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1. 发明申请

WO1995006075A1 ALLYL-EPOXY IPN 审中-公开
公开(公告)号：WO1995006075A1
公开(公告)日：1995-03-02
申请号：PCT/EP1994002664
申请日：1994-08-10
申请人： AKZO NOBEL N.V. , SCHUTYSER, Jan, André, Jozef , BUSER, Antonius, Johannes, Wilhelmus
发明人： AKZO NOBEL N.V.
IPC分类号： C08F283/10
CPC分类号： B32B15/08 , B32B27/38 , B32B2307/3065 , B32B2363/00 , B32B2457/08 , C08F283/10 , H05K1/0326 , C08F226/06
摘要： The invention pertains to an interpenetrating polymer network (IPN) composed of (1) epoxy network forming compounds comprising: (a) polyfunctional epoxy compounds (epoxy resin); (b) polyfunctional aromatic hydroxyl compounds; (2) allyl network forming compounds; in which the (1):(2) weight ratio is in the range of 95:5 to 40:60, and the epoxy network forming compounds (1a) and (1b) are in a non-stoichiometric ratio to each other, such that the percentage of stoichiometry is in the range of 10 to 80 %. The percentage of stoichiometry is defined as 100 % times the quotient of the number of hydroxyl equivalents and the number of epoxy equivalents, i.e., eq. OH/eq. epoxy x 100 %. Such IPNs are especially suitable for use in the electronics industry and exhibit a favourable, high Tg and a low TCE. This also applies in the case of comparatively high percentages of epoxy resin giving optimum peel strength. The epoxy resin preferably is based on the diglycidyl ether of Bisphenol-A, while the allyl compound is triallyl cyanurate (TAC) or triallyl isocyanurate (TAIC).
摘要翻译：本发明涉及由（1）环氧网络形成化合物组成的互穿聚合物网络（IPN），包括：（a）多官能环氧化合物（环氧树脂）; （b）多官能芳族羟基化合物; （2）烯丙基网络形成化合物; 其中（1）：（2）重量比在95:5至40:60的范围内，环氧网络形成化合物（1a）和（1b）彼此之间的非化学计量比，化学计量的百分比在10至80％的范围内。化学计量的百分数定义为羟基当量数和环氧当量数的商数的100％，即eq。 OH / EQ。环氧树脂×100％。这样的IPN尤其适用于电子工业，并具有良好的高Tg和低TCE。这也适用于相对较高百分比的赋予最佳剥离强度的环氧树脂的情况。环氧树脂优选基于双酚A的二缩水甘油醚，烯丙基化合物是三烯丙基氰尿酸酯（TAC）或三烯丙基异氰脲酸酯（TAIC）。

2. 发明申请

WO2011124665A1 CROSSLINKABLE COMPOSITION CROSSLINKABLE WITH A LATENT BASE CATALYST 审中-公开
标题翻译：可交联的组合物可与最新的碱性催化剂交联
公开(公告)号：WO2011124665A1
公开(公告)日：2011-10-13
申请号：PCT/EP2011/055465
申请日：2011-04-07
申请人： NUPLEX RESINS B.V. , BRINKHUIS, Richard, Hendrikus, Gerrit , SCHUTYSER, Jan, Andre, Jozef , DOLPHIJN, Paulus, Jozef , BUSER, Antonius, Johannes, Wilhelmus , ELFRINK, Petrus, Johannes, Maria, David , GESSNER, Michael, Anthony , SHALATI, Mohamad, Deeb
发明人： BRINKHUIS, Richard, Hendrikus, Gerrit , SCHUTYSER, Jan, Andre, Jozef , DOLPHIJN, Paulus, Jozef , BUSER, Antonius, Johannes, Wilhelmus , ELFRINK, Petrus, Johannes, Maria, David , GESSNER, Michael, Anthony , SHALATI, Mohamad, Deeb
IPC分类号： C08J3/24
CPC分类号： C08G63/916 , C08K5/098 , C09D167/02
摘要： The present invention relates to a crosslinkable composition comprising at least one crosslinkable component crosslinkable by a latent base crosslinking catalyst comprising a substituted carbonate salt according to formula 1 wherein X + represents a cation and wherein R is hydrogen, alkyl, aryl or aralkyl group, and wherein the crosslinkable composition comprises 0.1 – 10 wt%, preferably 0.1-5, more preferably 0.2-3 and most preferably 0.5-1.5 wt% water (relative to total weight of the crosslinkable composition). The invention further relates to a coating composition comprising the crosslinkable composition according to the invention, a novel catalyst composition and to the use of said catalyst composition according to the invention as a latent base crosslinking catalyst in coating compositions, preferably in RMA crosslinkable compositions.
摘要翻译：本发明涉及一种可交联组合物，其包含至少一种可通过潜碱交联催化剂交联的可交联组分，其包含根据式1的取代的碳酸盐，其中X +表示阳离子，其中R是氢，烷基，芳基或芳烷基，其中可交联组合物包含0.1-10重量％，优选0.1-5，更优选0.2-3，最优选0.5-1.5重量％的水（相对于可交联组合物的总重量）。本发明还涉及一种涂料组合物，其包含根据本发明的可交联组合物，新型催化剂组合物以及根据本发明的所述催化剂组合物在涂料组合物中优选在RMA可交联组合物中作为潜碱交联催化剂的用途。

3. 发明申请

WO2011124664A1 CROSSLINKABLE COMPOSITION CROSSLINKABLE WITH A LATENT BASE CATALYST 审中-公开
标题翻译：可交联的组合物可与最新的碱性催化剂交联
公开(公告)号：WO2011124664A1
公开(公告)日：2011-10-13
申请号：PCT/EP2011/055464
申请日：2011-04-07
申请人： NUPLEX RESINS B.V. , BRINKHUIS, Richard Hendrikus Gerrit , SCHUTYSER, Jan Andre Jozef , DOLPHIJN, Paulus Jozef , BUSER, Antonius Johannes Wilhelmus , ELFRINK, Petrus Johannes Maria David , GESSNER, Michael Anthony , SHALATI, Mohamad Deeb
发明人： BRINKHUIS, Richard Hendrikus Gerrit , SCHUTYSER, Jan Andre Jozef , DOLPHIJN, Paulus Jozef , BUSER, Antonius Johannes Wilhelmus , ELFRINK, Petrus Johannes Maria David , GESSNER, Michael Anthony , SHALATI, Mohamad Deeb
IPC分类号： C08J3/24
CPC分类号： C08G63/916 , C08K5/098 , C09D167/02
摘要： The present invention relates to a crosslinkable composition comprising at least one crosslinkable component and a latent base crosslinking catalyst, which crosslinkable composition has a solids content of typically at least 55 wt (dry weight after crosslinking relative to the total weight of the crosslinking composition) wherein the latent base catalyst is a substituted carbonate salt according to formula (I) wherein X + represents a non acidic cation, preferably a quaternary ammonium or phosphonium, and wherein R is hydrogen, alkyl, aryl or aralkyl group. The invention relates in particular to a composition crosslinkable by Real Michael Addition (RMA) reaction wherein a component with at least 2 activated unsaturated groups and a malonate component with at least 2 acidic protons C-H in activated methylene or methine groups react and crosslink to each other in the presence of the base catalyst. The invention further relates to a coating composition comprising the crosslinkable composition according to the invention, a novel catalyst composition and to the use of said catalyst composition according to the invention as a latent base crosslinking catalyst in coating compositions, preferably in RMA crosslinkable compositions of the base catalyst. The invention further relates to a coating composition comprising the crosslinkable composition according to the invention, a novel catalyst composition and to the use of said catalyst composition according to the invention as a latent base crosslinking catalyst in coating compositions, preferably in RMA crosslinkable compositions.
摘要翻译：本发明涉及包含至少一种可交联组分和潜碱交联催化剂的可交联组合物，该可交联组合物的固体含量通常至少为55重量％（交联后的干重相对于交联组合物的总重量），其中潜在碱催化剂是根据式（I）的取代的碳酸盐，其中X +表示非酸性阳离子，优选季铵或鏻，并且其中R是氢，烷基，芳基或芳烷基。本发明特别涉及通过实际迈克尔加成（RMA）反应可交联的组合物，其中具有至少2个活化不饱和基团的组分和具有活化亚甲基或次甲基中的至少2个酸性质子CH的丙二酸酯组分彼此反应和交联在碱催化剂的存在下。本发明还涉及一种涂料组合物，其包含根据本发明的可交联组合物，新型催化剂组合物以及根据本发明的所述催化剂组合物在涂料组合物中作为潜碱交联催化剂的用途，优选在RMA可交联组合物中碱催化剂。本发明还涉及一种涂料组合物，其包含根据本发明的可交联组合物，新型催化剂组合物以及根据本发明的所述催化剂组合物在涂料组合物中优选在RMA可交联组合物中作为潜碱交联催化剂的用途。

4. 发明申请

WO2011124663A1 CROSSLINKABLE COMPOSITION CROSSLINKABLE WITH A LATENT BASE CATALYST 审中-公开
标题翻译：可交联的组合物可与最新的碱性催化剂交联
公开(公告)号：WO2011124663A1
公开(公告)日：2011-10-13
申请号：PCT/EP2011/055463
申请日：2011-04-07
申请人： NUPLEX RESINS B.V. , BRINKHUIS, Richard, Hendrikus, Gerrit , SCHUTYSER, Jan, Andre, Jozef , DOLPHIJN, Paulus, Jozef , BUSER, Antonius, Johannes, Wilhelmus , ELFRINK, Petrus, Johannes, Maria, David , GESSNER, Michael, Anthony , SHALATI, Mohamad, Deeb
发明人： BRINKHUIS, Richard, Hendrikus, Gerrit , SCHUTYSER, Jan, Andre, Jozef , DOLPHIJN, Paulus, Jozef , BUSER, Antonius, Johannes, Wilhelmus , ELFRINK, Petrus, Johannes, Maria, David , GESSNER, Michael, Anthony , SHALATI, Mohamad, Deeb
IPC分类号： C08J3/24
CPC分类号： C08G63/916 , C08K5/098 , C09D167/02
摘要： The present invention relates to a crosslinkable composition comprising at least one crosslinkable component and a latent base crosslinking catalyst, which crosslinkable composition has a solids content of typically at least 55 wt (dry weight after crosslinking relative to the total weight of the crosslinking composition) wherein the latent base catalyst is a substituted carbonate salt according to formula (I) wherein X + represents a non acidic cation, preferably a quaternary ammonium or phosphonium, and wherein R is hydrogen, alkyl, aryl or aralkyl group. The invention relates in particular to a composition crosslinkable by Real Michael Addition (RMA) reaction wherein a component with at least 2 activated unsaturated groups and a component with at least 2 acidic protons C-H in activated methylene or methine groups, preferably malonate react and crosslink to each other in the presence of the base catalyst. The invention further relates to a coating composition comprising the crosslinkable composition according to the invention, a novel catalyst composition and to the use of said catalyst composition according to the invention as a latent base crosslinking catalyst in coating compositions, preferably in RMA crosslinkable compositions.
摘要翻译：本发明涉及包含至少一种可交联组分和潜碱交联催化剂的可交联组合物，该可交联组合物的固体含量通常至少为55重量％（交联后的干重相对于交联组合物的总重量），其中潜在碱催化剂是根据式（I）的取代的碳酸盐，其中X +表示非酸性阳离子，优选季铵或鏻，并且其中R是氢，烷基，芳基或芳烷基。本发明特别涉及通过实际迈克尔加成（RMA）反应可交联的组合物，其中具有至少2个活化的不饱和基团的组分和在活化的亚甲基或次甲基中具有至少2个酸性质子CH的组分，优选丙二酸酯反应并与在碱催化剂的存在下彼此。本发明还涉及一种涂料组合物，其包含根据本发明的可交联组合物，新型催化剂组合物以及根据本发明的所述催化剂组合物在涂料组合物中优选在RMA可交联组合物中作为潜碱交联催化剂的用途。

5. 发明申请

WO1993011176A1 PHOSPOROUS CONTAINING RESIN 审中-公开
标题翻译：含PHOSPOROUS的树脂
公开(公告)号：WO1993011176A1
公开(公告)日：1993-06-10
申请号：PCT/EP1992002705
申请日：1992-11-24
申请人： AKZO N.V. , SCHUTYSER, Jan, André, Jozef , BUSER, Antonius, Johannes, Wilhelmus , STEENBERGEN, André
发明人： AKZO N.V.
IPC分类号： C08F283/10
CPC分类号： C08G59/304 , C08F283/10 , H05K1/0373 , Y10S428/901 , Y10S525/903 , Y10T428/31518
摘要： Resin composed of an interpenetrating network (IPN) into which an organic phosphorous compound is incorporated. The IPN is composed of an allyl polymer network and an epoxy resin network. More particularly, a chemically incorporated phosphorus compound is present in at least one of the networks. Such an IPN can be produced by replacing at least one of the ingredients of an IPN-forming reaction mixture known in itself wholly or in part with an organic phosphorus compound which has at least one functional group reactive towards at least one of the other ingredients.
摘要翻译：由掺入有机磷化合物的互穿网络（IPN）构成的树脂。 IPN由烯丙聚合物网络和环氧树脂网络组成。更具体地，在至少一个网络中存在化学掺入的磷化合物。这样的IPN可以通过将本身完全或部分已知的具有至少一个官能团的有机磷化合物本身已知的至少一种本身已知的IPN形成反应混合物的成分替代至少一种其它成分来制备。

6. 发明申请

WO1998007731A1 ADDUCT OF AN EPOXY COMPOUND AND CYCLIC PHOSPHITE 审中-公开
标题翻译：环氧化合物和环磷酸盐的添加
公开(公告)号：WO1998007731A1
公开(公告)日：1998-02-26
申请号：PCT/EP1997004406
申请日：1997-08-06
申请人： AKZO NOBEL N.V. , BUSER, Antonius, Johannes, Wilhelmus , SCHUTYSER, Jan, André, Josef
发明人： AKZO NOBEL N.V.
IPC分类号： C07F09/6571
CPC分类号： C07F9/657136 , C07F9/657118 , C07F9/657181 , C08G59/1488 , C08G59/304
摘要： The invention pertains to an adduct comprising epoxy groups obtainable by condensation of an epoxy compound and at least a monocyclic phosphite according to Formula (1), wherein R1 and R2 may be the same or different and represent H or C1-4 alkyl and m is 1, optionally, in admixture with a bicyclic phosphite according to Formula (1) wherein R1 and R2 are absent, m is 2, and wherein R3-R6 may be the same or different and represent H or C1-4 alkyl.
摘要翻译：本发明涉及包含环氧基团的加合物，其可通过环氧化合物和至少一种式（1）的单环亚磷酸酯缩合获得，其中R 1和R 2可以相同或不同，表示H或C 1-4烷基，m是 1，任选地，与根据式（1）的双环亚磷酸酯的混合物，其中R 1和R 2不存在，m为2，并且其中R 3 -R 6可以相同或不同，表示H或C 1-4烷基。

7. 发明申请

WO1997011105A1 EPOXY RESIN COMPOSITION FOR ELECTROLAMINATES HAVING ARYL SUBSTITUTED GUANIDINE AND/OR BIGUANIDE AS CROSS-LINKING AGENT 审中-公开
标题翻译：具有ARYL取代的胍基和/或双胍作为交联剂的电解质的环氧树脂组合物
公开(公告)号：WO1997011105A1
公开(公告)日：1997-03-27
申请号：PCT/EP1996003995
申请日：1996-09-11
申请人： AKZO NOBEL N.V. , BUSER, Antonius, Johannes, Wilhelmus , SCHUTYSER, Jan, Andre, Jozef
发明人： AKZO NOBEL N.V.
IPC分类号： C08G59/40
CPC分类号： C08G59/4021 , C08G59/30 , H01L23/145 , H01L2924/0002 , H05K1/0326 , H01L2924/00
摘要： The present invention pertains to a bromine-containing epoxy resin composition for printed wiring board substrates, i.e., for electrolaminates. The present invention provides a bromine-containing epoxy resin composition where the use of dicy as cross-linking agent is avoided and environmentally acceptable solvents such as acetone and methylethyl ketone can be employed. When liquid bromine-containing epoxy resins are employed, additional solvents can in fact be avoided altogether (this gives so-called solvent-free resin compositions). The epoxy resin composition according to the invention comprises: bromine-containing epoxy resin; aryl substituted guanidine or biguanide as cross-linking agent; optionally, epoxy resin not containing bromine; optionally, a catalyst and; optionally methylethyl ketone or acetone as a solvent, no additional solvents being present. Particular preference is given to the use of diphenyl guanidine and o-tolyl biguanide as cross-linking agents. The invention is also aimed at electrolaminates comprising the resin composition according to the invention.
摘要翻译：本发明涉及用于印刷线路板基板的含溴环氧树脂组合物，即用于电解液。本发明提供一种含溴环氧树脂组合物，其中避免使用双键作为交联剂，并且可以使用环境友好的溶剂如丙酮和甲基乙基酮。当使用液态含溴环氧树脂时，实际上可以完全避免另外的溶剂（这产生所谓的无溶剂树脂组合物）。根据本发明的环氧树脂组合物包含：含溴环氧树脂; 芳基取代的胍或双胍作为交联剂; 任选的不含溴的环氧树脂; 任选的催化剂; 任选的甲基乙基酮或丙酮作为溶剂，不存在另外的溶剂。特别优选使用二苯胍和邻甲苯双胍作为交联剂。本发明还涉及包含根据本发明的树脂组合物的电解质。

8. 发明申请

WO1996007683A1 ALLYL-CONTAINING EPOXY RESIN COMPOSITION COMPRISING A COPOLYMER OF AN ETHYLENICALLY UNSATURATED ANHYDRIDE AND A VINYL COMPOUND 审中-公开
标题翻译：含有乙烯基芳族化合物和乙烯基化合物的共聚物的含环氧树脂组合物
公开(公告)号：WO1996007683A1
公开(公告)日：1996-03-14
申请号：PCT/EP1995003523
申请日：1995-09-07
申请人： AKZO NOBEL N.V. , SCHUTYSER, Jan, André, Jozef , BUSER, Antonius, Johannes, Wilhelmus
发明人： AKZO NOBEL N.V.
IPC分类号： C08F283/10
CPC分类号： C08F283/10 , H05K1/0326
摘要： The invention relates to a resin composition comprising epoxy resin, a cross linking agent for the epoxy resin in the form of a carboxylic anhydride, and at least one allyl network forming compound. According to the invention, the anhydride-functional compound is a copolymer of an ethylenically unsaturated anhydride and a vinyl compound. Notably suitable are styrene-maleic anhydride copolymers known as SMA Type 1. Surprisingly, it was found that the presence of at least 2 wt.% of triallyl cyanurate (TAC) results in an increase in Tg, such that even with simple difunctional epoxy compounds resins can be obtained which have a glass transition temperature of 130 DEG C and higher. It was further found that the processing as prepreg of epoxy resins cross-linked using anhydride-vinyl copolymers will be greatly enhanced by the presence of at least 10 % of allyl.
摘要翻译：本发明涉及包含环氧树脂，羧酸酐形式的环氧树脂交联剂和至少一种烯丙基网形成化合物的树脂组合物。根据本发明，酸酐官能化合物是烯属不饱和酸酐和乙烯基化合物的共聚物。特别合适的是称为SMA型1的苯乙烯 - 马来酸酐共聚物。令人惊奇地发现，存在至少2重量％的氰尿酸三烯丙酯（TAC）导致Tg增加，使得即使使用简单的双官能环氧化合物可以获得玻璃化转变温度为130℃以上的树脂。进一步发现，使用酸酐 - 乙烯基共聚物交联的环氧树脂预浸料的加工将通过至少10％的烯丙基的存在而大大提高。

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