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1. 发明申请

WO99051688A1 REACTIVE DYE COMPOUNDS 审中-公开
标题翻译：反应性染料化合物
公开(公告)号：WO99051688A1
公开(公告)日：1999-10-14
申请号：PCT/US1998/006561
申请日：1998-04-02
IPC分类号： A61K8/00 , A61K8/49 , A61Q5/06 , A61Q5/10 , C09B62/02 , C09B62/36 , D06P1/382 , A61K7/13
CPC分类号： C09B62/36 , A61K8/4926 , A61K8/494 , A61K8/4953 , A61Q5/065 , C09B62/02
摘要： Reactive dye compounds having formula (I), wherein D is a chromophore; X and Y are independently selected from SR', Cl, Br, or F, wherein R' is selected from: H, Cl-C4 alkyl, (CH2)nCOOH, (CH2)nCONH2, (CH2)nSO3H, (CH2)nCOOM, (CH2)nPO3H, (CH2)nOH, (CH2)nSSO3 , (CH2)nNR"2, (CH2)nN R"3, PhSSO3 , PhSO3H, PhPO3H, PhNR"2, PhN R"3, -CN, SO3 , (CH2)2CH(SH)R"(CH2)3COOH, -CH2CHOHCH2SH, and (1, 2, 3, 4, 5, 6, 7, 8, 9, 10, 11, 12), -CH2CH2NH2. n is an integer in the range of 1 to 4 wherein within the same molecule n is not necessarily the same integer; and M is a cation of alkaline earth metal, alkali metal, NH4 or NR"3 . L is a linking moiety; Z is a nitrogen containing heterocycle selected from pyridone, quinoxaline or pyrimidone; provided that at least one of X or Y is SR' and esters and salts thereof. The reactive dye compounds of the present invention provide improved wash fastness of dye on hair and less colour fade over time.
摘要翻译：具有式（I）的活性染料化合物，其中D是发色团; X和Y独立地选自SR'，Cl，Br或F，其中R'选自：H，C 1 -C 4烷基，（CH 2）n COOH，（CH 2）n CONH 2，（CH 2）n SO 3 H，（CH 2）n COOM ，（CH2）nPO3H，（CH2）nOH，（CH2）nSSO3 - ，（CH2）nNR“2，（CH2）nN + R”3，PhSSO3 - ，PhSO3H，PhPO3H，PhNR“ （CH 2）2 CH（SH）R“（CH 2）3 COOH，-CH 2 CHOHCH 2 SH和（1,2,3,4,5,6,7,8），9,10,11,12），-CH 2 CH 2 NH 2，n是1〜4的整数，其中在相同的分子内，n不一定是相同的整数; M是碱土金属的阳离子，碱金属， NH 4 +或NR“3 +。 L是连接部分; Z是选自吡啶酮，喹喔啉或嘧啶酮的含氮杂环; 条件是X或Y中的至少一个为SR'及其酯和盐。本发明的活性染料化合物提供染发剂在头发上的洗涤牢度提高，随着时间的推移，颜色渐渐减少。

2. 发明申请

WO99051684A1 REACTIVE DYE COMPOUNDS 审中-公开
标题翻译：反应性染料化合物
公开(公告)号：WO99051684A1
公开(公告)日：1999-10-14
申请号：PCT/US1998/006559
申请日：1998-04-02
IPC分类号： A61K8/00 , A61K8/49 , A61Q5/10 , C09B62/02 , C09B62/44 , C09B62/503 , D06P1/382 , D06P3/10
CPC分类号： C09B62/02 , C09B62/4401
摘要： A reactive dye compound comprising: (a) at least one chromophore moiety, (b) at least one nitrogen-containing heterocycle, (c) a linking group to link each chromophore moiety to each nitrogen-containing heterocycle; characterised in that at least one nitrogen-containing heterocycle is substituted with at least one thio-derivative and at least one quaternized nitrogen derivative. The reactive dye compounds of the invention high Exhaustion Values, high Fixation Values, particularly on cellulosic substrates such as cotton, and show significant improvements in terms of reducing spent dyestuff in effluent, increasing dye affinity to the substrate, increasing the dye-substrate covalent bonding, increasing the ability to dye substrates at room temperature, decreasing the amount of dye that is removed during the post dyeing "soaping off process" and therefore simplying the post dyeing "soaping off process" traditionally associated with dyeing cotton with fibre reactive dyes and reduction of staining of adjacent white fabrics. In addition, the compounds prepared above provide more intense dyeings and require less levels of salt for dyeing cotton substrates.
摘要翻译：一种活性染料化合物，其包含：（a）至少一个生色团部分，（b）至少一个含氮杂环，（c）将每个发色团部分连接至每个含氮杂环的连接基团; 其特征在于至少一个含氮杂环被至少一个硫代衍生物和至少一个季铵化的氮衍生物取代。本发明的活性染料化合物具有高的耗尽值，高固定值，特别是在诸如棉花等纤维素基材上，并且在减少流出物中的废染染色方面显示出显着的改进，增加了染料与底物共价键的染料亲和力，增加了在室温下染色基质的能力，减少了在后染色“皂洗过程”期间除去的染料的量，因此简单地将传统上与纤维活性染料染色棉相关的后染色“皂洗过程”减少的相邻白色织物的染色。此外，上述制备的化合物提供更强烈的染色，并且需要较少量的盐用于染色棉花基质。

3. 发明申请

WO01025337A1 REACTIVE DYE COMPOUNDS 审中-公开
标题翻译：反应性染料化合物
公开(公告)号：WO01025337A1
公开(公告)日：2001-04-12
申请号：PCT/US2000/026974
申请日：2000-09-29
IPC分类号： A61K8/00 , A61K8/49 , A61K8/55 , A61Q5/10 , C09B62/02 , C09B62/022 , C09B62/04 , C09B62/12 , C09B62/20 , C09B62/28 , C09B67/26 , D06P1/382 , D06P3/10 , D06P3/14 , D06P3/24 , D06P3/32 , D06P3/66 , C09B62/78 , D06P1/38 , D06P3/00
CPC分类号： C09B62/02 , A61K8/4906 , A61K8/4926 , A61K8/494 , A61K8/4953 , A61K8/4966 , A61K8/55 , A61K2800/438 , A61Q5/10
摘要： A reactive dye compound comprising: (a) at least one chromophore moiety; (b) at least one nitrogen-containing heterocycle; (c) a linking group to link each chromophore moiety to each nitrogen-containing heterocycle; characterised in that at least one nitrogen-containing heterocycle is substituted with at least one Y group whrein Y is a phosphonate or a borate derivative. The compounds herein have high Exhaustion Values (E), high Fixation Values (F) and high Efficiency Values (T) and show significant improvements in terms of reducing spent dyestuff in effluent, increasing dye affinity to the substrate, increasing the dye-substrate covalent bonding, increasing the ability to dye substrates at room temperature, decreasing the amount of dye that is removed during the post dyeing "soaping off process" and therefore simplifying the post dyeing "soaping off process" traditionally associated with dyeing cotton with fibre reactive dyes and reduction of staining of adjacent white fabrics. In addition, the compounds prepared above provide more intense dyeings and require less levels of salt for dyeing cotton substrates.
摘要翻译：一种活性染料化合物，包括：（a）至少一个发色团部分; （b）至少一种含氮杂环; （c）将每个发色团部分连接至每个含氮杂环的连接基团; 其特征在于至少一个含氮杂环被至少一个Y基团取代，Y是膦酸酯或硼酸酯衍生物。本文中的化合物具有高的耗尽值（E），高固定值（F）和高效率值（T），并且在减少流出物中的废染料方面显示出显着的改善，增加了对底物的染料亲和力，增加了染料 - 底物共价粘合，增加在室温下染色基质的能力，减少在后染色“皂洗过程”期间除去的染料的量，因此简化了传统上与纤维活性染料染色棉相关的后染色“皂洗过程” 减少相邻白色织物的染色。此外，上述制备的化合物提供更强烈的染色，并且需要较少量的盐用于染色棉花基质。

4. 发明申请

WO00069973A1 REACTIVE DYE COMPOUNDS 审中-公开
标题翻译：反应性染料化合物
公开(公告)号：WO00069973A1
公开(公告)日：2000-11-23
申请号：PCT/US2000/012749
申请日：2000-05-10
IPC分类号： C07D251/16 , A61K8/49 , A61Q5/06 , C07D239/42 , C07D241/44 , C07D251/42 , C07D251/46 , C07D251/48 , C07D251/50 , C07D401/04 , C07D401/14 , C09B43/16 , C09B62/02 , C09B62/085 , C09B62/245 , C09B62/32 , C09B62/80 , C09B62/825 , C09B67/26 , D06P1/38 , D06P1/382 , D06P3/10 , D06P3/14 , D06P3/24 , D06P3/66 , A61K7/13
CPC分类号： C09B62/02 , A61K8/494 , A61K8/4966 , A61K2800/43 , A61K2800/57 , A61Q5/065 , C09B43/16
摘要： A reactive dye compound comprising: (a) at least one chromophore moiety, (b) at least one nitrogen-containing heterocycle, (c) a linking group to link each chromophore moiety to each nitrogen-containing heterocycle; characterised in that at least one nitrogen-containing heterocycle is substituted with at least one oxy- or thio-carbonyl derivative wherein the oxy- or thio-carbonyl derivative is selected from Y wherein Y is -A(CO)R* wherein A is selected from O or S and wherein R* is an organic residue which comprises at least one nucleophilic group, and salts thereof. The compounds herein have high Exhaustion Values (E), high Efficiency Values (T) and show significant improvements in terms of reducing spent dyestuff in effluent, increasing dye affinity to the substrate, increasing the dye-substrate covalent bonding, increasing the ability to dye substrates at room temperature, decreasing the amount of the dye that is removed during the post dyeing "soaping off process" and therefore simplifying the post dyeing "soaping off process" traditionally associated with dyeing cotton with fibre reactive dyes and reduction of staining of adjacent white fabrics. In addition, the compounds prepared above provide more intense dyeings and require less levels of salt for dyeing cotton substrates.
摘要翻译：一种活性染料化合物，包括：（a）至少一个发色团部分，（b）至少一个含氮杂环，（c）将每个发色团部分连接到每个含氮杂环的连接基团; 其特征在于至少一个含氮杂环被至少一个氧基或硫代羰基衍生物取代，其中氧基或硫代羰基衍生物选自Y，其中Y是-A（CO）R *，其中选择A 其中R *是包含至少一个亲核基团的有机残基及其盐。本文的化合物具有高的耗尽值（E），高效率值（T），并且在减少流出物中的废染料方面显示出显着的改进，增加了对基材的染料亲和力，增加染料 - 底物共价键，增加染色能力底物在室温下降低了在后染色“皂洗过程”期间除去的染料的量，因此简化了染色棉纤维活性染料传统上染色后的“洗涤过程”，并减少了相邻白色染色面料。此外，上述制备的化合物提供更强烈的染色，并且需要较少量的盐用于染色棉花基质。

5. 发明申请

WO1999051683A1 REACTIVE DYE COMPOUNDS 审中-公开
标题翻译：反应性染料化合物
公开(公告)号：WO1999051683A1
公开(公告)日：1999-10-14
申请号：PCT/US1998006541
申请日：1998-04-02
申请人： THE PROCTER & GAMBLE COMPANY , BROCK, Earl, David , LEWIS, David, Malcolm , YOUSAF, Taher, Iqbal
发明人： THE PROCTER & GAMBLE COMPANY
IPC分类号： C09B62/02
CPC分类号： C09B62/4401 , C09B62/02 , C09B62/20
摘要： Reactive dye having a Fixation Value (F) on cellulosic substrates of 95 % or greater as measured by the Fixation Value Technical Test Method (at 2:1 standard depth). In addition, the compounds herein have high Exhaustion Values (E), high Efficiency Values (T) and show significant improvements in terms of reducing spent dyestuff in effluent, increasing dye affinity to the substrate, increasing the dye-substrate covalent bonding, increasing the ability to dye substrates at room temperature, decreasing the amount of dye that is removed during the post dyeing "soaping off process" and therefore simplifying the post dyeing "soaping off process" traditionally associated with dyeing cotton with fibre reactive dyes and reduction of staining of adjacent white fabrics. In addition, the compounds prepared above provide more intense dyeings and require less levels of salt for dyeing cotton substrates.
摘要翻译：通过固定值技术测试方法（以2：1标准深度）测量，在纤维素基材上具有95％或更高固定值（F）的活性染料。此外，本文的化合物具有高的耗尽值（E），高效率值（T），并且在减少流出物中的废染料方面显示出显着的改善，增加了对基材的染料亲和力，增加了染料 - 底物共价键，增加了在室温下染色基质的能力，减少在后染色“皂洗过程”中除去的染料的量，因此简化了与纤维活性染料染色棉相关的后染色“皂洗过程”，并减少染色相邻的白色面料。此外，上述制备的化合物提供更强烈的染色，并且需要较少量的盐用于染色棉花基质。

6. 发明申请

WO2009055216A2 METHOD OF PREPARING A MOLECULAR SIEVE COMPOSITION 审中-公开
标题翻译：制备分子筛组合物的方法
公开(公告)号：WO2009055216A2
公开(公告)日：2009-04-30
申请号：PCT/US2008078315
申请日：2008-09-30
申请人： EXXONMOBIL CHEM PATENTS INC , LAI WENYIH F , KAY ROBERT ELLIS
发明人： LAI WENYIH F , KAY ROBERT ELLIS
IPC分类号： C01B39/00 , C01B31/02 , C01B39/20 , C01B39/24 , C01B39/26 , C01B39/36 , C01B39/38 , C01B39/42 , C01B39/44 , C01B39/46 , C01B39/48
CPC分类号： B01J29/80 , B01J29/06 , B01J29/084 , B01J29/18 , B01J29/40 , B01J29/65 , B01J29/7007 , B01J29/7038 , B01J35/002 , B01J35/1019 , B01J35/1023 , B01J37/0018 , B01J2229/62 , B01J2229/64 , C01B39/02 , C01B39/46 , C01B39/48 , C09B62/02 , C10G11/05 , C10G25/03 , C10G29/205 , C10G45/00 , C10G45/54 , C10G45/64 , C10G47/16 , C10G50/00
摘要： This disclosure provides a method of preparing a crystalline molecular sieve comprising: (a) providing a reaction mixture comprising at least one source of ions of tetravalent element Y, at least one source of alkali metal hydroxide, water, optionally at least one seed crystal, and optionally at least one source of ions of trivalent element X, the reaction mixture having the following molar composition: Y:X2 = 2 to infinity, preferably from 15 to 100, OH-: Y = 0.001 to 2, preferably from 0.1 to 1, M+: Y = 0.001 to 2, preferably from 0.01 to 2 wherein M is an alkali metal and the amount of water is at least sufficient to permit extrusion of the reaction mixture, wherein the reaction mixture is substantially free of crystalline molecular sieve; (b) extruding the reaction mixture to form a pre-formed extrudate; and (c) crystallizing the pre-formed extrudate in a liquid medium comprising water under liquid phase crystallization conditions to form a crystallized extrudate having the crystalline molecular sieve.
摘要翻译：本公开提供了一种制备结晶分子筛的方法，包括：（a）提供反应混合物，其包含至少一种四价元素Y的离子源，至少一种碱金属氢氧化物源，水，任选的至少一种晶种，以及任选地至少一种三价元素X的离子源，所述反应混合物具有以下摩尔组成：Y：X2 = 2至无穷大，优选15至100，OH-：Y = 0.001至2，优选0.1至1 ，M +：Y = 0.001-2，优选0.01-2，其中M是碱金属，水的量至少足以使反应混合物挤出，其中反应混合物基本上不含结晶分子筛; （b）挤出反应混合物以形成预形成的挤出物; 和（c）在液相结晶条件下使预成形的挤出物在包含水的液体介质中结晶，以形成具有结晶分子筛的结晶挤出物。

7. 发明申请

WO99051689A1 REACTIVE DYE COMPOUNDS 审中-公开
标题翻译：反应性染料化合物
公开(公告)号：WO99051689A1
公开(公告)日：1999-10-14
申请号：PCT/US1999/007291
申请日：1999-04-01
IPC分类号： A61K8/00 , A61K8/49 , A61Q5/06 , A61Q5/10 , C09B62/02 , C09B62/36 , D06P1/382 , A61K7/13
CPC分类号： C09B62/36 , A61K8/4926 , A61K8/494 , A61K8/4953 , A61Q5/065 , C09B62/02
摘要： This invention relates to reactive dye compounds, and more especially to reactive dye compounds comprising a chromophore and a nitrogen-containing heterocycle comprising at least one thio-substituent. The reactive dye compounds of the present invention are particularly suitable for dyeing hair.
摘要翻译：本发明涉及活性染料化合物，更具体地涉及包含发色团和含有至少一个硫代取代基的含氮杂环的活性染料化合物。本发明的活性染料化合物特别适用于染发。

8. 发明申请

WO1986004080A1 IMPROVEMENTS IN OR RELATING TO ORGANIC COMPOUNDS 审中-公开
标题翻译：有机化合物的改善或有关
公开(公告)号：WO1986004080A1
公开(公告)日：1986-07-17
申请号：PCT/EP1985000745
申请日：1985-12-23
申请人： SANDOZ AG , AUERBACH, Günther , KOCH, Werner , MATZINGER, Peter , STEIGER, Jürg , VON TOBEL, Hans, Rudolf
发明人： SANDOZ AG
IPC分类号： C09B62/002
CPC分类号： C09B62/4413 , C09B62/02
摘要： New water-soluble, fibre-reactive compounds correspond to formula (I) in which the symbols are as defined in Claim 1, provided that a compound of formula (I) contains at least one of the following groups: (a) hydroxy groups, (b) ether groupings, (c) carbonyl groups, (d) carboxy groups, which group(s) is (are) in the compounds of formula (II) and/or in R. These compounds are prepared in conventional manner by condensation of a compound Qa-Hal with an appropriate starting compound containing a primary or secondary amine group. The compounds of formula (I) are suitable as fibre-reactive dyes for dyeing or printing hydroxy group or nitrogen containing organic substrates, especially cotton. The preferred dyeing temperature is in the cold-dyeing range. The dyeings and prints obtained have good general fastness properties and are stable to any oxidative influences.
摘要翻译：新的水溶性纤维反应性化合物对应于式（I），其中符号如权利要求1中所定义，条件是式（I）化合物含有至少一种以下基团：（a）羟基，（b）醚基团，（c）羰基，（d）羧基，这些基团在式（II）和/或R中的化合物中是（即）。这些化合物以常规方式通过缩合的化合物Qa-Hal与具有伯胺或仲胺基团的合适的起始化合物反应。式（I）化合物适用于染色或印刷羟基或含氮有机基质，特别是棉花的纤维活性染料。优选的染色温度为冷染色范围。获得的染色和印花具有良好的一般牢度性能，并且对任何氧化影响都是稳定的。

9. 发明申请

WO01025339A1 REACTIVE DYE COMPOUNDS 审中-公开
标题翻译：反应性染料化合物
公开(公告)号：WO01025339A1
公开(公告)日：2001-04-12
申请号：PCT/US2000/026976
申请日：2000-09-29
IPC分类号： A61K8/00 , A61K8/49 , A61Q5/06 , A61Q5/10 , C09B62/02 , C09B62/022 , C09B62/04 , C09B62/12 , C09B62/20 , D06P1/382 , D06P3/10 , D06P3/14 , D06P3/24 , D06P3/32 , D06P3/66 , C09B62/78 , D06P1/38 , D06P3/00
CPC分类号： C09B62/02 , A61K8/4906 , A61K8/494 , A61K8/4953 , A61K8/4966 , A61K2800/438 , A61Q5/065 , A61Q5/10
摘要： A reactive dye compound comprising: (a) at least one chromophore moiety; (b) at least one nitrogen-containing heterocycle (c) a linking group to link each chromophore moiety to each nitrogen-containing heterocycle; characterised in that at least one nitrogen-containing heterocycle is substituted with at least one Y group wherein Y is derived from a hydrated aldehyde, a hydrated ketone, a hydrated alpha-hydroxy ketone, or the hydrated form of formic acid and linked via one of its oxygen atoms to the nitrogen-containing heterocycle thereby forming a hemiacetal. The compounds herein have high Exhaustion Values (E), high Fixation Values (F) and high Efficiency Values (T) and show significant improvements in terms of reducing spent dyestuff in effluent, increasing dye affinity to the substrate, increasing the dye-substrate covalent bonding, increasing the ability to dye substrates at room temperature, decreasing the amount of dye that is removed during the post dyeing "soaping off process" and therefore simplifying the post dyeing "soaping off process" traditionally associated with dyeing cotton with fibre reactive dyes and reduction of staining of adjacent white fabrics. In addition, the compounds prepared above provide more intense dyeings and require less levels of salt for dyeing cotton substrates.
摘要翻译：一种活性染料化合物，包括：（a）至少一个发色团部分; （b）至少一个含氮杂环（c）将每个发色团部分连接到每个含氮杂环的连接基团; 其特征在于至少一个含氮杂环被至少一个Y基团取代，其中Y源自水合醛，水合酮，水合α-羟基酮或甲酸的水合形式，并通过以下之一其氧原子到含氮杂环，从而形成半缩醛。本文中的化合物具有高的耗尽值（E），高固定值（F）和高效率值（T），并且在减少流出物中的废染料方面显示出显着的改善，增加了对底物的染料亲和力，增加了染料 - 底物共价粘合，增加在室温下染色基质的能力，减少在后染色“皂洗过程”期间除去的染料的量，因此简化了传统上与纤维活性染料染色棉相关的后染色“皂洗过程” 减少相邻白色织物的染色。此外，上述制备的化合物提供更强烈的染色，并且需要较少量的盐用于染色棉花基质。

10. 发明申请

WO99051686A1 REACTIVE DYE COMPOUNDS 审中-公开
标题翻译：反应性染料化合物
公开(公告)号：WO99051686A1
公开(公告)日：1999-10-14
申请号：PCT/US1999/007294
申请日：1999-04-01
IPC分类号： C09B67/00 , C09B62/02 , C09B62/04 , C09B62/20 , C09B62/44 , C09B62/503
CPC分类号： C09B62/4401 , C09B62/02 , C09B62/20
摘要： Reactive dye having a Fixation Value (F) on cellulosic substrates of 95 % or greater as measured by the Fixation Value Technical Test Method (at 2:1 standard depth). In addition, the compounds herein have high Exhaustion Values (E), high Efficiency Values (T) and show significant improvements in terms of reducing spent dyestuff in effluent, increasing dye affinity to the substrate, increasing the dye-substrate covalent bonding, increasing the ability to dye substrates at room temperature, decreasing the amount of dye that is removed during the post dyeing "soaping off process" and therefore simplying the post dyeing "soaping off process" traditionally associated with dyeing cotton with fibre reactive dyes and reduction of staining of adjacent white fabrics. In addition, the compounds prepared above provide more intense dyeings and require less levels of salt for dyeing cotton substrates.
摘要翻译：通过固定值技术测试方法（以2：1标准深度）测量，在纤维素基材上具有95％或更高固定值（F）的活性染料。此外，本文的化合物具有高的耗尽值（E），高效率值（T），并且在减少流出物中的废染料方面显示出显着的改善，增加了对基材的染料亲和力，增加了染料 - 底物共价键，增加了在室温下染色基质的能力，减少在后染色“皂洗过程”期间除去的染料的量，因此简单地将染色棉与纤维活性染料传统上相关的后染色“皂洗过程” 相邻的白色面料。此外，上述制备的化合物提供更强烈的染色，并且需要较少量的盐用于染色棉花基质。

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