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    • 1. 发明申请
    • CIRCULARLY POLARIZED LIGHT METHOD AND DEVICE FOR DETERMINING WALL THICKNESS AND ORIENTATIONS OF FIBRILS OF CELLULOSIC FIBRES
    • 圆形极化光学方法和装置,用于确定壁厚度和纤维状纤维纤维的方向
    • WO2005054825A1
    • 2005-06-16
    • PCT/CA2004/002033
    • 2004-11-25
    • PULP AND PAPER RESEACH INSTITUTE OF CANADAJANG, Ho Fan
    • JANG, Ho Fan
    • G01N21/23
    • G01N21/23G01B11/0641G01B11/26G01N33/46G01N2021/216G01N2021/8681
    • This invention provides a novel, rapid method and device for determining the relative phase retardation of a multi-layered specimen, which is related to the thicknesses of its layers and walls, and the orientations of its optical axes. An intact wood pulp fibre is a typical multi-layered birefringent specimen. This new method is based on the change of polarization of polarized light that passes through a specimen composed of birefringent layers with different optical axis orientations, such as directions of cellulosic microfibrils oriented differently in various layers of wood fibres. In particular, a novel solution is found to relate the emerging light intensity from an intact wood fibre to the incident light intensity, the wavelength of the light, and the relative phase retardations of various layers and orientations of their cellulosic microfibrils, such as fibril angle, in a circular polarized light system. This new method evaluates the transmitted light intensities of multiple predetermined wavelengths simultaneously to determine the optical and physical properties of a multi-layered specimen being measured. A device for determining the relative phase retardation (retardance) of fibre walls and the fibril angle of intact wood fibres in accordance with the presented invention comprises a light source with well defined multi-wavelengths, an achromatic circular polarized light system, appropriate imaging optics, a multi-channel camera such as a digital color camera that has two or more wavelength (color) detection channels, and an image processing and data analysis system. The measurements take advantage of the birefringence of cellulosic microfibrils, and thus require neither sample preparation nor high resolution optics. Specimen alignment is not required as specimens such as wood fibres are evaluated under circularly polarized light. Compared with other methods, this invention is more rapid, accurate, and robust. This method can be automated, and implemented in a fibre flow-through system, thus allowing a rapid assessment of wood pulp fibre properties (on-line in real time).
    • 本发明提供了一种用于确定多层样品的相对相位延迟的新型快速方法和装置,其与其层和壁的厚度及其光轴的取向有关。 完整的木浆纤维是典型的多层双折射样品。 这种新方法基于通过由具有不同光轴取向的双折射层构成的试样的偏振光的偏振变化,例如在各种木纤维层中取向不同的纤维素微原纤维的方向。 特别地,发现一种新颖的解决方案将来自完整木纤维的出现的光强度与入射光强度,光的波长以及它们的纤维素微原纤的各种层和取向的相对相位延迟相关联,例如原纤维角 ,在圆偏振光系统中。 该新方法同时评估多个预定波长的透射光强度,以确定所测量的多层样品的光学和物理性质。 根据本发明的用于确定纤维壁的相对相位延迟(延迟)和完整木纤维的原纤维角的装置包括具有明确定义的多波长的光源,消色差圆偏振光系统,适当的成像光学器件, 诸如具有两个或更多个波长(彩色)检测通道的数字彩色相机的多通道相机,以及图像处理和数据分析系统。 测量利用纤维素微原纤维的双折射,因此既不需要样品制备也不需要高分辨率光学元件。 在圆偏振光下评估木纤维等样品,不需要样品校准。 与其他方法相比,本发明更加快速,准确,稳健。 该方法可以自动化,并在纤维流通系统中实现,从而可以快速评估木浆纤维的性能(实时在线)。