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1. 发明申请

WO2007076280A2 SIDE-SPECIFIC TREATMENT OF TEXTILES USING PLASMAS 审中-公开
标题翻译：使用等离子体处理纺织品的特殊处理
公开(公告)号：WO2007076280A2
公开(公告)日：2007-07-05
申请号：PCT/US2006/062040
申请日：2006-12-13
申请人： APJET, INC. , SELWYN, Gary, S. , HERRMANN, Hans, W. , BARNES, Matthew, R.
发明人： SELWYN, Gary, S. , HERRMANN, Hans, W. , BARNES, Matthew, R.
IPC分类号： D06M10/00
CPC分类号： D06M23/16 , D06B19/00 , D06M10/025
摘要： An apparatus (10) and method for generating gas-phase active chemical species suitable for selectively processing one side of a textile (16) or nonwoven material are described. Processing includes etching or stripping coatings, as examples. A low-temperature plasma (22) is used to produce an ionized gas containing radical species, atoms, ions, and electrons, some of which are suitable for removing or modifying the coating. For the purposes of the present invention, the plasma may be generated in a vacuum, or at atmospheric pressure. Dielectric-barrier discharges, atmospheric-pressure plasma jets, micro hollow-cathode discharges, coronas, or plasmas produced by a microwave discharge or laser-supplied energy may be used to generate the required species.
摘要翻译：描述了用于产生适于选择性地处理织物（16）或非织造材料的一侧的气相活性化学物质的装置（10）和方法。作为实例，加工包括蚀刻或剥离涂层。低温等离子体（22）用于产生含有自由基物质，原子，离子和电子的电离气体，其中一些适用于去除或改性涂层。为了本发明的目的，等离子体可以在真空中或在大气压下产生。可以使用介电阻挡放电，大气压等离子体射流，微空穴 - 阴极放电，通过微波放电或激光提供能产生的等离子体，以产生所需的物质。

2. 发明申请

WO2007076280A8 SIDE-SPECIFIC TREATMENT OF TEXTILES USING PLASMAS 审中-公开
标题翻译：使用等离子体处理纺织品的特殊处理
公开(公告)号：WO2007076280A8
公开(公告)日：2008-06-26
申请号：PCT/US2006062040
申请日：2006-12-13
申请人： APJET INC , SELWYN GARY S , HERRMANN HANS W , BARNES MATTHEW R
发明人： SELWYN GARY S , HERRMANN HANS W , BARNES MATTHEW R
IPC分类号： H05H1/24 , B44C1/22
CPC分类号： D06M23/16 , D06B19/00 , D06M10/025
摘要： An apparatus (10) and method for generating gas-phase active chemical species suitable for selectively processing one side of a textile (16) or nonwoven material are described. Processing includes etching or stripping coatings, as examples. A low-temperature plasma (22) is used to produce an ionized gas containing radical species, atoms, ions, and electrons, some of which are suitable for removing or modifying the coating. For the purposes of the present invention, the plasma may be generated in a vacuum, or at atmospheric pressure. Dielectric-barrier discharges, atmospheric-pressure plasma jets, micro hollow-cathode discharges, coronas, or plasmas produced by a microwave discharge or laser-supplied energy may be used to generate the required species.
摘要翻译：描述了用于产生适于选择性地处理织物（16）或非织造材料的一侧的气相活性化学物质的装置（10）和方法。处理包括蚀刻或剥离涂层，例如。低温等离子体（22）用于产生含有自由基物质，原子，离子和电子的电离气体，其中一些适用于去除或改性涂层。为了本发明的目的，等离子体可以在真空中或在大气压下产生。可以使用介电阻挡放电，大气压等离子体射流，由微波放电或激光提供的能量产生的微空心阴极放电，冠状物或等离子体来产生所需的物质。

3. 发明申请

WO2008057759A2 TREATMENT OF FIBROUS MATERIALS USING ATMOSPHERIC PRESSURE PLASMA POLYMERIZATION 审中-公开
标题翻译：使用大气压力等离子体聚合处理纤维材料
公开(公告)号：WO2008057759A2
公开(公告)日：2008-05-15
申请号：PCT/US2007082263
申请日：2007-10-23
申请人： APJET INC , SELWYN GARY S , BARNES MATTHEW R , VIDOLI CATERINA , VAZ HEATHCLIFF L
发明人： SELWYN GARY S , BARNES MATTHEW R , VIDOLI CATERINA , VAZ HEATHCLIFF L
IPC分类号： B05B5/00 , H05H1/00
CPC分类号： C23C16/50 , D06B19/00 , D06C29/00 , D06M10/10 , D06M14/18 , D06M15/277 , D21H19/16 , D21H19/32 , D21H23/44 , D21H25/04
摘要： An apparatus (10) and method for plasma finishing of fibrous materials including paper and knitted, woven and non-woven fibrous substrates such that desired characteristics are imparted are described. The method includes depositing a monomer comprising at least one fluorocarbon monomer with chemical additives, as required, at atmospheric pressure onto the paper or knitted, woven or non-woven substrate; exposing the monomer on a single surface of the fibrous material to an inert gas, atmospheric-pressure plasma, thereby causing polymerization of the monomer species; and repeating this sequence using multiple sequential deposition and plasma discharge steps to create a layered surface having durability against abrasion for both water-based laundry methods and dry-cleaning methods, and normal wear, without affecting the feel, drape, appearance or breathability of the substrate material. The present method uses a high-power, continuously operating plasma that is 104 times more powerful than the prior art plasma sources utilized in the textile industry, and produces a durable finish with between 0.5 and 2 s of plasma exposure. This is sufficiently rapid to meet commercial fabric processing throughput, and repeated cleaning of the electrodes is not required.
摘要翻译：描述了赋予纤维材料等离子体整理的装置（10）和方法，包括纸和针织，机织和非织造纤维基材，从而赋予所需的特性。该方法包括在大气压下将包含至少一种碳氟单体的单体与化学添加剂按需要沉积到纸或针织，机织或非编织基材上; 将单体在纤维材料的单个表面上暴露于惰性气体，大气压等离子体，从而引起单体物质的聚合; 并且使用多个顺序沉积和等离子体放电步骤重复该顺序，以产生具有耐水性的洗涤方法和干洗方法和正常磨损的耐磨性的层压表面，而不会影响鞋底的手感，悬垂性，外观或透气性基材。本方法使用大于等于在纺织工业中使用的现有技术等离子体的功率高出104倍的高功率，连续工作的等离子体，并产生0.5至2秒的等离子体曝光之间的耐用光洁度。这足以快速满足商业织物加工产量，并且不需要反复清洁电极。

4. 发明申请

WO2007076280A3 SIDE-SPECIFIC TREATMENT OF TEXTILES USING PLASMAS 审中-公开
标题翻译：用等离子体对纺织品进行侧面处理
公开(公告)号：WO2007076280A3
公开(公告)日：2008-01-03
申请号：PCT/US2006062040
申请日：2006-12-13
申请人： APJET INC , SELWYN GARY S , HERRMANN HANS W , BARNES MATTHEW R
发明人： SELWYN GARY S , HERRMANN HANS W , BARNES MATTHEW R
IPC分类号： H05H1/24 , B44C1/22
CPC分类号： D06M23/16 , D06B19/00 , D06M10/025
摘要： An apparatus (10) and method for generating gas-phase active chemical species suitable for selectively processing one side of a textile (16) or nonwoven material are described. Processing includes etching or stripping coatings, as examples. A low-temperature plasma (22) is used to produce an ionized gas containing radical species, atoms, ions, and electrons, some of which are suitable for removing or modifying the coating. For the purposes of the present invention, the plasma may be generated in a vacuum, or at atmospheric pressure. Dielectric-barrier discharges, atmospheric-pressure plasma jets, micro hollow-cathode discharges, coronas, or plasmas produced by a microwave discharge or laser-supplied energy may be used to generate the required species.
摘要翻译：描述了用于产生适合选择性处理纺织品（16）或非织造材料的一侧的气相活性化学物种的设备（10）和方法。作为例子，处理包括蚀刻或剥离涂层。低温等离子体（22）用于产生含有自由基物质，原子，离子和电子的电离气体，其中一些适合于去除或改变涂层。为了本发明的目的，可以在真空或大气压下产生等离子体。介质阻挡放电，大气压等离子体射流，微空心阴极放电，电晕或由微波放电或激光供应能量产生的等离子体可用于产生所需物质。

5. 发明申请

WO2017165714A1 METHOD FOR COLORING A SUBSTRATE USING ATMOSPHERIC PRESSURE PLASMA POLYMERIZATION 审中-公开
标题翻译：用大气压等离子体聚合着色基材的方法
公开(公告)号：WO2017165714A1
公开(公告)日：2017-09-28
申请号：PCT/US2017/023913
申请日：2017-03-23
申请人： APJET, INC.
发明人： CORNELIUS, Carrie E. , MCNEILL, III, James B.
IPC分类号： B05D3/06 , C08F2/52
CPC分类号： C09D11/107 , C09B62/473 , C09B69/106 , C09D4/00 , C09D5/14 , C09D5/18 , C09D11/106 , C09D11/328 , C09D133/14 , C09D133/26 , C09D135/02 , D06M16/00 , D06M2200/12 , D06M2200/30 , D06P1/006 , D06P5/2011 , C08F220/18
摘要： Methods for coloration of substrates, including textiles, by plasma polymerization of dyes to which polymerizable moieties have been chemically bonded at sites on the dye capable of bonding to such moieties, and that have been deposited on at least one surface of the substrate, are described. Atmospheric pressure plasmas were used for the polymerization process. Generally, the plasma polymerization is performed away from the dye deposition so that undeposited dye is not exposed to the plasma. Textiles may include cotton, polyester, wool, silk, acrylics, polypropylene, polyolefins, aramids, and nylon, and blends thereof. The plasma-polymerizable moiety may be chosen from acrylates, methacrylates, and vinyl amides. Dye functional groups may include hydroxyl groups, carboxyl groups, amines: primary, secondary, and tertiary, epoxides, carboxylic acids, and chlorides, and dyes may include acid dyes, disperse dyes, azo dyes, vat dyes, sulfur dyes, direct dyes, reactive dyes, basic dyes, pigment dyes, aniline dyes, anthraquinone dyes, and coumarin dyes, as examples.
摘要翻译：通过染料的等离子体聚合染色底物（包括纺织品）的方法，其中可聚合部分已经化学键合到染料上能够与这些部分键合的位点上，并且已经沉积在至少描述了衬底的一个表面。大气压等离子体用于聚合过程。通常，等离子体聚合远离染料沉积进行，以使未沉积的染料不暴露于等离子体。纺织品可以包括棉花，聚酯，羊毛，丝绸，丙烯酸树脂，聚丙烯，聚烯烃，芳族聚酰胺和尼龙，以及它们的混合物。等离子体可聚合部分可以选自丙烯酸酯，甲基丙烯酸酯和乙烯基酰胺。染料官能团可包括羟基，羧基，胺：伯，仲和叔，环氧化物，羧酸和氯化物，染料可包括酸性染料，分散染料，偶氮染料，还原染料，硫化染料，直接染料，活性染料，碱性染料，颜料染料，苯胺染料，蒽醌染料和香豆素染料作为例子。

6. 发明申请

WO2014046729A1 ATMOSPHERIC-PRESSURE PLASMA PROCESSING APPARATUS AND METHOD 审中-公开
标题翻译：大气压力等离子体处理装置和方法
公开(公告)号：WO2014046729A1
公开(公告)日：2014-03-27
申请号：PCT/US2013/031481
申请日：2013-03-14
申请人： APJET, INC. , CORNELIUS, Carrie, E. , ROCHE, Gregory, A. , TYNER, David, W.
发明人： CORNELIUS, Carrie, E. , ROCHE, Gregory, A. , TYNER, David, W.
IPC分类号： H05H1/24
CPC分类号： D06B19/007 , B23K10/003 , D06B1/02 , D10B2401/021 , H05H1/46 , H05H2001/466 , H05H2240/10 , H05H2245/123
摘要： A plasma processing apparatus including powered electrodes having elongated planar surfaces; grounded electrodes having elongated planar surfaces parallel to and coextensive with the elongated surfaces of the powered electrodes, and spaced-apart a chosen distance therefrom, forming plasma regions, is described. RF power is provided to the at least one powered electrode, both powered and grounded electrodes may be cooled, and a plasma gas is flowed through the plasma regions at atmospheric pressure; whereby a plasma is formed in the plasma regions. The material to be processed may be moved into close proximity to the exit of the plasma gas from the plasma regions perpendicular to the gas flow, and perpendicular to the elongated electrode dimensions, whereby excited species generated in the plasma exit the plasma regions and impinge unimpeded onto the material.
摘要翻译：一种等离子体处理装置，包括具有细长平面的动力电极描述了具有与被动电极的细长表面平行并且共同延伸的细长平面的接地电极，并且与其间隔开一定距离，形成等离子体区域。 RF功率被提供给至少一个供电电极，电源和接地电极都可以被冷却，等离子体气体在大气压力下流过等离子体区域; 由此在等离子体区域中形成等离子体。待处理的材料可以被移动到离垂直于气流的等离子体区域等离子体气体的出口附近，并且垂直于细长电极尺寸，由此在等离子体中产生的激发物质离开等离子体区域并且不受阻碍地撞击在材料上。

7. 发明申请

WO2009102603A1 LARGE AREA, ATMOSPHERIC PRESSURE PLASMA FOR DOWNSTREAM PROCESSING 审中-公开
标题翻译：大面积下水道加工大气压力等级
公开(公告)号：WO2009102603A1
公开(公告)日：2009-08-20
申请号：PCT/US2009/033144
申请日：2009-02-05
申请人： APJET, INC. , SELWYN, Gary, S.
发明人： SELWYN, Gary, S.
IPC分类号： H01J7/24
CPC分类号： H05H1/46 , H01J37/32082 , H01J37/32357 , H01J37/32596 , H01J37/32825 , H05H1/2406 , H05H2001/2418 , H05H2001/2431
摘要： An arcless, atmospheric-pressure plasma generating apparatus (10) capable of producing a large-area, temperature-controlled, stable discharge (20) at power densities between about 0.1 W/cm 3 and about 200 W/cm 3 , while having an operating gas temperature of less than 50 C, for processing materials (28) outside of the discharge, is described. The apparatus produces active chemical species, including gaseous metastables and radicals which may be used for polymerization (either free radical-induced or through dehydrogenation-based polymerization), surface cleaning and modification, etching, adhesion promotion, and sterilization, as examples. The invention may include either a cooled rf-driven electrode (12) or a cooled ground electrode (22), or two cooled electrodes, wherein active components of the plasma may be directed out of the plasma and onto an external workpiece (28) without simultaneously exposing a material to the electrical influence or ionic components of the plasma.
摘要翻译：一种无弧大气压等离子体发生装置（10），其能够以约0.1W / cm 3至约200W / cm 3的功率密度产生大面积，温度控制，稳定的放电（20），同时具有工作气体描述了低于50℃的温度，用于在放电之外的处理材料（28）。作为实例，该装置产生活性化学物质，包括可用于聚合（自由基诱导或基于脱氢的聚合），表面清洁和改性，蚀刻，粘附促进和灭菌的气态亚稳态和自由基。本发明可以包括冷却的rf驱动电极（12）或冷却的接地电极（22）或两个冷却的电极，其中等离子体的有源成分可以被引导出等离子体并且被引导到外部工件（28）上，而没有同时将材料暴露于等离子体的电学影响或离子组分。

8. 发明申请

WO2008057759A3 TREATMENT OF FIBROUS MATERIALS USING ATMOSPHERIC PRESSURE PLASMA POLYMERIZATION 审中-公开
公开(公告)号：WO2008057759A3
公开(公告)日：2008-05-15
申请号：PCT/US2007/082263
申请日：2007-10-23
申请人： APJET, INC. , SELWYN, Gary S. , BARNES, Matthew R. , VIDOLI, Caterina , VAZ, Heathcliff L.
发明人： SELWYN, Gary S. , BARNES, Matthew R. , VIDOLI, Caterina , VAZ, Heathcliff L.
IPC分类号： D06M10/00 , C08G10/00 , C08G77/00 , C08F283/00
摘要： Apparatus and method for plasma finishing of fibrous materials are disclosed. The method includes depositing a monomer comprising at least one fluorocarbon monomer with chemical additives, as required, at atmospheric pressure onto the fibrous material; exposing the monomer on a single surface of the fibrous material to an inert gas, atmospheric-pressure plasma, thereby causing polymerization of the monomer species; and repeating this sequence using multiple sequential deposition and plasma discharge steps to create a layered surface having durability against abrasion for both water-based laundry methods and dry-cleaning methods, and normal wear, without affecting the feel, drape, appearance or breathability of the substrate material. The present method uses a high-power, continuously operating plasma that is 10. sup 4 times more powerful than the prior art plasma sources and produces a durable finish with between 0.5 and 2 s of plasma exposure, whereby repeated cleaning of the electrodes is not required.

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