![一种微波焙烧回收三元正极材料中锂的方法](/CN/2019/1/253/images/201911266754.jpg)
基本信息:
- 专利标题: 一种微波焙烧回收三元正极材料中锂的方法
- 专利标题(英):Method for recovering lithium in ternary positive electrode material by microwave roasting
- 申请号:CN201911266754.0 申请日:2019-12-11
- 公开(公告)号:CN110817905A 公开(公告)日:2020-02-21
- 发明人: 文小强 , 周有池 , 郭春平 , 王玉香 , 刘雯雯 , 赖华生 , 普建 , 周新华
- 申请人: 赣州有色冶金研究所
- 申请人地址: 江西省赣州市经济技术开发区迎宾大道62号
- 专利权人: 赣州有色冶金研究所
- 当前专利权人: 赣州有色冶金研究所
- 当前专利权人地址: 江西省赣州市经济技术开发区迎宾大道62号
- 代理机构: 北京高沃律师事务所
- 代理人: 张敏
- 主分类号: C01D15/04
- IPC分类号: C01D15/04
The invention relates to the technical field of lithium battery material recovery, and provides a method for recovering lithium in a ternary positive electrode material by microwave roasting, whereinthe method comprises the steps: mixing a waste ternary positive electrode material, diluted hydrochloric acid and an assistant, carrying out microwave roasting, carrying out ball milling and water leaching on the roasted product to obtain a lithium chloride solution, concentrating, crystallizing, carrying out solid-liquid separation, and drying to obtain lithium chloride. According to the method provided by the invention, conventional roasting is replaced with microwave roasting, materials are heated from inside to outside through microwaves, the roasting temperature is reduced, and the roasting time is shortened; ball-milling water leaching is adopted to replace crushing and water leaching or crushing and acid leaching in a traditional method, the water leaching process is accelerated through ball-milling water leaching, the leaching rate is increased, leachate hardly contains other high-valence metal ions, and lithium chloride can be directly prepared without purification and impurity removal.
公开/授权文献:
- CN110817905B 一种微波焙烧回收三元正极材料中锂的方法 公开/授权日:2022-06-10