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1. 发明申请

WO2018049407A3 POLYPHENOL ALKOXYLATE CONTAINING BLENDS AND COATINGS 审中-公开
公开(公告)号：WO2018049407A3
公开(公告)日：2018-03-15
申请号：PCT/US2017/051197
申请日：2017-09-12
申请人： RESINATE MATERIALS GROUP, INC.
发明人： SPILMAN, Gary, E. , CHRISTY, Michael, R. , TABOR, Rick , COMSTOCK-REID, Brian, T. , KOVSKY, Jack, R. , SAMSON, Michelle, Marie
IPC分类号： C08G18/48 , C08G18/75 , C08G18/76 , C08G18/08 , C08G18/28 , C09D175/04 , C08G18/32 , C08G18/36
摘要： The present invention relates to polyol blends containing a polyol and a polyphenol alkoxylate, i.e. an aikoxylated polyphenol, and coatings prepared from these blends. The polyol blends have the advantage of a low residual polyphenol content and have desirable viscosity characteristics without the need for diluents or solvents which could result in unwanted VOC emissions. In another aspect of the invention, polyester polyols are prepared using polyphenol aikoxyiates. Coatings prepared using these polyol compositions have improved salt spray corrosion resistance, along with a variety of other excellent coating performance properties. Also, the polyols used herein can contain a significant recycle and biorenewabie content, making these blends and coatings sustainable alternatives to petroleum based polyol products.

2. 发明申请

WO2016069622A1 HIGH RECYCLE CONTENT POLYESTER POLYOLS FROM HYDROXY-FUNCTIONAL KETAL ACIDS, ESTERS OR AMIDES 审中-公开
标题翻译：来自羟基功能性糖，高分子或氨基酸的高回收率聚酯多元醇
公开(公告)号：WO2016069622A1
公开(公告)日：2016-05-06
申请号：PCT/US2015/057620
申请日：2015-10-27
申请人： RESINATE MATERIALS GROUP, INC.
发明人： TABOR, Rick , VRABEL, Eric, David , ROGERS, Kevin, Anthony , BEATTY, Matthew, James , BAE, Woo-Sung , KOVSKY, Jack, Rogers , CHRISTY, Michael, Robert
IPC分类号： C08G18/42 , C08J11/24 , C08G63/60 , C08G63/66
CPC分类号： C08G63/66 , C08G18/14 , C08G18/4244 , C08G18/4252 , C08G18/4837 , C08G18/7621 , C08G63/60 , C08G2101/0008 , C08G2101/0083 , C08J11/24 , C08J2367/02 , C09D175/06 , C09J175/06 , Y02P20/582 , Y02W30/706
摘要： Polyester polyols, processes for making them, and applications for the polyols are disclosed. In some aspects, the polyols comprise recurring units from a thermoplastic polyester or an aromatic polyacid source, a glycol, and a hydroxy-functional ketal acid, ester or amide. Optionally, the polyols incorporate recurring units of a hydrophobe. The polyols are made in one or multiple steps; in some aspects, the thermoplastic polyester or aromatic polyacid source and the glycol are reacted first, followed by reaction with the hydroxy-functional ketal acid, ester or amide. The resulting polyols have good transparency and little or no particulate settling or phase separation. High-recycle-content polyols having desirable properties and attributes for formulating polyurethane products, including aqueous polyurethane dispersions, flexible and rigid foams, coatings, adhesives, sealants, and elastomers can be made. The polyols provide a sustainable alternative to bio- or petrochemical-based polyols.
摘要翻译：公开了聚酯多元醇，其制备方法和多元醇的应用。在一些方面，多元醇包括来自热塑性聚酯或芳族多酸源，二醇和羟基官能的缩酮酸，酯或酰胺的重复单元。任选地，多元醇包含疏水物的重复单元。多元醇制成一个或多个步骤; 在一些方面，首先使热塑性聚酯或芳族多酸源和二醇反应，然后与羟基官能的缩酮酸，酯或酰胺反应。得到的多元醇具有良好的透明度和很少或没有微粒沉降或相分离。可以制备具有用于配制聚氨酯产品，包括水性聚氨酯分散体，柔性和刚性泡沫，涂料，粘合剂，密封剂和弹性体的所需性质和特性的高回收含量的多元醇。多元醇为生物或石油化学的多元醇提供了可持续的替代方案。

3. 发明申请

WO2018044502A1 SUSTAINABLE BASE OILS FOR LUBRICANTS 审中-公开
标题翻译：可持续的润滑油基础油
公开(公告)号：WO2018044502A1
公开(公告)日：2018-03-08
申请号：PCT/US2017/045500
申请日：2017-08-04
申请人： RESINATE MATERIALS GROUP, INC.
发明人： BAE, Woo-sung , KOVSKY, Jack, R. , TABOR, Rick
IPC分类号： C10M105/44 , C08J11/24 , C10M107/32 , C10M109/02
摘要： Sustainable lubricant compositions made from recycled thermoplastic polyesters and other reclaimed or biorenewable reactants and a method of formulating them are disclosed. The lubricant compositions comprise a polyester base oil, which incorporates recurring units from a digested thermoplastic polyester, a low-molecular-weight polyol, and C 8 -C 24 fatty acid. The base oil has a number-average molecular weight within the range of 300 to 5000 g/mol, a hydroxyl value less than 50 mg KOH/g, and a viscosity at 40°C less than 5000 cSt. Some of the lubricant compositions comprise the polyester base oil and one or more additives including anti-wear agents, corrosion inhibitors, antioxidants, thickeners, detergents, and the like. The lubricants have properties that rival those of commercial products made from nonrenewable hydrocarbon blends or polyol esters and are useful for many practical applications such as internal combustion engine oils, gear lubrication oils, hydraulic oils, compressor oils, metal working fluids, and lubricating greases.
摘要翻译：公开了由回收的热塑性聚酯和其他回收或生物可再生反应物制成的可持续润滑剂组合物及其配制方法。润滑剂组合物包含聚酯基础油，其包含来自消化的热塑性聚酯，低分子量多元醇和C 8 -C 24脂肪酸的重复单元。该基础油的数均分子量在300-5000g / mol的范围内，羟值小于50mg KOH / g，并且在40℃下的粘度小于5000cSt。一些润滑剂组合物包含聚酯基础油和一种或多种添加剂，包括抗磨剂，缓蚀剂，抗氧化剂，增稠剂，去污剂等。润滑剂具有与由不可再生烃混合物或多元醇酯制成的商业产品相媲美的性能，并且可用于许多实际应用，例如内燃机油，齿轮润滑油，液压油，压缩机油，金属加工液和润滑脂。

4. 发明申请

WO2017044330A1 POLYESTER POLYOLS FOR REACTIVE HOT-MELT ADHESIVES 审中-公开
标题翻译：用于反应性热熔胶粘剂的聚酯多元醇
公开(公告)号：WO2017044330A1
公开(公告)日：2017-03-16
申请号：PCT/US2016/049190
申请日：2016-08-29
申请人： RESINATE MATERIALS GROUP, INC.
发明人： BAE, Woo-sung , ROGERS, Kevin , CHRITY, Michael , TABOR, Rick
IPC分类号： C08G18/76 , C08G63/183 , C08G63/64 , C08G18/42 , C08G18/44 , C09J175/04
CPC分类号： C08G18/4216 , C08G18/44 , C08G18/7671 , C08G63/183 , C08G63/64 , C08G2170/20 , C09J175/04 , Y02P20/582
摘要： Semi-crystalline polyester polyols and their use in reactive hot-melt adhesives are disclosed. The polyols comprise recurring units of a C 2 -C 10 aliphatic diol, a C 8 -C 24 aliphatic dicarboxylic acid, and 1 to 20 wt.% of an aromatic dicarboxylic acid source, a polycarbonate, or a combination thereof. The polyols have a hydroxyl number within the range of 14 to 1 12 mg KOH/g. Reactive hot-melt adhesives from the polyols and composite structures produced using the adhesives are also disclosed. A minor proportion of aromatic dicarboxylic acid, polycarbonate content in the polyester polyol surprisingly improves the properties of reactive hot-melt adhesives when compared with a commercial hot-melt adhesive or an adhesive formulated using an all-aliphatic polyester polyol. The adhesives are useful for bonding a wide variety of substrates, including paper, wood, glass, ceramics, plastics, and metals.
摘要翻译：公开了半结晶聚酯多元醇及其在反应性热熔粘合剂中的用途。多元醇包括C 2 -C 10脂族二醇，C 8 -C 24脂族二羧酸和1至20重量％芳族二羧酸源，聚碳酸酯或其组合的重复单元。多元醇的羟值在14-112mg KOH / g的范围内。还公开了使用粘合剂制备的多元醇和复合结构的活性热熔粘合剂。当与商业热熔粘合剂或使用全脂族聚酯多元醇配制的粘合剂相比时，少量的芳族二羧酸，聚酯多元醇中的聚碳酸酯含量令人惊奇地改善了反应性热熔粘合剂的性能。粘合剂可用于粘合各种基材，包括纸，木材，玻璃，陶瓷，塑料和金属。

5. 发明申请

WO2015171433A1 POLYESTER POLYOLS FROM THERMOPLASTIC POLYESTERS AND DIMER FATTY ACIDS 审中-公开
标题翻译：来自热塑性聚酯和二脂肪酸的聚酯多元醇
公开(公告)号：WO2015171433A1
公开(公告)日：2015-11-12
申请号：PCT/US2015/028644
申请日：2015-04-30
申请人： RESINATE MATERIALS GROUP, INC.
发明人： MUKERJEE, Shakti, L. , TABOR, Rick , EMERSON, Adam, William , ROGERS, Kevin, Anthony , VRABEL, Eric, D. , BROWN, Matthew, T. , BEATTY, Matthew, J. , KOVSKY, Jack, Rogers , KELLERMAN, Michael, D. , CHRISTY, Michael, Robert
IPC分类号： C08G18/36 , C08J11/24 , C08G63/553 , C08G18/42 , C08L67/08
CPC分类号： C08G63/916 , C07C67/03 , C07C67/08 , C07C69/82 , C07C2601/14 , C08G18/36 , C08G18/4213 , C08G18/4288 , C08G18/735 , C08G18/755 , C08G63/553 , C08G2101/0008 , C08G2101/0025 , C08J11/24 , C08J2367/02 , C09D167/07 , C09D175/06 , Y02W30/706
摘要： Polyester polyols made from thermoplastic polyesters are disclosed. The polyols can be made by heating a thermoplastic polyester such as virgin PET, recycled PET, or mixtures thereof, with a glycol to give a digested intermediate, which is then condensed with a dimer fatty acid to give the polyol. The invention includes a polyester polyol comprising recurring units of a glycol-digested thermoplastic polyester and a dimer fatty acid. The polyester polyol can also be made in a single step by reacting the thermoplastic polyester, glycol, and dimer acid under conditions effective to produce the polyol. High-recycle-content polyols having desirable properties and attributes for formulating polyurethane products, including aqueous polyurethane dispersions, can be made. The polyols provide a sustainable alternative to bio- or petrochemical-based polyols.
摘要翻译：公开了由热塑性聚酯制成的聚酯多元醇。多元醇可以通过将热塑性聚酯如原始PET，再循环PET或其混合物与二醇加热来制备，得到消化的中间体，然后将其与二聚脂肪酸缩合得到多元醇。本发明包括含有二醇消化的热塑性聚酯和二聚脂肪酸的重复单元的聚酯多元醇。聚酯多元醇也可以通过在有效制备多元醇的条件下使热塑性聚酯，二醇和二聚酸反应在一个步骤中制备。可以制备具有用于配制聚氨酯产品（包括水性聚氨酯分散体）的所需性质和特性的高回收含量的多元醇。多元醇为生物或石油化学的多元醇提供了可持续的替代方案。

6. 发明申请

WO2017058846A1 HIGH PERFORMANCE COATINGS 审中-公开
标题翻译：高性能涂料
公开(公告)号：WO2017058846A1
公开(公告)日：2017-04-06
申请号：PCT/US2016/054069
申请日：2016-09-28
申请人： RESINATE MATERIALS GROUP, INC.
发明人： SPILMAN, Gary , CHRISTY, Michael , VRABEL, Eric , FRYZ, Gage , TABOR, Rick , COMSTOCK-REID, Brian, T.
IPC分类号： C08J11/24 , C08G64/14 , C09D167/02 , C09D169/00 , C09D175/04 , C08G63/64 , C08L67/02 , C08L69/00
CPC分类号： C09D175/06 , C08G18/227 , C08G18/246 , C08G18/4225 , C08G18/4288 , C08G18/44 , C08G18/6607 , C08G18/722 , C08G18/73 , C08G18/755 , C08G18/8074 , C08G63/64 , C08G64/14 , C08G2101/0025 , C08G2105/02 , C08G2150/20 , C08G2150/90 , C08J11/24 , C08J2367/02 , C08J2369/00 , C08K3/22 , C08K5/13 , C08K2003/2241 , C08L67/02 , C08L69/00 , C09D5/08 , C09D167/02 , C09D169/00 , C09D169/005 , C09D175/04
摘要： The present invention relates to coatings, particularly high performance coatings, containing a polyester polyol comprising recurring units derived from a polyacid source, poly(bisphenol-A carbonate) (PBAC), and a glycol. The PBAC is preferably recycled poly(bisphenol-A carbonate) (rPBAC). These coatings provide improved salt spray and stain resistance along with a variety of other coating performance attributes. The polyols can contain a significant recycle and biobased content, making them sustainable alternatives to petroleum based polyols.
摘要翻译：本发明涉及包含聚酯多元醇的涂料，特别是高性能涂料，其包含衍生自多酸源，聚（双酚A碳酸酯）（PBAC）和二醇的重复单元。 PBAC优选是再循环的聚（双酚A碳酸酯）（rPBAC）。这些涂层提供改善的盐雾和耐污染性以及各种其它涂层性能特征。多元醇可以含有显着的循环和生物基含量，使其成为石油基多元醇的可持续替代品。

7. 发明申请

WO2016168043A1 POLYESTER POLYOLS WITH INCREASED CLARITY 审中-公开
标题翻译：聚酯多元醇具有增加的清晰度
公开(公告)号：WO2016168043A1
公开(公告)日：2016-10-20
申请号：PCT/US2016/026337
申请日：2016-04-07
申请人： RESINATE MATERIALS GROUP, INC.
发明人： TABOR, Rick , VRABEL, Eric, D.
IPC分类号： C08G63/19 , C08J11/24 , C08G18/42 , C08K5/13 , C08L67/00 , C08L67/02 , C08L75/04 , C08L75/06 , C08G63/18 , C08G63/91 , C08G63/183 , C08G63/193 , C08G63/195
CPC分类号： C08G63/12 , C08G18/42 , C08G18/4225 , C08G18/4288 , C08G63/195 , C08G63/64 , C08G63/6886 , C08G63/916 , C08J11/10 , Y02P20/582
摘要： Polyester polyols, processes for making them, and applications for the polyols are disclosed. Some of the polyols comprise recurring units from a digested thermoplastic polyester (e.g., recycled polyethylene terephthalate), a diol, an optional hydrophobe, and a clarifier. The clarifier, which in some cases is a bisphenol, bisphenol alkoxylate, bisphenol polycarbonate, sulfonyl diphenol, or sulfonyl diphenol alkoxylate, helps the polyol remain clear for weeks or months after its preparation. In some aspects, the clarifier is a monophenol, bisphenol, or poly-phenol having two or more phenylene rings wherein at least two of the phenylene rings lack a common molecular axis. The clarifier may also be an alkylated phenol, an epoxy resin, an epoxy novolac resin, a diphenylmethane, or a tris(aryloxy)phosphate. The polyols are valuable for formulating a variety of polyurethanes and related products-including polyurethane dispersions, flexible and rigid foams, coatings, adhesives, sealants, and elastomers and they provide a sustainable alternative to bio- or petrochemical-based polyols.
摘要翻译：公开了聚酯多元醇，其制备方法和多元醇的应用。一些多元醇包含来自消化的热塑性聚酯（例如，再循环的聚对苯二甲酸乙二醇酯），二醇，任选的疏水物和澄清剂的重复单元。在一些情况下，澄清剂是双酚，双酚烷氧基化物，双酚聚碳酸酯，磺酰基二酚或磺酰基二酚烷氧基化物，有助于多元醇在其制备后保持清洁数周或数月。在一些方面，澄清器是具有两个或更多个亚苯基环的单酚，双酚或聚苯酚，其中至少两个亚苯基环缺少共同的分子轴。澄清剂也可以是烷基化酚，环氧树脂，环氧酚醛树脂，二苯基甲烷或三（芳氧基）磷酸酯。多元醇对于配制各种聚氨酯和相关产品（包括聚氨酯分散体，柔性和刚性泡沫，涂料，粘合剂，密封剂和弹性体）是有价值的，并且它们提供了基于生物或石油化学的多元醇的可持续替代品。

8. 发明申请

WO2016153780A1 CYCLOALIPHATIC POLYESTER POLYOLS FROM THERMOPLASTIC POLYESTERS 审中-公开
标题翻译：来自热塑性聚酯的环状聚酯多元醇
公开(公告)号：WO2016153780A1
公开(公告)日：2016-09-29
申请号：PCT/US2016/021437
申请日：2016-03-09
申请人： RESINATE MATERIALS GROUP, INC.
发明人： TABOR, Rick , VRABLE, Eric, David , BEATTY, Matthew
IPC分类号： C08G63/91 , C08J11/24 , C08G63/553 , C09D175/06 , C08G18/42
CPC分类号： C08G63/916 , C08G18/4202 , C08G18/423 , C08G18/4288 , C08G63/553 , C08J11/24 , C08J2367/02 , C09D175/06 , Y02W30/706
摘要： Cycloaliphatic polyester polyols and processes for making them from thermoplastic polyesters are disclosed. One process comprises heating a thermoplastic polyester with a glycol to give a digested intermediate and hydrogenating aromatic rings in the digested intermediate to produce the cycloaliphatic polyester polyol. Optionally, the digested intermediate is reacted with a hydrophobe to give a modified polyol prior to hydrogenation, and the modified polyol is hydrogenated to give the cycloaliphatic polyester polyol. The high-recycle-content cycloaliphatic polyester polyols have desirable attributes for formulating polyurethane dispersions, two-component polyurethane coatings, mono- or poly(meth)acrylates, polyisocyanurates, flexible and rigid foams, coatings, adhesives, sealants, and elastomers, and they provide a sustainable alternative to petrochemical-based polyols.
摘要翻译：公开了环脂族聚酯多元醇及其由热塑性聚酯制备它们的方法。一种方法包括用二醇加热热塑性聚酯以在消化的中间体中产生消化的中间体和氢化芳环以制备脂环族聚酯多元醇。任选地，将消化的中间体与疏水物反应以在氢化之前得到改性的多元醇，并将改性的多元醇氢化得到环脂族聚酯多元醇。高回收含量的脂环族聚酯多元醇具有用于配制聚氨酯分散体，双组分聚氨酯涂料，单或多（甲基）丙烯酸酯，聚异氰脲酸酯，柔性和刚性泡沫，涂料，粘合剂，密封剂和弹性体的所需属性，并且它们为石化多元醇提供可持续的替代方案。

9. 发明申请

WO2016123558A1 INTEGRATED PROCESS FOR TREATING RECYCLED STREAMS OF PET AND PTT 审中-公开
标题翻译：用于处理PET和PTT回收流的综合过程
公开(公告)号：WO2016123558A1
公开(公告)日：2016-08-04
申请号：PCT/US2016/015799
申请日：2016-01-29
申请人： RESINATE MATERIALS GROUP, INC.
发明人： PHILLIPS, Brian, Douglas , TABOR, Rick , MUKERJEE, Shakti, L. , ROGERS, Kevin , EMERSON, Adam, W. , VRABEL, Eric, David , CHERMSIDE, Brian
IPC分类号： C08J5/24 , C08G18/08 , C08G18/36 , C08G18/42 , C08G63/91
CPC分类号： C08J11/24 , C08G18/0823 , C08G18/10 , C08G18/36 , C08G18/42 , C08G18/4288 , C08G63/916 , C08J5/24 , C08J2367/02 , C08J2375/06 , C08J2423/02 , C08K5/12 , Y02P20/125
摘要： A process for producing a polyester polyol comprising reacting a recycle stream selected from recycled PET carpet, carpet fiber, containers, textiles, articles or mixtures thereof, with a glycol in a reactor, thereby forming a digested product stream comprising polyols, and an undigested stream; and then reacting the digested product stream with a hydrophobe selected from dimer fatty acids, trimer fatty acids, oleic acid, ricinoleic acid, tung oil, corn oil, canola oil, soybean oil, sunflower oil, bacterial oil, yeast oil, algae oil, castor oil, triglycerides or alkyl carboxylate esters having saturated or unsaturated C6-C36 fatty acid units, saturated or unsaturated C6-C36 fatty acids, alkoxylated castor oil, saturated or unsaturated C9-C18 dicarboxylic acids or diols, cardanol-based products, recycled cooking oil, branched or linear C6-C36 fatty alcohols, hydroxy- functional materials derived from epoxidized, ozonized, or hydroformylated fatty esters or acids, or mixtures thereof.
摘要翻译：一种制备聚酯多元醇的方法，包括使选自回收的PET地毯，地毯纤维，容器，织物，制品或其混合物的再循环料流与反应器中的二醇反应，从而形成包含多元醇的消化产物流和未消化的流 ; 然后将消化的产物流与选自二聚脂肪酸，三聚体脂肪酸，油酸，蓖麻油酸，桐油，玉米油，菜籽油，大豆油，向日葵油，细菌油，酵母油，藻油，具有饱和或不饱和C6-C36脂肪酸单元，饱和或不饱和C6-C36脂肪酸，烷氧基化蓖麻油，饱和或不饱和C 9 -C 18二羧酸或二醇的蓖麻油，甘油三酸酯或烷基羧酸酯，腰果酚基产物，再循环烹饪油，支链或直链C6-C36脂肪醇，衍生自环氧化，臭氧化或加氢甲酰化脂肪酸酯或酸的羟基官能材料，或其混合物。

10. 发明申请

WO2019100058A1 POLYOL COMPOSITIONS FROM THERMOPLASTIC POLYESTERS AND THEIR USE IN HOT-MELT ADHESIVES AND BINDERS 审中-公开
公开(公告)号：WO2019100058A1
公开(公告)日：2019-05-23
申请号：PCT/US2018/062004
申请日：2018-11-20
申请人： RESINATE MATERIALS GROUP, INC.
发明人： CHRISTY, Michael, Robert , COMSTOCK-REID, Brian, T. , ROGERS, Kevin, Anthony , PILON, Samantha , SIMOS, Crystal , MUKERJEE, Shakti, L. , TABOR, Rick
IPC分类号： C08G63/91 , C08G63/183 , C08J11/24
CPC分类号： C08G63/183 , C08G63/48 , C08G63/916 , C08J11/24
摘要： Polyester polyols made from partially glycolyzed thermoplastics and useful as components of hot-melt adhesives and binder compositions are disclosed. The polyols comprise recurring units of a thermoplastic polyester, a diol, optionally, a vegetable oil- based hydrophobe, optionally a C4-C36 dicarboxylic acid, diester, or anhydride; and optionally a polyether polyol. Some of the polyols have a hydroxyl number within the range of 10 to 50 mg KOH/g, an acid number within the range of 10 to 50 mg KOH/g, and a ring-and-ball softening point of at least 40°C. Hot-melt adhesive compositions comprising the polyols are also described. Binder compositions, including asphalt binder compositions, comprising the polyester polyols are also disclosed. While glycolysis is most often used to generate monomeric building blocks, we found that partially glycolyzed thermoplastics can be valuable intermediates for producing hot-melt adhesives and binder compositions.

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