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1. 发明申请

WO2004076408A3 PROCESS 审中-公开
标题翻译：处理
公开(公告)号：WO2004076408A3
公开(公告)日：2005-03-10
申请号：PCT/EP2004050208
申请日：2004-02-26
申请人： SHELL INT RESEARCH , FOONG WAN SHI , JUNE RAYMOND LAWRENCE
发明人： FOONG WAN SHI , JUNE RAYMOND LAWRENCE
IPC分类号： C07C409/08 , C07D301/19 , C07C407/00
CPC分类号： C07D301/19 , C07C407/00 , C07C407/003 , C07C409/08
摘要： Process for preparing organic hydroperoxides, which process comprises (a) oxidation of an organic compound to obtain reaction product containing organic hydroperoxide, (b) treating at least part of the organic hydroperoxide containing reaction product with a basic aqueous solution and separating hydrocarbonaceous phase containing organic hydroperoxide from basic aqueous phase, (c) washing with water at least part of the separated hydrocarbonaceous phase containing organic hydroperoxide and separating hydrocarbonaceous phase containing organic hydroperoxide from aqueous phase, and (d) optionally repeating step (c) one or more times, in which process solid particles are removed from the reaction product containing organic hydroperoxide and/or basic aqueous solution before use in step (b), preferably by filtering, and a process for preparing oxirane compounds in which such organic hydroperoxide is used.
摘要翻译：制备有机氢过氧化物的方法，该方法包括（a）有机化合物的氧化以获得含有机氢过氧化物的反应产物，（b）用碱性水溶液处理至少部分含有机氢过氧化物的反应产物并分离含有机物的含有机物（c）用水洗涤含有有机氢过氧化物的至少部分分离的含烃相，并从水相中分离含烃有机氢过氧化物，和（d）任选地重复步骤（c）一次或多次，在该方法优选通过过滤将步骤（b）中使用前的固体颗粒从包含有机氢过氧化物和/或碱性水溶液的反应产物中除去，以及制备其中使用这种有机氢过氧化物的环氧乙烷化合物的方法。

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