![一种连续化生产N-甲基单乙醇胺的工艺方法](/CN/2010/1/23/images/201010117788.jpg)
基本信息:
- 专利标题: 一种连续化生产N-甲基单乙醇胺的工艺方法
- 专利标题(英):Process for continuously producing N-monomethylethanolamine
- 申请号:CN201010117788.6 申请日:2010-01-30
- 公开(公告)号:CN101830812A 公开(公告)日:2010-09-15
- 发明人: 梁坤
- 申请人: 茂名云龙工业发展有限公司
- 申请人地址: 广东省茂名市茂港区小良开发区168号茂名云龙工业发展有限公司
- 专利权人: 茂名云龙工业发展有限公司
- 当前专利权人: 茂名云龙工业发展有限公司
- 当前专利权人地址: 广东省茂名市茂港区小良开发区168号茂名云龙工业发展有限公司
- 代理机构: 东莞市华南专利商标事务所有限公司
- 代理人: 曾琦
- 主分类号: C07C215/08
- IPC分类号: C07C215/08 ; C07C213/00 ; C07C213/10
The invention discloses a process for continuously producing N-monomethylethanolamine, which comprises the following steps of: (1) pumping an ethylene oxide raw material and a monomethylamine raw material into a mixer or a two-stage mixer through a metering pump respectively, mixing the raw materials, and then reacting the mixed materials in a reactor to generate a mixture containing the N-monomethylethanolamine, wherein the mass ratio of the ethylene oxide raw material to the monomethylamine raw material is 1: 2-3; (2) delivering the mixture containing the N-monomethylethanolamine to an amine distillation tower, separating monomethylamine and an N-monomethylethanolamine coarse product by distillation, and conveying the distilled monomethylamine to a monomethylamine raw material container; and (3) conveying the N-monomethylethanolamine coarse product to a light component distillation tower and a reduced pressure rectifying tower in which efficient pore plate ripple fillers are filled and which are connected in series, separating an N-monomethylethanolamine product by continuous distillation, and continuously discharging the N-monomethylethanolamine product from the side or the topof the reduced pressure rectifying tower. The process is characterized in that the production process is continuous, the produced product has stable quality and high yield, and meanwhile, the processcan improve the yield and reduce the energy consumption and the material consumption, and is suitable for industrialized popularization and application.
公开/授权文献:
- CN101830812B 一种连续化生产N-甲基单乙醇胺的工艺方法 公开/授权日:2013-08-14
IPC结构图谱:
C | 化学;冶金 |
--C07 | 有机化学 |
----C07C | 无环或碳环化合物 |
------C07C215/00 | 含连接在同一个碳架上的氨基和羟基的化合物 |
--------C07C215/02 | .与同一个碳架的非环碳原子连接的羟基和氨基 |
----------C07C215/04 | ..碳架是饱和的 |
------------C07C215/06 | ...和无环的 |
--------------C07C215/08 | ....仅有1个羟基和1个氨基与碳架连接 |