
基本信息:
- 专利标题: 纳米团簇结构磷酸铁的制备方法
- 专利标题(英):Preparation method for nanocluster structure iron phosphate
- 申请号:CN201210232914.1 申请日:2012-07-06
- 公开(公告)号:CN102807203A 公开(公告)日:2012-12-05
- 发明人: 艾常春 , 李耀基 , 吴元欣 , 张晖 , 阳杨 , 潘志权 , 李先福 , 吴高安 , 刘洋 , 胡意
- 申请人: 云南磷化集团有限公司 , 武汉工程大学
- 申请人地址: 云南省昆明市晋宁县昆阳镇永乐大街403号
- 专利权人: 云南磷化集团有限公司,武汉工程大学
- 当前专利权人: 云南磷化集团有限公司,武汉工程大学
- 当前专利权人地址: 云南省昆明市晋宁县昆阳镇永乐大街403号
- 代理机构: 湖北武汉永嘉专利代理有限公司
- 代理人: 崔友明
- 主分类号: C01B25/37
- IPC分类号: C01B25/37 ; B82Y40/00 ; C01B25/45 ; H01M4/58
The invention relates to a preparation method for nanocluster structure iron phosphate, which comprises the following steps of: 1) adding ferric salt solution and inorganic phosphorous compound into a percussion flow device to be mixed, or adding ferrous salt solution and inorganic phosphorous compound into the percussion flow device, meanwhile, adding oxidant into ferrous salt solution, mixing after the ferrous salt solution is completely oxidized, and obtaining mixed solution containing ferric iron ions; and 2) keeping the stirring state, regulating and controlling a reaction system by alkaline solution at a certain reaction temperature, meanwhile controlling the percussion flow speed to be 1000-3000rmp, continuously stirring after the alkaline solution is added, ageing, separating, washing with pure water, and drying to obtain the nanocluster structure iron phosphate. The preparation method for the nanocluster structure iron phosphate has the beneficial effect of simple technical process, and the good-dispersibility nanocluster structure iron phosphate of which the primary particle diameter is 10-100nm and the secondary particle diameter is 1-3mu m can be obtained.