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1. 发明专利

JP2011011201A Carbon-based solid acid and method for producing the same 有权
标题翻译：碳基固体酸及其制造方法
公开(公告)号：JP2011011201A
公开(公告)日：2011-01-20
申请号：JP2009210531
申请日：2009-09-11
申请人： Futamura Chemical Co Ltd , Kanagawa Acad Of Sci & Technol , Nisso Engineering Co Ltd , Tokyo Institute Of Technology , フタムラ化学株式会社 , 国立大学法人東京工業大学 , 日曹エンジニアリング株式会社 , 財団法人神奈川科学技術アカデミー
发明人： KITANO MASAAKI , HARA YUKIKAZU , KODAMA ATSUSHI , KOSAKA TSUTOMU , ISHIKAWA TAKAHIRO , SUDO TOSHIYUKI , IWAKOSHI MARI , YONETANI AKIRA
IPC分类号： B01J31/26 , B01J31/02 , B01J35/10 , B01J37/08 , C07C309/28 , C07C309/62
摘要： PROBLEM TO BE SOLVED: To provide a carbon-based solid acid capable of being produced from raw materials which can be obtained at low prices and are suitable for mass production and to provide a method for producing the carbon-based solid acid, which satisfies preparation conditions suitable for producing the carbon-based solid acid and the efficiency of which is made higher than that of a method for producing the carbon-based solid acid by a reaction using strong sulfuric acid or fuming sulfuric acid.SOLUTION: The carbon-based solid acid includes porous carbon into which a sulfonate group is introduced and which has 3-1,600 m/g BET specific surface area to be defined below. The amount of the sulfonate group in the porous carbon is ≥0.2 mmol/g. The porous carbon is sulfonated by bringing sulfur trioxide or a sulfur trioxide-containing sulfonating agent into contact with a cellulose-containing raw material or a vegetable raw material. Otherwise, the porous carbon is sulfonated by impregnating the vegetable raw material with zinc chloride or phosphoric acid, heating and preliminarily carbonating the raw material thus impregnated, and heating and sulfonating the preliminarily-carbonated raw material in strong sulfuric acid or fuming sulfuric acid or in the gas or liquid of sulfur trioxide.
摘要翻译：要解决的问题：提供能够以低价格获得并适合于批量生产的原料生产的碳基固体酸，并提供满足制备的碳基固体酸的制备方法适用于生产碳基固体酸的条件，其效率高于通过使用强硫酸或发烟硫酸的反应生产碳基固体酸的方法。条件：碳基固体酸包括其中引入磺酸盐基团的多孔碳，其具有下面定义的3-1,600m 2 / g BET比表面积。多孔碳中磺酸盐基团的量为≥0.2mmol/ g。通过使三氧化硫或含三氧化硫的磺化剂与含纤维素的原料或植物原料接触来将多孔碳磺化。另外，通过用氯化锌或磷酸浸渍植物原料来对多孔碳进行磺化，对浸渍的原料进行加热并预先碳酸化，并将预先碳酸化的原料在强硫酸或发烟硫酸或三氧化硫的气体或液体。

2. 发明专利

JP2012102072A Adsorbent for medicine and its production method 有权
标题翻译：药物摄入及其生产方法
公开(公告)号：JP2012102072A
公开(公告)日：2012-05-31
申请号：JP2011200213
申请日：2011-09-14
申请人： Futamura Chemical Co Ltd , フタムラ化学株式会社
发明人： KUROKAWA HIROYUKI , HIBI KEITA , KOSAKA TSUTOMU , SUZUKI KEISUKE
IPC分类号： A61K33/44 , A61P1/16 , A61P13/12 , C01B32/336
CPC分类号： A61L15/18 , A61K9/14 , A61K33/44 , B01J20/20 , B01J20/28004 , B01J20/28011 , B01J20/28064 , B01J20/28066 , B01J20/2808 , B01J20/28083 , B01J20/3078 , C01B32/336
摘要： PROBLEM TO BE SOLVED: To provide an adsorbent for medicine for oral administration which is excellent in the adsorption capacity and selective adsorption of a toxin which should be removed while being small in dose amount, favorable in terms of economy and suppressed in environmental load.SOLUTION: The adsorbent for medicine for oral administration is characterized in that the adsorbent is composed of granular activated carbon which is obtained by carbonizing and activating refined cellulose or regenerated cellulose, and in which an average fine pore diameter is 1.5 to 2.2 nm, a BET-ratio surface area is 700 to 3,000 m/g, an average particle diameter is 100 to 1,100 μm, a surface oxidation amount is not smaller than 0.05 meq/g, and filling density is 0.4 to 0.8 g/mL, and which is used as an oral administration therapeutic agent or an oral administration prevention agent for a renal disease or a liver disease.
摘要翻译：待解决的问题：提供一种口服药物用吸附剂，其吸附能力优异且选择性吸附毒素，其剂量少，应该被去除，有利于经济性和环境抑制加载。解决方案：用于口服药物的吸附剂的特征在于吸附剂由通过碳化和活化精制纤维素或再生纤维素获得的颗粒活性炭组成，其中平均细孔直径为1.5至2.2nm BET比表面积为700〜3000μm，平均粒径为100〜1100μm，表面氧化量不小于0.05meq / g ，填充密度为0.4〜0.8g / mL，用作肾脏疾病或肝脏疾病的口服给药治疗剂或口服给药预防剂。版权所有（C）2012，JPO＆INPIT

3. 发明专利

JP2007197338A Medicinal adsorbent 有权
标题翻译：药物吸收剂
公开(公告)号：JP2007197338A
公开(公告)日：2007-08-09
申请号：JP2006015221
申请日：2006-01-24
申请人： Futamura Chemical Co Ltd , Gun Ei Chem Ind Co Ltd , Merck Seiyaku Kk , フタムラ化学株式会社 , メルク製薬株式会社 , 群栄化学工業株式会社
发明人： UMEKAWA TOMOMICHI , KOSAKA TSUTOMU , ISHIHARA KAZUHIRO , HIBI KEITA , INAGAKI TOMOMI , HATORI TOICHIRO
IPC分类号： A61K33/44 , A61P1/00 , A61P39/02
摘要： PROBLEM TO BE SOLVED: To provide a medicinal adsorbent which hardly causes side effects such as constipation, is excellent in the adsorption of ionic organic compounds causing uremia and the like, exhibits sufficient adsorption performance at a small dose, and inhibits the adsorption of compounds necessary for living bodies.
SOLUTION: This medicinal adsorbent is characterized by comprising spherical activated carbon which is obtained by carbonizing and activating a spherical phenolic resin produced by the condensation reaction of a phenol compound with an aldehyde compound in a phenol compound/aldehyde compound condensation reaction molar ratio of 1.0 to 2.3, and satisfies a specific surface area of 800 to 2,000 m
2 /g, a pore volume of 0.2 to 1.0 mL/g, a packing density of 0.5 to 0.7 g/mL, an average pore diameter of 1.7 to 2.0 nm, the maximum particle diameter of ≤425 μm, an average particle diameter of ≤350 μm, a total pore (having pore diameters of ≤1.0 nm) volume of ≥55% based on the total volume of all the pores, and a total pore (having pore diameters of 20 to 1,000 nm) volume of ≤0.04 mL/g.
COPYRIGHT: (C)2007,JPO&INPIT
摘要翻译：待解决的问题：为了提供几乎不引起便秘等副作用的药物吸附剂，引起尿毒症等的离子性有机化合物的吸附性优异，在小剂量下表现出充分的吸附性能，并抑制吸附的生物体必需的化合物。解决方案：该药用吸附剂的特征在于包含球形活性炭，其通过使苯酚化合物与醛化合物在醛化合物中的缩合反应生成的球形酚醛树脂以酚化合物/醛化合物缩合反应摩尔比为1.0〜2.3，比表面积为800〜2000m 2 / SP / g，孔体积为0.2〜1.0mL / g，填充密度为0.5〜0.7g / mL，平均孔径为1.7〜2.0nm，最大粒径≤425μm，平均粒径≤350μm，总孔径（孔径≤1.0nm）体积为≥55％，基于总体积所有孔和总孔（孔径为20〜1000nm）体积≤0.04mL/ g。版权所有（C）2007，JPO＆INPIT

4. 发明专利

JP2014004561A Cellulose-based binder molded solid acid and method for producing the same 有权
标题翻译：基于纤维素的粘合剂模制的固体酸及其生产方法
公开(公告)号：JP2014004561A
公开(公告)日：2014-01-16
申请号：JP2012143391
申请日：2012-06-26
申请人： Futamura Chemical Co Ltd , フタムラ化学株式会社
发明人： KODAMA ATSUSHI , MATSUOKA YOHEI , YAMADA HIROSHI , KOSAKA TSUTOMU
IPC分类号： B01J31/26 , B01J27/22 , B01J31/02
摘要： PROBLEM TO BE SOLVED: To provide molded solid acids and a method for producing the same in which the cost is lowered by employing woody raw materials and at the same time by choosing a binder itself from cellulose-based materials the binder can be made carbonizable thereby avoiding deterioration of the catalytic performance for which the binder itself may exert its influence, and which has a high degree of freedom of a shape design.SOLUTION: A method for producing the cellulose-based binder molded solid acids comprises: a raw materials kneading step of kneading raw materials to obtain a kneaded woody raw materials product by kneading together a woody raw materials powder and a cellulose-based binder selected from methyl cellulose, carboxymethyl cellulose or viscose; a molding step to obtain a molded raw materials product by molding the kneaded woody raw materials product into a predetermined shape; a carbonization step to obtain a molded carbide by calcinating the molded raw materials product under an inert atmosphere; and a sulfonation step to obtain a molded solid acid product by incorporating a sulfo group into the molded carbide.
摘要翻译：要解决的问题：提供成型固体酸及其制造方法，其中通过使用木质原料降低成本，同时通过从纤维素基材料中选择粘合剂本身，可以使粘合剂可碳化，从而避免粘合剂本身可能发挥其影响的催化性能的劣化，并且具有高的形状设计自由度。解决方案：一种用于生产纤维素基粘合剂的固体酸的方法包括：原料捏合步骤捏合原料以通过将木质原料粉末和选自甲基纤维素，羧甲基纤维素或粘胶纤维素的纤维素类粘合剂混合在一起来获得捏合的木质原料产品; 模制步骤，通过将捏合的木质原料产品模制成预定形状来获得模制原料产品; 碳化步骤，通过在惰性气氛下煅烧模制原料产品来获得模制的碳化物; 和磺化步骤，通过将磺基掺入到模制的碳化物中来获得模制的固体酸产物。

5. 发明专利

JP2014004560A Granular solid acid and method for producing the same 有权
标题翻译：颗粒状固体酸及其制造方法
公开(公告)号：JP2014004560A
公开(公告)日：2014-01-16
申请号：JP2012143390
申请日：2012-06-26
申请人： Futamura Chemical Co Ltd , フタムラ化学株式会社
发明人： KODAMA ATSUSHI , MATSUOKA YOHEI , YAMADA HIROSHI , KOSAKA TSUTOMU
IPC分类号： B01J31/02 , B01J27/22 , C07C303/06 , C07C309/62
摘要： PROBLEM TO BE SOLVED: To provide a granular solid acid capable of maintaining granular shape thereof in a production process independently of a binder, capable of retaining a catalytic activity, and having high design freedom for a granule diameter, and a method for producing the same.SOLUTION: A method for producing a granular solid acid comprises: molding regenerated cellulose derived from viscose to a granular shape to obtain a granular cellulose raw material, as a raw material preparation step; calcining the granular cellulose raw material at 290°C-420°C under an inert atmosphere to obtain a granular carbonized material having granule diameter of 0.075 mm or more, as a carbonization step; and introducing sulfo groups into the granular carbonized material in oleum, as a sulfonation step. The sulfo group content in the granular solid acid is 0.7-2.7 mmol/g. The granular solid acid produced according to the method is also provided.
摘要翻译：要解决的问题：提供能够保持其催化活性并且具有高的颗粒直径设计自由度的与粘合剂无关的生产过程中能够保持其颗粒形状的颗粒状固体酸及其制备方法解决方案：一种颗粒状固体酸的制造方法，其特征在于，将来自粘胶的再生纤维素成型为粒状，得到粒状纤维素原料作为原料制备工序; 在290℃〜420℃的惰性气氛下煅烧粒状纤维素原料，得到粒径为0.075mm以上的粒状碳化物作为碳化工序; 并将磺基引入发烟硫酸的颗粒碳化材料中，作为磺化步骤。颗粒状固体酸中的磺基含量为0.7-2.7mmol / g。还提供了根据该方法生产的颗粒状固体酸。

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