆含有由具有由-O-PO（OH）（R1）表示的磷酸基的不饱和单体形成的聚合物的组合物（C）（其中R1是羟基，苯基或C 1-20烷基）和含羟基的不饱和单体，然后将透明涂层（B）涂布在组合物（C）的膜上。该方法可以形成改善金属涂膜和透明涂膜之间层间粘合性的多层涂膜，而不会降低由含叶片型铝片的金属涂膜提供的优异的效果和金属感。

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