![一种高碱值硫化烷基酚钙的制备方法](/CN/2014/1/145/images/201410729904.jpg)
基本信息:
- 专利标题: 一种高碱值硫化烷基酚钙的制备方法
- 专利标题(英):Preparation method of overbased calcium sulfurized alkyl phenate
- 申请号:CN201410729904.8 申请日:2014-12-03
- 公开(公告)号:CN104529844A 公开(公告)日:2015-04-22
- 发明人: 禹培根 , 赵岷江 , 袁汉民 , 郭鹏飞
- 申请人: 锦州康泰润滑油添加剂股份有限公司
- 申请人地址: 辽宁省锦州市太和区福州街25号
- 专利权人: 锦州康泰润滑油添加剂股份有限公司
- 当前专利权人: 锦州康泰润滑油添加剂有限公司
- 当前专利权人地址: 辽宁省锦州市太和区福州街25号
- 代理机构: 北京超凡志成知识产权代理事务所
- 代理人: 栾波
- 主分类号: C07C323/20
- IPC分类号: C07C323/20 ; C07C319/14 ; C07C319/22 ; C10M135/30 ; C10N30/04
The invention provides a preparation method of overbased calcium sulfurized alkyl phenate. The preparation method comprises the following steps: (A) carrying out catalytic hydrogenation on a nutshell extract product and distilling to obtain m-Pentadecylphenol; (B) carrying out alkylation between 0.01-100 wt% of m-Pentadecylphenol and alpha-olefins to obtain dialkylphenol; (C) mixing the substances obtained in the above two steps with base oil, a promoter, a cosurfactant, a composite cure activator, lime and sulphur, and carrying out a neutralizing sulfuration reaction to obtain a first product; (D) adding the first product into a promoter and lime and carrying out a carbonatation reaction by introducing carbon dioxide to obtain a second product; and (E) carrying out reduced pressure distillation on the second product and filtering to obtain the product overbased calcium sulfurized alkyl phenate. The preparation method has advantages as follows: without using high-boiling point alcohol and solvent naphtha as a solvent, post-treatment cost is reduced; and the product obtained has high base number and small viscosity.
公开/授权文献:
- CN104529844B 一种高碱值硫化烷基酚钙的制备方法 公开/授权日:2016-06-22
IPC结构图谱:
C | 化学;冶金 |
--C07 | 有机化学 |
----C07C | 无环或碳环化合物 |
------C07C323/00 | 被卤素、氧或氮原子或非硫代基硫原子取代的硫醇、硫醚、氢化多硫化物或多硫化物 |
--------C07C323/01 | .硫代基和卤原子或硝基或亚硝基连接在同一碳架上 |
----------C07C323/18 | ..有至少1个硫代基的硫原子连接在碳架的六元芳环的碳原子上 |
------------C07C323/20 | ...单键氧原子连接在同一非稠合六元芳环的碳原子上 |