基本信息:
- 专利标题: METHOD OF PARTICLE CHARACTERIZATION BASED ON FLUORESCENCE IMAGING
- 专利标题(中):基于荧光成像的粒子表征方法
- 申请号:PCT/US2002/034998 申请日:2002-10-31
- 公开(公告)号:WO2003040701A1 公开(公告)日:2003-05-15
- 发明人: BLAND, Ronald, G. , JONES, Tom
- 申请人: BAKER HUGHES INCORPORATED
- 申请人地址: 3900 Essex Lane, Suite 1200, Houston, TX 77027 US
- 专利权人: BAKER HUGHES INCORPORATED
- 当前专利权人: BAKER HUGHES INCORPORATED
- 当前专利权人地址: 3900 Essex Lane, Suite 1200, Houston, TX 77027 US
- 代理机构: WELBORN, Brian, S.
- 优先权: US60/338,311 20011102
- 主分类号: G01N15/14
- IPC分类号: G01N15/14
摘要:
The invention concerns a method for determining the particle size distribution (PSD) of bridging agents in fluids, particularly aqueous fluids used in hydrocarbon recovery such as drilling fluids, drill-in fluids, completion fluids, and the like. It was discovered that the PSD could be selectively determined for calcium carbonate as a bridging agent because it auto-fluoresces. The method is reproducible and is not bothered by the presence of other particles such as drill solids which interferes with conventional methods, for instance, light-scattering techniques. The light used to fluoresce the bridging agent may be filtered to a particular frequency if there are other components present that fluoresce. Flow cytometry is another technique that could be used to implement the invention.
摘要(中):
本发明涉及一种用于确定流体中桥连剂的颗粒尺寸分布PSD的方法,特别是用于烃回收的含水流体,例如钻井液,钻入流体,完井液等。 已经发现,由于自发荧光,PSD可以选择性地测定碳酸钙作为桥连剂。 该方法是可再现的,并且不受其它颗粒例如钻石固体的影响的困扰,这些颗粒干扰常规方法,例如光散射技术。 用于荧光桥接剂的光可以被过滤到特定的频率,如果存在荧光的其它成分。 流式细胞术是可用于实现本发明的另一种技术。