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    • 3. 发明申请
    • AQUEOUS SOLUTIONS OF DIRECT DYES
    • 直接染色质的水溶液
    • WO2006122891A3
    • 2007-03-15
    • PCT/EP2006062115
    • 2006-05-08
    • CIBA SC HOLDING AGLAUTENBACH HOLGERKAESER ADOLF
    • LAUTENBACH HOLGERKAESER ADOLF
    • C09B67/26C09B67/34D21H21/28
    • C09B67/0073C09B67/0076D21H21/28Y10S8/919Y10S8/921
    • The invention relates to an aqueous dye solution comprising a) 5 to 30% by weight of an anionic or cationic direct dye, b) 0.01 to 5% by weight of the compound of formula (1), in which M represents hydrogen, an alkali metal or alkaline earth metal, ammonium or ammonium, that is mono-, di-, tri- or tetra-substituted by C 1 -C 4 alkyl or C 2 -C 4 hydroxyalkyl or mixtures thereof, c) 0 to 10% by weight of an inorganic or an organic acid, d) 0 to 20% by weight of further additives and e) water to complete to 100%, with the proviso that direct dyes of the formula (2) in which K is a residue of a coupling component of the acetoacetanilide, pyridone, pyrazolone or pyrimidine series and M is as defined above, are excluded, a process for their preparation and the use thereof for dyeing paper.
    • 本发明涉及一种含水染料溶液,其包含a)5至30重量%的阴离子或阳离子直接染料,b)0.01至5重量%的式(1)化合物,其中M表示氢,碱 金属或碱土金属,铵或铵,其是被C 1 -C 4烷基或C 1 -C 4烷基取代的单 - ,二 - ,三 - 或四 - 2%-C 4羟烷基或其混合物,c)0至10重量%的无机或有机酸,d)0-20重量%的其它添加剂,和e) 水完成至100%,条件是不包括其中K为乙酰乙酰苯胺,吡啶酮,吡唑啉酮或嘧啶系列和M的偶联组分的残基的直接染料如上所定义, 其制备方法及其用于染色纸的用途。
    • 8. 发明申请
    • PROCESS FOR PREPARING SOLUTIONS OF ANIONIC ORGANIC COMPOUNDS
    • 制备阴离子有机化合物溶液的方法
    • WO01090257A2
    • 2001-11-29
    • PCT/EP2001/005796
    • 2001-05-21
    • C09B29/045C09B29/52C09B57/00C09B67/00C09B67/26C09B67/44C09B67/54D21H21/30
    • C09B67/0096Y10S8/919
    • Described is a process for preparing concentrated solutions or suspensions of anionic organic compounds which comprises a) acidifying an aqueous solution or suspension of an anionic organic compound containing salts and/or impurities to a pH of 4.5 or less, if the pH is above this value, so that b) the anionic organic compound is water-insoluble and precipitates in the form of the free acid, c) bringing the suspension to a salt content below 2 % by weight, based on the total weight of the retentate, by means of ultrafiltration with a membrane having pore diameters of from 0.001 to 0.02 mu m, and d) optionally washing out the salts with water having a pH below 4,5, e) optionally carrying out acid-free washing with water thereafter, and then f) concentrating, so that the amount of anionic organic compound is 5-50 % by weight, and g) if desired, bringing the anionic organic compound into solution by adding an appropriate base.
    • 描述了一种制备阴离子有机化合物的浓缩溶液或悬浮液的方法,其包括:a)如果pH高于该值,则酸化含有盐和/或杂质的阴离子有机化合物的水溶液或悬浮液至pH 4.5或更低 ,使得b)阴离子有机化合物是水不溶性的并以游离酸的形式沉淀,c)使悬浮液的含盐量基于渗余物的总重量低于2重量%,借助于 用孔径为0.001-0.2μm的膜进行超滤,以及d)任选地用pH低于4.5的水洗出盐,e)任选地用水进行无酸洗涤,然后f) 浓缩,阴离子有机化合物的量为5-50重量%,g)如果需要,通过加入适当的碱使阴离子有机化合物溶解。