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    • 10. 发明申请
    • METHOD OF PRODUCING MAGNESIUM ALUMINATE SPINELS
    • 生产铝镁合金钢丝的方法
    • WO2016122838A1
    • 2016-08-04
    • PCT/US2016/012112
    • 2016-01-05
    • SASOL (USA) CORPORATION
    • PEOPLES, Brian, C.HANN, Allison, L.
    • C01F7/16
    • C01F7/162C01P2002/32C01P2006/12C01P2006/14
    • The invention provides for a method of making a magnesium aluminate spinel including an alumina compound and a magnesium compound, the method including the steps of; dispersing the alumina compound by dispersing it in a aqueous solution, to form an alumina dispersion, the aqueous solution having a pH of between 2 and 5; preferably between 2 and 4, flocculating the alumina by increasing the pH of the alumina dispersion to a pH of between 8 and 10 by adding a base; adding the alumina dispersion to an aqueous dispersion of the magnesium compound to form a slurry; drying the slurry to produce a dried spinel precursor; and calcining the dried spinel precursor to produce the magnesium aluminate spinel. Dispersing at such a low pH results in a conversion to spinel as well as allows for the control of the surface area of the spinel.
    • 本发明提供一种制备包括氧化铝化合物和镁化合物的铝酸镁尖晶石的方法,所述方法包括以下步骤: 通过将氧化铝分散在水溶液中来分散氧化铝化合物,形成氧化铝分散体,该水溶液的pH为2至5; 优选2至4之间,通过添加碱将氧化铝分散体的pH增加至8至10的pH来使矾土絮凝; 将氧化铝分散体加入到镁化合物的水分散体中以形成浆料; 干燥浆料以产生干燥的尖晶石前体; 并煅烧干燥的尖晶石前体以产生铝酸镁尖晶石。 在如此低的pH下分散导致转化为尖晶石以及允许控制尖晶石的表面积。