基本信息:
- 专利标题: CONTROLLING DOPING OF SYNTHETIC DIAMOND MATERIAL
- 专利标题(中):控制合成金刚石材料的掺杂
- 申请号:PCT/EP2011/072820 申请日:2011-12-14
- 公开(公告)号:WO2012084656A1 公开(公告)日:2012-06-28
- 发明人: COE, Steven Edward , WILMAN, Jonathan James , TWITCHEN, Daniel James , SCARSBROOK, Geoffrey Alan , BRANDON, John Robert , WORT, Christopher John Howard , MARKHAM, Matthew Lee
- 申请人: ELEMENT SIX LIMITED , COE, Steven Edward , WILMAN, Jonathan James , TWITCHEN, Daniel James , SCARSBROOK, Geoffrey Alan , BRANDON, John Robert , WORT, Christopher John Howard , MARKHAM, Matthew Lee
- 申请人地址: Isle of Man Freeport P O Box 6 Ballasalla Isle of Man IM99 6AQ GB
- 专利权人: ELEMENT SIX LIMITED,COE, Steven Edward,WILMAN, Jonathan James,TWITCHEN, Daniel James,SCARSBROOK, Geoffrey Alan,BRANDON, John Robert,WORT, Christopher John Howard,MARKHAM, Matthew Lee
- 当前专利权人: ELEMENT SIX LIMITED,COE, Steven Edward,WILMAN, Jonathan James,TWITCHEN, Daniel James,SCARSBROOK, Geoffrey Alan,BRANDON, John Robert,WORT, Christopher John Howard,MARKHAM, Matthew Lee
- 当前专利权人地址: Isle of Man Freeport P O Box 6 Ballasalla Isle of Man IM99 6AQ GB
- 代理机构: ATKINSON, Ian Anthony et al.
- 优先权: GB1021870.9 20101223; US61/439,322 20110203; GB1102877.6 20110218; US61/448,894 20110303
- 主分类号: H01J37/32
- IPC分类号: H01J37/32 ; C30B29/04
摘要:
A method of manufacturing synthetic CVD diamond material, the method comprising: providing a microwave plasma reactor comprising: a plasma chamber; one or more substrates disposed in the plasma chamber providing a growth surface area over which the synthetic CVD diamond material is to be deposited in use; a microwave coupling configuration for feeding microwaves from a microwave generator into the plasma chamber; and a gas flow system for feeding process gases into the plasma chamber and removing them therefrom, injecting process gases into the plasma chamber; feeding microwaves from the microwave generator into the plasma chamber through the microwave coupling configuration to form a plasma above the growth surface area; and growing synthetic CVD diamond material over the growth surface area, wherein the process gases comprise at least one dopant in gaseous form, selected from a one or more of boron, silicon, sulphur, phosphorous, lithium and beryllium at a concentration equal to or greater than 0.01 ppm and/or nitrogen at a concentration equal to or greater than 0.3 ppm, wherein the gas flow system includes a gas inlet comprising one or more gas inlet nozzles disposed opposite the growth surface area and configured to inject process gases towards the growth surface area, and wherein the process gases are injected towards the growth surface area at a total gas flow rate equal to or greater than 500 standard cm 3 per minute and/or wherein the process gases are injected into the plasma chamber through the or each gas inlet nozzle with a Reynolds number a Reynolds number in a range 1 to 100.
摘要(中):
一种制造合成CVD金刚石材料的方法,所述方法包括:提供微波等离子体反应器,包括:等离子体室; 设置在等离子体室中的一个或多个衬底提供在使用中沉积合成CVD金刚石材料的生长表面区域; 用于将微波从微波发生器馈入等离子体室的微波耦合配置; 以及用于将工艺气体进料到等离子体室中并将其从其中除去的气体流系统,将工艺气体注入到等离子体室中; 通过微波耦合配置将微波从微波发生器馈送到等离子体室中,以在生长表面积之上形成等离子体; 以及在所述生长表面积上生长的合成CVD金刚石材料,其中所述工艺气体包含至少一种气体形式的掺杂剂,其选自硼,硅,硫,磷,锂和铍中的一种或多种,其浓度等于或大于 处于浓度等于或大于0.3ppm的0.01ppm和/或氮气,其中所述气体流动系统包括气体入口,所述气体入口包括与生长表面区域相对设置的一个或多个气体入口喷嘴,并且被配置为朝着生长表面注入工艺气体 并且其中所述工艺气体以等于或大于500标准立方厘米/分钟的总气体流速向所述生长表面区域注入,和/或其中所述工艺气体通过所述或每个气体入口喷嘴注入所述等离子体室 雷诺数雷诺数在1到100之间。