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1. 发明申请

WO2008003420A2 PROCESS FOR PRODUCTION OF FATTY ACIDS, FATTY ACID ESTERS AND STEROLESTERS FROM SOAPSTOCK 审中-公开
标题翻译：生产脂肪酸，脂肪酸酯和甾醇酯的方法
公开(公告)号：WO2008003420A2
公开(公告)日：2008-01-10
申请号：PCT/EP2007/005663
申请日：2007-06-27
申请人： COGNIS IP MANAGEMENT GMBH , KEMPERS, Peter , SCHÖRKEN, Ulrich , WOLF, Thomas , SATO, Setsuo , BUENO DE ALMEIDA, Wanderson , SILVA BIZZARRI, Pablo , SHIGUERU ARAUJO, Alexssander
发明人： KEMPERS, Peter , SCHÖRKEN, Ulrich , WOLF, Thomas , SATO, Setsuo , BUENO DE ALMEIDA, Wanderson , SILVA BIZZARRI, Pablo , SHIGUERU ARAUJO, Alexssander
IPC分类号： C11B13/02 , A23K1/16 , C11C3/10
CPC分类号： C11B13/02 , A23L33/11 , C10G2300/1011 , C11C1/045 , C11C1/10 , C11C3/003 , Y02E50/13 , Y02P30/20 , Y02W30/74
摘要： The invention relates to a first process for production of fatty acids directly from any soapstock generated in the alkali refining process comprising of a) adding a lipase directly to the alkaline soapstock to facilitate hydrolysis of mono-,di- and triglycerides without prior neutralisation b) neutralizing and splitting the soaps with strong acids until reaching pH 1-6, c) separating the fatty acid phase from the aqueous by settling and/or centrifugation. In a second embodiment a second process for production of fatty acids directly from any soapstock is subject of the invention. This process comprises i) neutralizing and splitting the soaps with strong acids until reaching pH 1-6 ii) adding a lipase to facilitate mono-/di-/triglyceride hydrolysis iii) separating the fatty acid phase from the aqueous by settling and / or centrifugation In a further subject matter the invention deals with the use of said fatty acids for enzymatic or chemical synthesis of C1 to C6 alcanol esters and / or for chemical dimerisation of the fatty acids. As a consequence the invention also refers to a process for obtaining sterolesters and/or fatty acid esters characterized in that the fatty acids obtained according to the processes for production of fatty acids directly from any soapstock as aforementioned described are a) esterified with C1 to C6 alkanol with a Lipase that is selective for fatty acids and does not transesterify the sterolesters b) the fatty acid esters are separated from the sterolesters by distillation The use of said sterolesters for animal feed, food, health foods and as pharmaceutical agent for lowering cholesterol and/or as precursor for steroid synthesis as well as the use of said fatty acid esters as solvent, for the production of fatty alcohols, as biofuel, and biodiesel, as plastisicer or for dimerization is also subject of the invention.
摘要翻译：本发明涉及直接从碱精制方法中生产的任何皂液生产脂肪酸的第一种方法，包括：a）直接向碱性皂料中加入脂肪酶，以促进甘油单酯，甘油二酯和甘油三酯的水解，而无需预先中和b）用强酸中和和分解肥皂直至pH达到1-6，c）通过沉降和/或离心将脂肪酸相与水相分离。在第二个实施方案中，直接从任何皂片生产脂肪酸的第二种方法是本发明的主题。该方法包括：i）用强酸中和并分离肥皂直到达到pH 1-6 ii）加入脂肪酶以促进单 - /二 - /甘油三酯水解iii）通过沉降和/或离心将脂肪酸相与水相分离在另一主题中，本发明涉及所述脂肪酸用于C1至C6烷醇酯的酶或化学合成和/或用于脂肪酸的化学二聚化的用途。因此，本发明还涉及一种获得甾体和/或脂肪酸酯的方法，其特征在于根据如上所述直接从任何皂片生产脂肪酸的方法获得的脂肪酸是a）用C1至C6酯化链烷醇具有对脂肪酸选择性且不酯交换酯基的脂肪酶b）脂肪酸酯通过蒸馏与甾体分离使用所述甾体为动物饲料，食品，保健食品和用作降低胆固醇的药剂， /或作为类固醇合成的前体以及使用所述脂肪酸酯作为溶剂，用于生产作为生物燃料的脂肪醇和作为增塑剂的生物柴油或二聚体也是本发明的主题。

2. 发明申请

WO2006058091A1 A SYSTEM AND METHOD FOR THE RECOVERY OF AN OLEAGINOUS MATERIAL 审中-公开
标题翻译：一种用于恢复原料的系统和方法
公开(公告)号：WO2006058091A1
公开(公告)日：2006-06-01
申请号：PCT/US2005/042496
申请日：2005-11-22
申请人： CARGILL, INCORPORATED , PURTLE, Ian, C. , EYAL, Aharon, M. , VITNER, Asher
发明人： PURTLE, Ian, C. , EYAL, Aharon, M. , VITNER, Asher
IPC分类号： C11B13/00 , C11B3/00 , C11B13/02 , B01D17/04 , B01D17/02
CPC分类号： C11B13/00 , B01D17/042 , B01D17/047 , C11B3/003 , C11B13/02 , Y02W30/74
摘要： A method for the recovery of an oleaginous material from a feed stream that includes oleaginous material or an oleaginous material precursor, at least one emulsifier other than a fatty-acid salt, and water. In one embodiment, the method includes the steps of treating the feed stream to reduce the emulsification capacity of the emulsifier, and/or increase its hydrophilicity, and fractionating the treated feed stream into at least one aqueous phase and at least one lipophilic phase.
摘要翻译：一种从包含含油材料或含油材料前体，至少一种除脂肪酸盐以外的乳化剂和水的进料流中回收含油材料的方法。在一个实施方案中，该方法包括以下步骤：处理进料流以降低乳化剂的乳化能力和/或增加其亲水性，以及将经处理的进料流分馏成至少一个水相和至少一个亲油相。

3. 发明申请

WO2005095565A1 SOAPSTOCK TREATMENT 审中-公开
标题翻译： SOAPSTOCK治疗
公开(公告)号：WO2005095565A1
公开(公告)日：2005-10-13
申请号：PCT/US2005/010480
申请日：2005-03-29
申请人： CARGILL INCORPORATED , PURTLE, Ian , EYAL, Aharon , VITNER, Asher
发明人： PURTLE, Ian , EYAL, Aharon , VITNER, Asher
IPC分类号： C11B13/02
CPC分类号： C11B13/02 , C11C3/003 , Y02W30/74
摘要： A method for the recovery of fatty acids comprising a salt of the fatty acid is disclosed. The method comprises the steps of: (a) reacting the salt of the fatty acid with CO 2 and with a reagent other than hydroxide and selected from a group of compounds carrying at least one of O-H, N-H, S-H, C-O-C and C-O-N moieties, to form a reaction mixture comprising at least one of a carbonate and a bicarbonate and a product selected from fatty acids and derivatives thereof, and (b) separating the product from the reaction mixture. A method for the production of fatty acid ester from free fatty acid of crude vegetable oil is also disclosed. A free fatty acid that is substantially free of emulsifier is also disclosed.
摘要翻译：公开了一种用于回收包含脂肪酸盐的脂肪酸的方法。该方法包括以下步骤：（a）使脂肪酸的盐与二氧化碳和除氢氧化物以外的试剂选择一组携带OH，NH，SH，COC和CON部分中的至少一种的化合物反应，形成包含碳酸盐和碳酸氢盐中的至少一种和选自脂肪酸及其衍生物的产物的反应混合物，和（b）从反应混合物中分离产物。还公开了由粗植物油的游离脂肪酸生产脂肪酸酯的方法。还公开了基本上不含乳化剂的游离脂肪酸。

4. 发明申请

WO00064921A2 PROCESS OF PURIFYING PHYTOSTEROLS FROM WOOD OR PLANT-DERIVED SOURCES AND COMPOSITIONS RESULTING THEREFROM 审中-公开
标题翻译：从木材或植物衍生的来源净化植物甾醇的方法及其结果的组合物
公开(公告)号：WO00064921A2
公开(公告)日：2000-11-02
申请号：PCT/CA2000/000455
申请日：2000-04-27
IPC分类号： A61K31/575 , A61P3/06 , A61P9/10 , C07J9/00 , C11B13/00 , C11B13/02
CPC分类号： C11B13/02 , A61K31/575 , C07J9/00 , C11B13/005 , Y02W30/74 , A61K31/57 , A61K2300/00
摘要： A universal process for purifying phytosterols from a wood or plant derived source comprises extracting from the source a concentrated extract comprising phytosterols and a hydrocarbon; complexing the extract so formed with a metal salt; separating the phytosterol/metal salt complex from the hydrocarbon; washing the complex with a solvent mixture comprising one or both of a hydrocarbon and a ketone; hydrolysing the washed complex so formed and finally separating the phytosterols therefrom. A novel composition comprises beta-sitosterol, campesterol, campestanol, sitostanol and optionally brassicasterol and brassicastanol.
摘要翻译：从木材或植物衍生来源纯化植物甾醇的通用方法包括从源中提取包含植物甾醇和烃的浓缩提取物; 使由金属盐形成的提取物络合; 将植物甾醇/金属盐络合物与烃分离; 用包含一种或两种烃和酮的溶剂混合物洗涤络合物; 水解所形成的洗涤过的配合物，最后从其中分离植物甾醇。一种新型组合物包括β-谷甾醇，菜油甾醇，菜油甾醇，谷甾烷醇和任选的菜子甾醇和黄豆酚醇。

5. 发明申请

WO1996034932A1 NEUTRALIZATION OF TALL OIL SOAP 审中-公开
标题翻译：中和油脂的中和
公开(公告)号：WO1996034932A1
公开(公告)日：1996-11-07
申请号：PCT/FI1996000243
申请日：1996-05-03
申请人： OY POLARGAS AB , AITTA, Eero , VARILA, Elias
发明人： OY POLARGAS AB
IPC分类号： C11B13/02
CPC分类号： C11B13/02 , Y02W30/74
摘要： The invention relates to a method for improving the separation of water in a tall oil preparation process which comprises: a neutralization step, in which a mixture of tall oil soap and water is neutralized with carbon dioxide; a water separation step, in which the aqeuous phase containing bicarbonate is separated from the tall oil soap; and a cooking step, in which the tall oil soap obtained from the previous step is cooked with sulfuric acid in order to form tall oil, the improvement comprising the fact that, after the neutralization with carbon dioxide but before the water separation step, the pH is adjusted with an acidically reacting substance, such as bisulfite. The invention also relates to a method for the preparation of tall oil, the method comprising the steps stated above.
摘要翻译：本发明涉及一种在妥尔油制备方法中改进水分离的方法，其包括：中和步骤，其中妥尔油皂和水的混合物用二氧化碳中和; 水分离步骤，其中含有碳酸氢盐的酸性相与妥尔油皂分离; 以及烹饪步骤，其中由上一步获得的妥尔油皂以硫酸烹制以形成妥尔油，其改进包括以下事实：在用二氧化碳中和但在水分离步骤之前，将pH 用酸反应物质如亚硫酸氢盐进行调节。本发明还涉及一种制备妥尔油的方法，该方法包括上述步骤。

6. 发明申请

WO2022265930A1 UPGRADING BIO-WASTE IN FCC 审中-公开
公开(公告)号：WO2022265930A1
公开(公告)日：2022-12-22
申请号：PCT/US2022/033042
申请日：2022-06-10
申请人： EXXONMOBIL TECHNOLOGY AND ENGINEERING COMPANY
发明人： XU, Xiaochun , CAMPANI, Dario , KIM, Hyung, Rae
IPC分类号： C10G3/00 , C11B1/04 , C11B1/16 , C11B1/10 , C11C3/00 , C10G11/18 , C11B13/02
摘要： A method may include: providing bio waste stream wherein the bio waste stream comprises at least one bio waste selected from the group consisting of palm oil mill effluent, soapstock, and combinations thereof; introducing the bio waste effluent stream into a fluidized catalytic cracking unit; contacting the bio waste with a catalyst in the fluidized catalytic caching unit; and cracking at least a portion of the bio waste stream to form cracked products that comprise a cracked product stream.

7. 发明申请

WO2022185258A1 RECOVERY METHOD FOR NEUTRAL AND LIPID COMPONENTS CONTAINED IN TALL OIL SOAP (TOS) OR ITS SAPONIFIED DERIVATIVES: LIPID COMPONENTS SUCH AS FATTY ACIDS (FA), ROSINIC ACIDS (RA), NEUTRAL COMPONENTS OR NEUTRAL MATERIAL (NM) INCLUDING PHYTOSTEROLS 审中-公开
公开(公告)号：WO2022185258A1
公开(公告)日：2022-09-09
申请号：PCT/IB2022/051901
申请日：2022-03-03
申请人： AMERICAN BIOPROCESS LIMITADA , FUENZALIDA DIAZ, Miguel Angel
发明人： MANCILLA VILLALOBOS, Rodrigo Alejandro , ARAVENA CONTRERAS, Raúl Ignacio
IPC分类号： C11B13/02 , C11B3/04 , C07J9/00
摘要： The invention relates to a method of separation and recovery of neutral and lipid components contained in saponifiable mixtures such as lipids and residues of plant and animal origin or saponified such as Tall Oil Soap (TOS), or in their saponified derivatives, said method is based on differences in their solubility in a solvent or in a mixture of solvents from the group consisting of water and alcohols.

8. 发明申请

WO2021260275A1 METHOD FOR PROCESSING BLACK LIQUOR SOAP 审中-公开
公开(公告)号：WO2021260275A1
公开(公告)日：2021-12-30
申请号：PCT/FI2021/050495
申请日：2021-06-24
申请人： MOLCYCLE OY
发明人： RAATIKAINEN, Olavi , SUVANTO, Petro , VEPSÄLÄINEN, Jouko , LEPPÄNEN, Jukka , TURHANEN, Petri
IPC分类号： C11B13/02 , C11C3/00
摘要： The invention relates to a method for processing black liquor soap, particularly to a method for producing and recovering fatty acid esters and resin acids from black liquor soap. The method is based on a catalytic selective esterification of the soap.

9. 发明申请

WO2013173077A2 SEMI-CONTINUOUS ACIDULATION PROCESS 审中-公开
标题翻译：半连续处理过程
公开(公告)号：WO2013173077A2
公开(公告)日：2013-11-21
申请号：PCT/US2013039322
申请日：2013-05-02
申请人： ARIZONA CHEMICAL CO LLC
发明人： BOWLES ROBERT E , GRIFFIN JOSEPH H
IPC分类号： C11B13/02
CPC分类号： C11B13/02 , B01D21/00 , B01J19/2415 , B01J19/242 , B01J19/2425 , B01J2219/00002 , B01J2219/00031 , B01J2219/00123 , B01J2219/00765 , B01J2219/0286 , C11B13/005 , Y02W30/74
摘要： A semi-continuous acidulation process for converting tall oil soap to crude tall oil is disclosed. Reactants are continuously mixed, and the product mixture is continuously transferred to a settling tank having a conical lower section and a capacity at least 25 times that of the mixer. Batches settle to give a solid phase comprising calcium sulfate, a clean spent acid phase, a dirty spent acid phase, and a crude tall oil phase. Each phase is removed sequentially through a port at or near the bottom of the settling tank. Compared with traditional batch acidulation, continuous mixing minimizes the corrosive environment and enables the use of less expensive materials for the settling tank. Sequential removal of four phases from one port allows calcium sulfate to be purged from every batch, permits clean separation of clean spent acid from dirty spent acid, and enables clean recovery of tall oil. Compared with processes that isolate product continuously, inherent difficulties in using centrifuges or continuous decanters to separate four phases are avoided. The process facilitates generation of clean alkaline brine and integration of new soap washing methods that enable improved conversion yields of CTO and better removal of calcium from the soap.
摘要翻译：公开了一种用于将妥尔油皂转化为粗妥尔油的半连续酸化方法。将反应物连续混合，将产物混合物连续地转移到具有锥形下部和至少是混合器的25倍的容量的沉淀槽中。批料沉淀以得到包含硫酸钙，清洁的废酸相，脏的废酸相和粗的妥尔油相的固相。每个阶段依次通过位于沉淀池底部或附近的端口排出。与传统的批量酸化相比，连续混合可最大限度地减少腐蚀环境，并可使用较便宜的沉淀池材料。从一个端口连续去除四相允许从每批次中清除硫酸钙，允许从脏的废酸中清洁分离清洁的废酸，并能清洁回收妥尔油。与连续分离产品的方法相比，避免了使用离心机或连续滗析器分离四相的固有困难。该方法有助于生成清洁的碱性盐水并整合新的皂洗方法，从而提高CTO的转化率，并更好地从皂中去除钙。

10. 发明申请

WO2010136079A1 PROCESS FOR PRODUCING TALL OIL AND USE OF BRINE DEACTIVATION IN THE PRODUCTION OF TALL OIL 审中-公开
标题翻译：生产沥青的方法和使用脱水在生产油中
公开(公告)号：WO2010136079A1
公开(公告)日：2010-12-02
申请号：PCT/EP2009/057340
申请日：2009-06-15
申请人： LINDE AKTIENGESELLSCHAFT , VUORIKARI, Olavi , LEINO, Hannu , KJELLBERG, Nils
发明人： VUORIKARI, Olavi , LEINO, Hannu , KJELLBERG, Nils
IPC分类号： C11B13/00 , C11B13/02 , C11C1/02
CPC分类号： C11B13/005 , C11B13/02 , C11C1/025 , Y02W30/74
摘要： The invention relates to a process for producing of tall oil from soap oil and to the use of a bicarbonate brine deactivation reaction in the production of tall oil. Soap oil is produced by neutralization of tall oil soap with carbon dioxide. Bicarbonate brine remaining in admixture with the soap oil is deactivated with a first portion of a strong acid and then the soap oil is acidulated with a second portion of a strong acid in order to free the tall oil. The deactivation reaction releases carbon dioxide gas and reduces foaming in the acidulation.
摘要翻译：本发明涉及一种从皂油中生产妥尔油的方法，以及在妥尔油的生产中使用碳酸氢盐盐水失活反应。肥皂油通过用二氧化碳中和妥尔油皂来生产。与肥皂油混合残留的碳酸氢盐盐水与强酸的第一部分失活，然后皂油用强酸的第二部分酸化，以释放妥尔油。失活反应释放二氧化碳气体并减少酸化中的起泡。

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