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31. 发明申请

WO2004113597A1 THE TECHNIQUE OF PRODUCTION OF FANCY RED DIAMONDS 审中-公开
标题翻译：粉红色钻石生产技术
公开(公告)号：WO2004113597A1
公开(公告)日：2004-12-29
申请号：PCT/RU2004/000205
申请日：2004-05-27
IPC分类号： C30B33/04
CPC分类号： C30B29/04 , B01J3/062 , B01J19/085 , B01J2203/062 , B01J2203/0655 , B01J2203/0695 , C01B32/28
摘要： The invention concerns the treatment of diamonds in order to give them different colors and it can be made ise of by gem trade. The Essence of invention: The technique consists in producing isolated substitutional nitrogen atoms, or C centers in the crystal lattice of natural type Ia diamond containing A centers or of natural high-nitrogenous type Ia diamond containing over 800 ppm of nitrogen in the form of A and B1 centers. Natural type Ia diamonds containing A centers are annealed in a high-pressure apparatus at a temperature over 2150 DEG C under stabilizing pressure of 6.0-7.0 Gpa, then irradiated with 5x10 -5x10 cm 2-4 MeV electrons and finally annealed in vacuum at a temperature no lower than 1100 DEG C. Natural high-nitrogenous type Ia diamonds, containing over 800 ppm of nitrogen in the form of A and B1 centers, are irradiated with high-energy electrons with the irradiation dose over 10 cm and are annalead in vacuum at a temperature no lower than 1100 DEG C. Thus Fancy Red diamonds are produced with stable N-V cenetrs absorbing in the 400-to-640 nm range.
摘要翻译：本发明涉及钻石的处理以使其具有不同的颜色，并且可以通过宝石贸易来制造。发明的本质：该技术包括在含有A中心的天然Ia型金刚石或含有超过800ppm氮的形式的天然高氮型Ia金刚石的晶格中产生分离的取代氮原子或C中心，其形式为A 和B1中心。含有A中心的天然Ia型金刚石在高压设备中在温度超过2150℃，稳定压力为6.0-7.0Gpa的条件下退火，然后用5×10 -5×10 18 cm -2 2- 4 MeV电子，最后在不低于1100℃的温度下真空退火。含有超过800ppm A和B1中心形式的氮的天然高氮型Ia金刚石用高能电子照射辐射剂量超过10 19 cm -2，并且在不低于1100℃的温度下在真空中放置。因此，在400至640nm范围内吸收的稳定的NV透明层产生花式红色金刚石。

32. 发明申请

WO02048038A2 JADEITE AND ITS PRODUCTION 审中-公开
标题翻译：玉米及其生产
公开(公告)号：WO02048038A2
公开(公告)日：2002-06-20
申请号：PCT/US2001/046615
申请日：2001-12-05
IPC分类号： B01J3/06 , C01B33/20 , C01B33/26
CPC分类号： C01B33/26 , B01J3/062 , B01J2203/068 , C01B33/20 , Y10T428/2982 , Y10T428/2996
摘要： A jadeite material has a thickness in excess of about 1.0 mm and CIELAB indices of L* > 42, a* +6. The grain size of the jadeite material is less than about 30 microns and is an equiaxed grain structure. The jadeite material has an optical transmission peak between 500 and 565 nm with an I/Io optical transmission ratio of over 40 %. The first step in making the jadeite material is to wrap a glass block, convertible by HP/HT into jadeite and having a nominal composition of NaAlSi2O6, with a graphite or refractive metal sheet. The wrapped glass block is placed in an HP/HT apparatus, rapidly heated, and subjected therein to a pressure in excess of about 3 GPa and a temperature in excess of about 1000 DEG C for a time adequate to convert the glass block into jadeite. The jadeite material then is cooled and the pressure subsequently released.
摘要翻译：翡翠材料的厚度超过约1.0mm，CIELAB指数L *> 42，a * <-6，b *> +6。翡翠材料的晶粒尺寸小于约30微米，是等轴晶粒结构。翡翠材料的光传输峰值在500和565nm之间，I / Io光传输比率超过40％。制造翡翠材料的第一步是将玻璃块包裹，由HP / HT转化为翡翠，并具有标称组成的NaAlSi 2 O 6与石墨或折射金属片。将包裹的玻璃块放置在HP / HT装置中，快速加热，并在其中进行超过约3GPa的压力和超过约1000℃的温度足以将玻璃块转化成翡翠的时间。然后将翡翠材料冷却并随后释放压力。

33. 发明申请

WO01024920A1 GROWTH OF DIAMOND CLUSTERS 审中-公开
标题翻译：金刚石簇的生长
公开(公告)号：WO01024920A1
公开(公告)日：2001-04-12
申请号：PCT/IB2000/001415
申请日：2000-10-04
IPC分类号： B01J3/06 , B01J23/74 , C01B31/06 , C30B29/04
CPC分类号： B01J3/062 , B01J23/74 , B01J2203/062 , B01J2203/0655 , B01J2203/068 , B01J2203/0685 , C01B32/25
摘要： A diamond cluster comprises a core (14) and an overgrown region, the overgrown region containing a plurality of diamond crystallites (16) extending outwards from the core (14), the majority of the diamond crystallites (16) having a cross-sectional area which increases as the distance from the core increases. A method of producing diamond clusters is also provided.
摘要翻译：金刚石簇包括芯（14）和长满的区域，所述长满的区域包含从芯（14）向外延伸的多个金刚石微晶（16），大部分金刚石微晶（16）具有横截面积随着距核心距离的增加而增加。还提供了一种生产金刚石簇的方法。

34. 发明申请

WO1993016015A1 PROCESS FOR PREPARING AN AMORPHOUS, EXTRA-HARD MATERIAL BASED ON BORON NITRIDE 审中-公开
标题翻译：基于硼酸盐制备不定形，超硬材料的方法
公开(公告)号：WO1993016015A1
公开(公告)日：1993-08-19
申请号：PCT/EP1993000314
申请日：1993-02-09
申请人： FIRMA SIEGFRIED GÖLZ , WILDENBURG, Jörg
发明人： FIRMA SIEGFRIED GÖLZ
IPC分类号： C04B35/58
CPC分类号： C03B19/06 , B01J3/062 , B01J2203/0645 , B01J2203/066 , B01J2203/068 , C03C3/328 , C04B35/583 , Y02P40/57
摘要： A process is disclosed for preparing an amorphous ultra-hard material based on boron nitride that is sufficiently hard to scratch diamond. Hexagonal or turbostratic boron nitride hBN is compressed under pressures of at least 70kbar or more and heated up to temperatures of at least 1650 °C or more, until a molten mass of boron nitride is obtained. The thus formed molten mass of boron nitride is quenched by stopping heat supply, then the pressure on the quenched molten mass of boron nitride is relieved. The hexagonal or turbostratic boron nitride used as feedstock is treated in the presence of crystallisation inhibitors, so that no crystals are formed, and the amorphous crystalline structure is condensed by deposition of reaction products, such as boron suboxides.

35. 发明申请

WO1986004890A1 SINTERING PROCESS 审中-公开
标题翻译：烧结工艺
公开(公告)号：WO1986004890A1
公开(公告)日：1986-08-28
申请号：PCT/JP1986000069
申请日：1986-02-14
申请人： KABUSHIKI KAISHA KOMATSU SEISAKUSHO , OGATA, Masaru , TAKEDA, Shuichi
发明人： KABUSHIKI KAISHA KOMATSU SEISAKUSHO
IPC分类号： C04B35/64
CPC分类号： B01J3/062 , B01J2203/0645 , B01J2203/066 , B01J2203/0685 , B22F3/08 , B22F3/14 , C04B35/645 , C04B35/651
摘要： A process for densely sintering metal powder, ceramic powder or a mixture thereof by conducting high-temperature heating in a short time under a super-high pressure of 100,000 atm or above. The high-temperature heating is conducted by causing a thermit reaction within a super-high pressure-generating apparatus equipped with a pyrophyllite gasket and a cylinder and an anvil having a heat insulator. Hexagonal boron nitride and/or tantalum barriers are arranged in place in the apparatus for preventing any reaction between the resulting thermit composition and sintered powder or heater and for electric insulation.
摘要翻译：通过在100,000atm以上的超高压下在短时间内进行高温加热，将金属粉末，陶瓷粉末或其混合物密集烧结的方法。高温加热是通过在配备有叶蜡石垫圈的超高压发生装置和具有隔热材料的圆筒和砧座之间引起热反应而进行的。六边形氮化硼和/或钽屏障布置在设备中的适当位置，用于防止所得到的热敏组合物与烧结粉末或加热器之间的任何反应，并用于电绝缘。

36. 发明申请

WO2016210428A1 HIGH PRESSURE REACTOR AND METHOD OF GROWING GROUP III NITRIDE CRYSTALS IN SUPERCRITICAL AMMONIA 审中-公开
标题翻译：高压反应器及其在超临界氨基酸中生长III族氮化物晶体的方法
公开(公告)号：WO2016210428A1
公开(公告)日：2016-12-29
申请号：PCT/US2016/039622
申请日：2016-06-27
申请人： SIXPOINT MATERIALS, INC. , SEOUL SEMICONDUCTOR CO., LTD.
发明人： HASHIMOTO, Tadao
IPC分类号： C30B7/10 , C30B29/40 , B01J3/00 , B01J3/04 , B01J3/06
CPC分类号： C30B29/406 , B01J3/008 , B01J3/042 , B01J3/062 , C30B7/105
摘要： Provided is a high-pressure reactor suitable for a high-pressure process using supercritical ammonia grow bulk crystal of group III nitride having lateral dimension larger than 2 inches or to form various transition metal nitrides. The reactor has nutrient distributed along the reactor's longitudinal axis and seed material positioned at the reactor's inner wall and along the reactor's longitudinal axis. Nutrient diffuses through supercritical ammonia from the reactor's longitudinal axis and deposits on the seed material positioned by the reactor's inner wall. Both the nutrient and seed material are heated by the same heater. Material growth can primarily be due to material diffusion through supercritical ammonia. This configuration and methodology reduce convective movement of supercritical ammonia due to temperature differential, providing a more quiescent environment in which group III nitride or transition metal nitride is formed.
摘要翻译：提供了适用于使用横向尺寸大于2英寸的III族氮化物的超临界氨生长体晶体或形成各种过渡金属氮化物的高压法的高压反应器。反应器具有沿着反应器的纵向轴线的分布的营养物质和位于反应器的内壁和沿着反应器的纵向轴线的种子材料。营养物通过超临界氨从反应器的纵轴扩散并沉积在由反应器内壁定位的种子材料上。营养物质和种子材料均由相同的加热器加热。材料生长主要是由于通过超临界氨的物质扩散。这种配置和方法减少了由于温差引起的超临界氨的对流运动，提供了形成III族氮化物或过渡金属氮化物的更静态的环境。

37. 发明申请

WO2016146570A1 PRESS APPARATUS FOR ULTRA-HIGH PRESSURES AND METHODS OF CONTROLLING SAME 审中-公开
标题翻译：用于超高压的压力设备及其控制方法
公开(公告)号：WO2016146570A1
公开(公告)日：2016-09-22
申请号：PCT/EP2016/055430
申请日：2016-03-14
申请人： ELEMENT SIX (UK) LIMITED
发明人： VUKOVIC, Dragan
IPC分类号： B01J3/06
CPC分类号： B01J3/067 , B01J3/062 , B01J2203/062 , B01J2203/0645 , B01J2203/0655 , B01J2203/066 , B01J2203/068 , B01J2203/0685
摘要： Press apparatus for pressurising a capsule to at least one gigapascal (GPa) and a method of controlling the press apparatus. The press apparatus comprises a frame for accommodating the capsule and at least four load devices, each securable in relation to the frame and capable of applying variable load onto the capsule in response to control of a first or second variable operating parameter. Measurement mechanisms for measuring the values of first or second operating parameters in respect of each of the load devices are provided. A control mechanism controls each load device according to a set-point for the first or the second operating parameter. The method includes controlling a first of the load devices according to a set-point of the first operating parameter; measuring the second operating parameter in respect of the first load device; and controlling a second of the load devices according to the measured second operating parameter in respect of the first load device.
摘要翻译：用于将胶囊加压至至少一个千兆（GPa）的压制装置和控制该压制装置的方法。压制装置包括用于容纳胶囊的框架和至少四个负载装置，每个装载装置可相对于框架固定，并且能够响应于第一或第二可变操作参数的控制而将可变负载施加到胶囊上。提供了用于测量关于每个负载装置的第一或第二操作参数的值的测量机构。控制机构根据第一或第二操作参数的设定点来控制每个负载装置。该方法包括根据第一操作参数的设定点来控制第一负载装置; 测量关于所述第一负载装置的所述第二操作参数; 以及根据所测量的关于所述第一负载装置的第二操作参数来控制所述负载装置中的第二负载装置。

38. 发明申请

WO2016099738A1 ALUMINA FORMING REFINERY PROCESS TUBES WITH MIXING ELEMENT 审中-公开
标题翻译：用混合元件形成精炼工艺管的铝
公开(公告)号：WO2016099738A1
公开(公告)日：2016-06-23
申请号：PCT/US2015/060897
申请日：2015-11-16
申请人： EXXONMOBIL RESEARCH AND ENGINEERING COMPANY
发明人： CHUN, Changmin , SPICER, David, B.
IPC分类号： B01J19/24 , C10G9/20 , C22C19/05 , C22C38/44 , C23C28/00 , C23C30/00 , F16L9/02 , F28F1/40 , F28F21/08 , B01F5/06 , B23K10/02 , B01J19/00
CPC分类号： B01J19/02 , B01F2005/0636 , B01J3/062 , B01J19/0026 , B01J19/2415 , B01J19/2425 , B01J19/244 , B01J2219/00099 , B01J2219/00117 , B01J2219/00157 , B01J2219/00247 , B01J2219/00252 , B01J2219/00765 , B01J2219/024 , B01J2219/0277 , B23K10/02 , B23K2203/10 , C01B3/34 , C01B2203/0833 , C10G9/203 , C22C19/05 , C22C19/055 , C22C19/056 , C22C30/00 , C22C38/44 , F28D2021/0059 , F28F19/00 , F28F21/08
摘要： This disclosure relates to weldments useful as heat transfer tubes in refinery processes dealing with gas phase hydrocarbon process streams at high temperatures. This disclosure also relates to tubes that are useful in refinery processes dealing with gas phase hydrocarbon process streams at high temperatures. The weldments include a tubular member and at least one mixing element. The tubular member comprises an aluminum-containing alloy. The mixing element comprises an aluminum-containing alloy. The mixing element's aluminum-containing alloy can be the same as or different from the tubular member's aluminum-containing alloy. Other aspects of the disclosure relate to refinery processes dealing with gas phase hydrocarbon process streams at high temperatures which include such weldments.
摘要翻译：本公开涉及用作在高温下处理气相烃工艺流的炼油工艺中的换热管的焊件。本公开还涉及在高温下处理气相烃工艺流的炼油工艺中有用的管。焊件包括管状构件和至少一个混合元件。管状构件包括含铝合金。混合元件包括含铝合金。混合元件的含铝合金可以与管状构件的含铝合金相同或不同。本公开的其它方面涉及在高温下处理包括这种焊件的气相烃工艺流的炼油工艺。

39. 发明申请

WO2016065018A1 POLYCRYSTALLINE DIAMOND-METAL COMPOSITE STRUCTURES AND METHOD OF MANUFACTURE 审中-公开
标题翻译：多晶金刚石金属复合结构及其制造方法
公开(公告)号：WO2016065018A1
公开(公告)日：2016-04-28
申请号：PCT/US2015/056685
申请日：2015-10-21
申请人： SMITH INTERNATIONAL, INC.
发明人： MIDDLEMISS, Stewart
IPC分类号： C23C24/00 , C23C24/08 , E21B10/06 , E21B10/50
CPC分类号： E21B10/5673 , B01J3/062 , B01J2203/062 , B01J2203/0655 , B01J2203/0685 , E21B10/52
摘要： A method of manufacturing a polycrystalline diamond construction includes placing diamond powder in a reaction container, placing a layer of a ceramic powder or an inert metal having a melting temperature greater than 1600°C in powdered form on top of the diamond powder in the reaction container, the layer of the ceramic powder or inert metal powder extending across the entire inner diameter of the reaction container, placing additional diamond powder on top of the layer of ceramic powder or inert metal powder in the reaction container, placing a substrate material into the reaction container on top of the additional diamond powder, and subjecting the reaction container and its contents to high temperature, high pressure sintering conditions.
摘要翻译：制造多晶金刚石结构的方法包括将金刚石粉末放置在反应容器中，将粉末状的熔融温度大于1600℃的陶瓷粉末或惰性金属层放置在反应容器中的金刚石粉末的顶部，陶瓷粉末或惰性金属粉末层延伸穿过反应容器的整个内径，将另外的金刚石粉末放置在反应容器中的陶瓷粉末或惰性金属粉末的顶部上，将基底材料放入反应器容器放置在附加金刚石粉末的顶部，并使反应容器及其内容物经受高温高压烧结条件。

40. 发明申请

WO2015167358A1 METHOD OF OBTAINING A CARBON-BASED COMPOSITE MATERIAL, AND THE COMPOSITE MATERIAL OBTAINED THEREBY 审中-公开
标题翻译：获得基于碳的复合材料的方法及其获得的复合材料
公开(公告)号：WO2015167358A1
公开(公告)日：2015-11-05
申请号：PCT/RU2014/000868
申请日：2014-11-14
申请人： FEDERAL STATE BUDGETARY INSTITUTION "TECHNOLOGICAL INSTITUTE FOR SUPERHARD AND NOVEL CARBON MATERIALS"
发明人： BLANK, Vladimir Davydovich , MORDKOVICH, Vladimir Zal'manovich , OVSYANNIKOV, Danila Alekseevich , PERFILOV, Sergei Alekseevich , POZDNYAKOV, Andrey Anatol'evich , POPOV, Mikhail Yur'evich , PROKHOROV, Vyacheslav Maksimovich
IPC分类号： C04B35/52 , B01J3/06 , C01B31/02 , C04B35/528 , C04B35/581 , C04B35/645 , C04B35/563
CPC分类号： C04B35/645 , B01J3/062 , C01B32/05 , C04B35/52 , C04B35/528 , C04B35/563 , C04B2235/3217 , C04B2235/3821 , C04B2235/3826 , C04B2235/386 , C04B2235/3865 , C04B2235/422 , C04B2235/427 , C04B2235/446 , C04B2235/5248 , C04B2235/5445 , C04B2235/5454 , C04B2235/726 , C04B2235/762 , C04B2235/77 , C04B2235/95 , C04B2235/96 , C04B2235/9607
摘要： The invention relates to composite materials, in particular, to carbon- based composite materials and methods of obtaining thereof, and may be used in aerospace and aviation industries and in processing metals, natural stones or other hard and superhard materials. A method of obtaining a carbon-based composite material is claimed, comprising the exposure of a mixture of a carbon-containing material and a filler to high pressure and temperature, characterized by the addition to the mixture of a sulfur-containing compound, preferably carbon disulfide, with the said exposure being conducted in the temperature range of 600-2000°C and a pressure of 0.1-20 GPa., The material obtained by the above method is characterized with high strength and low density, high hardness (not less than 10 GPa) and high heat resistance in the air.
摘要翻译：本发明涉及复合材料，特别涉及碳基复合材料及其获得方法，并且可用于航空和航空工业以及加工金属，天然石材或其它硬质和超硬材料。一种获得碳基复合材料的方法，包括将含碳材料和填料的混合物暴露于高压和高温下，其特征在于将含硫化合物，优选碳二硫化物，所述曝光在600-2000℃的温度范围和0.1-20GPa的压力下进行。通过上述方法获得的材料的特征在于高强度和低密度，高硬度（不小于 10 GPa）和高耐热性。

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