![一种节能环保型分散染料的制备方法](/CN/2014/1/87/images/201410438041.jpg)
基本信息:
- 专利标题: 一种节能环保型分散染料的制备方法
- 专利标题(英):Preparation method of energy-efficient and environmentally-friendly disperse dye
- 申请号:CN201410438041.9 申请日:2014-08-29
- 公开(公告)号:CN105440737A 公开(公告)日:2016-03-30
- 发明人: 徐万福 , 傅伟松 , 陈华祥 , 唐智勇 , 徐斌 , 丁亚刚
- 申请人: 浙江迪邦化工有限公司
- 申请人地址: 浙江省绍兴市上虞市杭州湾工业园区纬七东路1号
- 专利权人: 浙江迪邦化工有限公司
- 当前专利权人: 浙江迪邦化工有限公司
- 当前专利权人地址: 浙江省绍兴市上虞市杭州湾工业园区纬七东路1号
- 代理机构: 杭州天勤知识产权代理有限公司
- 代理人: 胡红娟
- 主分类号: C09B67/36
- IPC分类号: C09B67/36 ; C09B67/48 ; C09B29/085
The invention discloses a preparation method of an energy-efficient and environmentally-friendly disperse dye. The method comprises the following steps: carrying out a coupling reaction on a diazo salt and a coupling component to obtain a corresponding azo compound, adding an alkali to to adjust the pH value of the obtained system to 2-7.5, carrying out heating crystal transformation to obtain a stable crystal form, press-filtering obtained crystals, and washing the press-filtered crystals with water to obtain a dye filter cake. The method mainly has the following advantages: 1, the pH value of the system is improved, so obtaining of the stable crystal form through dye crystal transformation is facilitated, and electricity and time are saved in the sand milling process; 2, parts of the disperse dye dissolved in a mother liquor can be recovered, so the content of organic matters in the mother liquor is greatly reduced, and the wastewater treatment difficulty is reduced; 3, the filter cake mother liquor is rich in ammonium sulfate (or sodium sulfate), and can be used to prepare ammonium sulfate (or sodium sulfate), so wastewater recycling is realized; and 4, the amount of water for washing is greatly reduced, so the wastewater discharge is greatly reduced.
公开/授权文献:
- CN105440737B 一种节能环保型分散染料的制备方法 公开/授权日:2017-08-08