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1. 发明申请

WO2019105287A1 一种纳米纤维素及其制备方法和用途审中-公开
公开(公告)号：WO2019105287A1
公开(公告)日：2019-06-06
申请号：PCT/CN2018/117072
申请日：2018-11-23
申请人：济南圣泉集团股份有限公司
发明人：张金柱 , 王鹏辉 , 张安 , 刘顶
IPC分类号： C08B3/00
CPC分类号： C08B3/00 , C08B15/00 , C08B15/02 , C08J3/03 , C08L1/04
摘要：本文涉及一种纳米纤维素的制备方法，所述制备方法包括：（1）向酸酐类化合物的熔融液中加入纤维素原料，升温至熔点以上，进行预处理反应，反应完毕后过滤，得到预处理的纤维素原料；（2）将预处理的纤维素原料分散于水中，得到分散液；（3）将分散液机械粉碎，得到纳米纤维素分散液。本文通过将纤维素原料与酸酐熔融液接触，使酸酐分子进入至基元单元纤维之间，在机械力作用下，剥离得到纳米纤维素，处理过程除了酸酐不加入其他任何有机溶剂，环境污染小，工艺方法简单，能耗低，成本低；本文通过酸酐处理纤维素原料制备得到的纳米纤维素表面富含羧基基团，其具有良好的水分散性和储存稳定性。

2. 发明申请

WO2017058706A1 CELLULOSE ESTER MATERIALS WITH TUNABLE DEGRADATION CHARACTERISTICS 审中-公开
标题翻译：具有可降解特性的纤维素酯材料
公开(公告)号：WO2017058706A1
公开(公告)日：2017-04-06
申请号：PCT/US2016/053689
申请日：2016-09-26
申请人： EASTMAN CHEMICAL COMPANY
发明人： COLLINS, Nick, Allen , FLINT, Kenneth , GHOSH, Koushik , GOODRICH, Jacob, Donald , ISLAM, SM, Bedarul , SEILER, Brian, Douglas , WILSON, Steven, Anthony
IPC分类号： C09K8/035 , C09K8/70 , C08B3/00
CPC分类号： C08L1/12 , C08B3/00 , C08B3/24 , C08L1/10 , C09K8/035 , C09K8/68 , C09K8/70 , C09K8/90 , C09K2208/08 , D01D1/02 , D01D5/04 , D01F2/28
摘要： Degradable materials are provided that may be utilized in various wellbore treatment fluids, such as hydraulic fracturing fluids. In particular, the degradable materials can be formed from cellulose esters that are capable of effectively degrading at specific rates when exposed to the aqueous environments commonly found in wellbores. More particularly, the degradable materials can be in the form of degradable fibers that are formed from the cellulose esters described herein.
摘要翻译：可提供的可降解材料可用于各种井眼处理流体，如水力压裂液。特别地，可降解材料可以由纤维素酯形成，所述纤维素酯当暴露于通常在井眼中发现的含水环境时能够以特定的速率有效地降解。更具体地，可降解材料可以是由本文所述的纤维素酯形成的可降解纤维的形式。

3. 发明申请

WO2013106433A1 CELLULOSE DERIVATIVES FOR INHIBITING CRYSTALLIZATION OF POORLY WATER-SOLUBLE DRUGS 审中-公开
标题翻译：用于抑制不溶性水溶性药物结晶的纤维素衍生物
公开(公告)号：WO2013106433A1
公开(公告)日：2013-07-18
申请号：PCT/US2013/020835
申请日：2013-01-09
申请人： VIRGINIA TECH INTELLECTUAL PROPERTIES, INC. , PERDUE RESEARCH FOUNDATION
发明人： EDGAR, Kevin, J. , LI, Bin , TAYLOR, Lynne , ILEVBARE, Grace , WILLIAMS, Stephanie, M. , LIU, Haoyu
IPC分类号： A61K47/38 , A61K47/30 , A61K9/08 , A61K31/70
CPC分类号： A61K47/38 , A61K9/146 , A61K31/05 , A61K31/352 , A61K31/357 , A61K31/40 , A61K31/427 , A61K31/536 , A61K31/70 , C08B3/00
摘要： The present invention relates to the fields of chemistry and pharmaceuticals. Embodiments of the invention provide cellulose esters useful for inhibiting solution crystallization of drugs. Specific polymers of the invention include cellulose esters of formula (I) : wherein n of the ω-carboxyalkanoyl group, Formula (II), is 3, 4, 6, or 8 to provide a ω-carboxyalkanoyl group chosen from succinoyl, glutaroyl, adipoyl, sebacyl, and suberyl groups; and wherein R is chosen from : a hydrogen atom; and an alkanoyl group chosen from acetyl, propionyl, butyryl, valeroyl, hexanoyl, nonanoyl, decanoyl, lauroyl, palmitoyl, and stearoyl groups; wherein there is a total degree of substitution of the alkanoyl group and the ω-carboxyalkanoyl group of at least 2.0; and wherein the polymer comprises m repeating units where n = 1 to 1,000,000, or 10 to 100,000, or 100 to 1,000, such as 1 to 6,000. Embodiments further include compositions comprising cellulose esters and poorly water-soluble drugs, which compositions exhibit greater solubility and stability in solution as compared to the drugs alone. Drugs that can be used in combination with such polymers include but are not limited to ritonavir, efavirenz, etravirine, celecoxib, clarithromycin, curcumin, ellagic acid, quercetin, naringenin, and resveratrol. Methods for making and using the compounds and compositions are also included within the scope of the invention.
摘要翻译：本发明涉及化学和药物领域。本发明的实施方案提供了可用于抑制药物溶液结晶的纤维素酯。本发明的具体聚合物包括式（I）的纤维素酯：其中式（II）的ω-羧基烷酰基中的n为3,4,6或8，以提供选自琥珀酰基，戊酰基，己二酰基，癸二酰基和辛二酸基; 并且其中R选自：氢原子; 和选自乙酰基，丙酰基，丁酰基，戊酰基，己酰基，壬酰基，癸酰基，月桂酰基，棕榈酰基和硬脂酰基的烷酰基; 其中烷酰基和ω-羧基烷酰基的总取代度为至少2.0; 并且其中所述聚合物包含m个重复单元，其中n = 1至1,000,000，或10至100,000，或100至1,000，如1至6,000。实施方案还包括包含纤维素酯和水溶性差的药物的组合物，与单独的药物相比，该组合物在溶液中表现出更大的溶解度和稳定性。可以与这些聚合物组合使用的药物包括但不限于利托那韦，依法韦仑，依伐维林，塞来昔布，克拉霉素，姜黄素，鞣花酸，槲皮素，柚皮苷和白藜芦醇。制备和使用化合物和组合物的方法也包括在本发明的范围内。

4. 发明申请

WO2010120269A1 CELLULOSE SOLUTIONS COMPRISING TETRAALKYLAMMONIUM ALKYLPHOSPHATE AND PRODUCTS PRODUCED THEREFROM 审中-公开
标题翻译：包含四乙基氨基磺酸镁的纤维素溶液及其生产的产品
公开(公告)号：WO2010120269A1
公开(公告)日：2010-10-21
申请号：PCT/US2009/004626
申请日：2009-08-13
申请人： EASTMAN CHEMICAL COMPANY
发明人： BUCHANAN, Charles, Michael , BUCHANAN, Norma, Lindsey , GUZMAN-MORALES, Elizabeth
IPC分类号： C08B1/00 , C08B3/06 , C08B3/16 , C08J5/18
CPC分类号： C08B3/16 , C08B1/003 , C08B3/00 , C08B3/04 , C08B3/06 , C08B3/08 , C08B3/10 , G02B1/105 , G02B1/14 , G02B5/32 , Y10T428/13
摘要： This invention relates a cellulose solution comprising cellulose and at least one tetraalkylammonium alkylphosphate and processes to produce the cellulose solution. Another aspect of this invention relates to shaped articles prepared from a cellulose solution comprising cellulose and at least one tetraalkylammonium alkylphosphate. Another embodiment of this invention relates to compositions comprising derivatives of cellulose prepared from a cellulose solution comprising at least one tetraalkylammonium alkylphosphate. Another embodiment of this invention relates to compositions comprising regioselectively substituted cellulose esters prepared from a cellulose solution comprising cellulose and at least one tetraalkylammonium alkylphosphate. In another embodiment of the invention, the cellulose esters of the present invention are used as protective and compensation films for liquid crystalline displays.
摘要翻译：本发明涉及包含纤维素和至少一种烷基磷酸烷基铵的纤维素溶液，并且生产纤维素溶液的方法。本发明的另一方面涉及由包含纤维素和至少一种烷基磷酸烷基铵的纤维素溶液制备的成型制品。本发明的另一个实施方案涉及包含由包含至少一种烷基磷酸烷基铵的纤维素溶液制备的纤维素衍生物的组合物。本发明的另一个实施方案涉及由包含纤维素和至少一种烷基磷酸烷基铵的纤维素溶液制备的区域选择性取代的纤维素酯的组合物。在本发明的另一个实施方案中，本发明的纤维素酯用作液晶显示器的保护膜和补偿膜。

5. 发明申请

WO2009102306A1 CELLULOSE ESTERS AND THEIR PRODUCTION IN HALOGENATED IONIC LIQUIDS 审中-公开
标题翻译：纤维素酯及其在卤代离子液体中的生产
公开(公告)号：WO2009102306A1
公开(公告)日：2009-08-20
申请号：PCT/US2008/009624
申请日：2008-08-12
申请人： EASTMAN CHEMICAL COMPANY
发明人： BUCHANAN, Charles, Michael , BUCHANAN, Norma, Lindsey
IPC分类号： C08B3/00 , C08B1/00
CPC分类号： C08B1/003 , C08B3/00 , C08B3/06 , C08B3/16 , C08B3/18
摘要： Ionic liquids and cellulose ester compositions and processes for producing ionic liquids and cellulose esters. Cellulose esters can be produced by esterifying cellulose in a reaction medium comprising one or more halide ionic liquids and at least one binary component. Cellulose esters prepared via the methods of the present invention can have a degree of substitution ('DS') of at least 1.5 and can comprise a plurality of ester substituents, where at least 50 percent of the ester substituents comprise alkyl esters having a carbon chain length of at least 6 carbons.
摘要翻译：离子液体和纤维素酯组合物和用于生产离子液体和纤维素酯的方法。纤维素酯可以通过在包含一种或多种卤离子液体和至少一种二元组分的反应介质中酯化纤维素来制备。通过本发明的方法制备的纤维素酯可以具有至少1.5的取代度（'DS'），并且可以包含多个酯取代基，其中至少50％的酯取代基包括具有碳链的烷基酯长度至少为6个碳。

6. 发明申请

WO2008100566A1 CELLULOSE ESTERS AND THEIR PRODUCTION IN CARBOXYLATED IONIC LIQUIDS 审中-公开
标题翻译：纤维素酯及其在羧基离子液体中的生产
公开(公告)号：WO2008100566A1
公开(公告)日：2008-08-21
申请号：PCT/US2008/001952
申请日：2008-02-14
申请人： EASTMAN CHEMICAL COMPANY
发明人： BUCHANAN, Charles, Michael , BUCHANAN, Norma, Lindsey , HEMBRE, Robert, Thomas , LAMBERT, Juanelle, Little
IPC分类号： C08B1/00 , C08B3/06 , C08B3/08 , C08B3/10 , C08B3/16 , C08B3/18
CPC分类号： C07D233/54 , C08B1/003 , C08B3/00 , C08B3/06 , C08B3/08 , C08B3/10 , C08B3/16 , C08B3/18 , Y02P20/542
摘要： Ionic liquids and cellulose ester compositions and processes and apparatus for producing ionic liquids and cellulose esters. Cellulose esters can be produced by dissolving cellulose in carboxylated ionic liquids and thereafter contacting the cellulose solution with at least one acylating reagent. Cellulose esters produced via the present invention can comprise ester groups that originate from the carboxylated ionic liquid and/or the acylating reagent.
摘要翻译：离子液体和纤维素酯组合物和用于生产离子液体和纤维素酯的方法和设备。纤维素酯可以通过将纤维素溶解在羧化离子液体中，然后使纤维素溶液与至少一种酰化剂接触来制备。通过本发明生产的纤维素酯可以包含源自羧化离子液体和/或酰化试剂的酯基。

7. 发明申请

WO2008036452A2 A METHOD OF MAKING CELLULOSE ESTER POLYMER AND PRE-TREATING CELLULOSE FOR THE MANUFACTURE OF CELLULOSE ESTER POLYMER 审中-公开
标题翻译：制备纤维素酯聚合物和预处理纤维素制备纤维素酯聚合物的方法
公开(公告)号：WO2008036452A2
公开(公告)日：2008-03-27
申请号：PCT/US2007/073006
申请日：2007-07-09
申请人： CELANESE ACETATE LLC
发明人： WANG, Linfu , KIZER, Lawton, E. , SAMZ, Frederick, C. , STOGNER, Henry, P. , TONEY II, Charles, E.
IPC分类号： C08B3/00
CPC分类号： C08B1/02 , C08B3/00 , C08B3/06
摘要： A method of making cellulose ester polymer comprises the steps of : pre- treating a cellulose source; esterifying the pretreated cellulose source to form a cellulose ester; and optionally hydrolyzing the cellulose ester. The pretreatment step further comprises: mixing, in a first stage, the cellulose source with a first solution of a weak acid and water, whereby the cellulose source being suspended in the first solution; de-liquefying the first stage suspension; mixing, in a second stage, the de-liquefied mass with a second solution of weak acid and water, whereby the mass being suspended in the second solution; and de-liquefying the second stage suspension.
摘要翻译：制备纤维素酯聚合物的方法包括以下步骤：预处理纤维素源; 酯化预处理的纤维素源以形成纤维素酯; 并任选地水解纤维素酯。预处理步骤还包括：在第一阶段中将纤维素源与弱酸和水的第一溶液混合，由此将纤维素源悬浮在第一溶液中; 去液化第一级悬浮液; 在第二阶段中将所述脱液体与弱酸和水的第二溶液混合，由此所述物质悬浮在所述第二溶液中; 并使第二级悬浮液脱液化。

8. 发明申请

WO2007144282A1 VERFAHREN ZUR ACYLIERUNG VON CELLULOSE 审中-公开
标题翻译：方法酰化纤维素
公开(公告)号：WO2007144282A1
公开(公告)日：2007-12-21
申请号：PCT/EP2007/055445
申请日：2007-06-04
申请人： BASF AKTIENGESELLSCHAFT , STEGMANN, Veit , MASSONNE, Klemens , D'ANDOLA, Giovanni , MORMANN, Werner , WEZSTEIN, Markus , LENG, Wei
发明人： STEGMANN, Veit , MASSONNE, Klemens , D'ANDOLA, Giovanni , MORMANN, Werner , WEZSTEIN, Markus , LENG, Wei
IPC分类号： C08B1/00 , C08B3/06 , C08B3/00
CPC分类号： C08B1/003 , C08B3/00 , C08B3/06
摘要： Die vorliegende Erfindung beschreibt ein Verfahren zur Acylierung von Poly-, Oligo- oder Disacchariden, oder Derivaten hiervon, indem man diese in einer ionischen Flüssigkeit löst und mit einem Keten umsetzt, sowie neue acylierte Poly-, Oligo- oder Disacchariden, oder Derivaten hiervon.
摘要翻译：本发明描述了一种用于聚酰化，低聚 - 或二糖，或它们的衍生物，通过在离子液体中溶解它们，并用烯酮，以及新的酰化聚反应，低聚 - 或二糖，或其衍生物。

9. 发明申请

WO2007136472A1 USE OF SPECIAL SCREENS IN THE PREPARATION OF CELLULOSE POWDER 审中-公开
标题翻译：在制备纤维素粉末时使用特殊筛选
公开(公告)号：WO2007136472A1
公开(公告)日：2007-11-29
申请号：PCT/US2007/009070
申请日：2007-04-12
申请人： DOW GLOBAL TECHNOLOGIES INC. , BEER, Wolfgang , SCHNEIDER, Hans-peter , MERZ, Gunnar, R. , KRUSE, Peter
发明人： BEER, Wolfgang , SCHNEIDER, Hans-peter , MERZ, Gunnar, R. , KRUSE, Peter
IPC分类号： C08B1/00 , C08J3/12 , C08B3/00 , C08B5/00 , C08B7/00 , C08B9/00 , C08B11/00 , C08B13/00 , C08B15/00
CPC分类号： C08B1/00 , C08B3/00 , C08B5/00 , C08B7/00 , C08B9/00 , C08B11/00 , C08B13/00 , C08B15/00
摘要： The present invention refers to the use of screens comprising at least two layers of different mesh or pore size in a cellulose powder preparation method as well as to said method, wherein grinding the cellulose pulp and sieving the obtained particles can be carried out on-line.
摘要翻译：本发明涉及在纤维素粉末制备方法中使用包含不同网孔或孔径的至少两层的筛网以及所述方法，其中研磨纤维素纸浆并筛分所得颗粒可以在线进行。

10. 发明申请

WO2005041986A3 USE OF BIOCOMPATIBLE POLYMERS FOR THE PREPARATION OF A COMPOSITION OR A MEDICAL DEVICE 审中-公开
标题翻译：用于制备组合物或医疗设备的生物易燃聚合物的使用
公开(公告)号：WO2005041986A3
公开(公告)日：2006-04-20
申请号：PCT/FR2004002780
申请日：2004-10-28
申请人： OTR3 ORGANES TISSUS REGENERATI , BARRITAULT DENIS , BARBIER-CHASSEFIERE VERONIQUE
发明人： BARRITAULT DENIS , BARBIER-CHASSEFIERE VERONIQUE
IPC分类号： A61K31/737 , A61K31/795 , A61K47/36 , A61K47/42 , A61P17/02 , A61P29/00
CPC分类号： C08B3/00 , A61K8/73 , A61K8/731 , A61K8/85 , A61K31/737 , A61K31/795 , A61Q19/00 , A61Q19/02 , C08B37/0009 , C08B37/0021 , C08G63/06
摘要： The invention relates to a biocompatible polymer having general formula (I) AaXxYy, wherein: A denotes a monomer; X denotes an RCOOR' group; Y denotes an O or N-sulphonate group which is fixed to A and which has either formula -ROS03R' or -RNS03R' in which R denotes an optionally branched and/or unsaturated aliphatic hydrocarbon chain which can contain one or more aromatic rings and R' denotes a hydrogen atom or a cation; a denotes the number of monomers; x denotes the rate of substitution of the A monomers by the X groups; and y denotes the rate of substitution of the A monomers by the Y groups. More specifically, the invention relates to the use of said biocompatible polymers for the preparation of a pharmaceutical, dermatological or cosmetic composition or a medical device, which are intended to prevent, relieve and/or treat discomfort, distress, itches, irritations and/or pain and/or to protect tissues against same. In addition, in certain cases, the use of said biocompatible polymers for pain treatment can impact on the actual curing of certain diseases. Significant improvements and even cures have been observed in relation to chronic and painful diseases that are associated with alterations in the extracellular matrix regardless of the origin thereof.
摘要翻译：本发明涉及具有通式（I）A a X x Y y的生物相容性聚合物，其中：A表示单体; X表示RCOOR'基团; Y表示固定在A上并具有式-ROS03R'或-RNS03R'的O或N-磺酸盐基团，其中R表示可含有一个或多个芳环的任选支链和/或不饱和脂族烃链，R '表示氢原子或阳离子; a表示单体数目; x表示X单体的A单体的取代率; y表示Y单体由Y基取代的比例。更具体地，本发明涉及所述生物相容性聚合物用于制备药物，皮肤病学或化妆品组合物或医疗装置的用途，其旨在防止，缓解和/或治疗不适，痛苦，瘙痒，刺激和/或疼痛和/或保护组织免受同样的影响。此外，在某些情况下，使用所述生物相容性聚合物进行疼痛治疗可能会影响某些疾病的实际固化。对于与细胞外基质的改变相关的慢性和疼痛性疾病，观察到显着的改善甚至治愈，不管其来源如何。

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