发明申请
WO2008136818A2 SUSPENSIONS OF TITANIUM (IV) OXIDE PARTICLES AND PROCESS FOR THEIR PRODUCTION
审中-公开
基本信息:
- 专利标题: SUSPENSIONS OF TITANIUM (IV) OXIDE PARTICLES AND PROCESS FOR THEIR PRODUCTION
- 专利标题(中):钛(IV)氧化物颗粒的悬浮液及其生产方法
- 申请号:PCT/US2007/026106 申请日:2007-12-20
- 公开(公告)号:WO2008136818A2 公开(公告)日:2008-11-13
- 发明人: SCOTT, David, M. , TORARDI, Carmine , GRUSHIN, Vladimir
- 申请人: E. I. DU PONT DE NEMOURS AND COMPANY , SCOTT, David, M. , TORARDI, Carmine , GRUSHIN, Vladimir
- 申请人地址: 1007 Market Street Wilmington, Delaware 19898 US
- 专利权人: E. I. DU PONT DE NEMOURS AND COMPANY,SCOTT, David, M.,TORARDI, Carmine,GRUSHIN, Vladimir
- 当前专利权人: E. I. DU PONT DE NEMOURS AND COMPANY,SCOTT, David, M.,TORARDI, Carmine,GRUSHIN, Vladimir
- 当前专利权人地址: 1007 Market Street Wilmington, Delaware 19898 US
- 代理机构: SINNOTT, Jessica, M.
- 优先权: US60/876,218 20061221
摘要:
The disclosure pertains to a process for making a suspension of finely divided titanium (IV) oxide particles, comprising: vigorously mixing (a) a volume of a first component comprising a major proportion of an alcohol, a minor proportion of a titanium alkoxide and a minor proportion of a titanium alkoxide activator selected from the group consisting of water and a first aqueous base, and (b) a volume of a second component selected from the group consisting of water and a second aqueous base, at least one of the first component or the second component having a base therein, the second component being substantially free of alcohol, to form a mixture comprising a suspension of finely divided titanium (IV) oxide particles, the mixture having a water to titanium molar ratio ranging from about 40 to about 1 to about 5000 to about 1, wherein the proportion of the titanium alkoxide, the proportion of the activator, the mixing vigor, and a ratio of the volume of the first component to the volume of the second component are effective for the suspension of the finely divided particles to form in the mixture. The suspensions can be dried to recover a powder. Typically the particles are nanoparticles.
摘要(中):
本公开内容涉及制备细碎的氧化钛(IV)颗粒的悬浮液的方法,其包括:剧烈混合(a)一定体积的第一组分,所述第一组分包含主要部分的醇,少部分的钛醇盐和 少量比例的选自水和第一含水碱的烷氧基钛活化剂,和(b)一定体积的选自水和第二水性碱的第二组分,第一组分 或其中具有碱的第二组分,第二组分基本上不含醇,以形成包含细碎的钛(IV)氧化物颗粒的悬浮液的混合物,所述混合物的水与钛的摩尔比范围为约40至约 1至约5000至约1,其中钛醇盐的比例,活化剂的比例,混合活度以及第一组分与体积的比例 第二组分的e对于在混合物中形成的细碎颗粒的悬浮是有效的。 可以将悬浮液干燥以回收粉末。 通常颗粒是纳米颗粒。