
基本信息:
- 专利标题: 间苯二胺连续水解生产间苯二酚的工艺
- 专利标题(英):Process for producing resorcinol by continuously hydrolyzing m-phenylenediamine
- 申请号:CN200910156657.6 申请日:2009-12-31
- 公开(公告)号:CN101735019B 公开(公告)日:2012-09-26
- 发明人: 何旭斌 , 王新武 , 陶建国 , 孟明 , 朱敬鑫 , 张桂香
- 申请人: 浙江龙盛化工研究有限公司 , 浙江鸿盛化工有限公司
- 申请人地址: 浙江省上虞市杭州湾上虞工业园区纬三路15号
- 专利权人: 浙江龙盛化工研究有限公司,浙江鸿盛化工有限公司
- 当前专利权人: 浙江鸿盛化工有限公司,上海鸿源鑫创材料科技有限公司,浙江龙盛化工研究有限公司
- 当前专利权人地址: 浙江省上虞市杭州湾上虞工业园区纬三路15号
- 代理机构: 杭州天正专利事务所有限公司
- 代理人: 黄美娟; 王兵
- 主分类号: C07C39/08
- IPC分类号: C07C39/08 ; C07C37/05
The invention discloses a process for producing resorcinol by continuously hydrolyzing m-phenylenediamine. The devices adopted by the process include a pipe mixer, a heat exchanger and a tower reactor, wherein baffle plates are distributed in the tower reactor from top down and the external wall of the tower reactor is provided with a heating pipe coil. The process comprises the following steps: 1, continuously preparing a hydrolysis raw material by using the pipe mixer to form homogeneous aqueous solution of m-phenylenediamine sulfate; 2, preheating the aqueous solution of m-phenylenediaminesulfate to 225 to 245 DEG C by the heat exchanger, continuously filling the aqueous solution of m-phenylenediamine sulfate to the tower reactor from the top part of the tower reactor, keeping the reaction and retention time of the reaction material in the tower reactor between 120 and 240 minutes, and performing continuous hydrolysis reaction; and 3, performing post-processing step of the hydrolysis reaction solution obtained by the hydrolysis reaction to obtain the resorcinol. The process has the characteristics of high equipment efficiency, short production period, high product yield, stable product quality and simple and convenient process control.
公开/授权文献:
- CN101735019A 间苯二胺连续水解生产间苯二酚的工艺 公开/授权日:2010-06-16
IPC结构图谱:
C | 化学;冶金 |
--C07 | 有机化学 |
----C07C | 无环或碳环化合物 |
------C07C37/00 | 有羟基或氧—金属基连接在六元芳环碳原子上化合物的制备 |
--------C07C37/64 | .氧—金属基连在六元芳环碳原子上的氧—金属化合物的制备 |
----------C07C39/08 | ..二羟基苯;它们的烷基化衍生物 |