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21. 发明申请

WO2017173018A1 METHOD OF MAKING MESOPOROUS ZIRCONIUM-BASED MIXED OXIDES 审中-公开
标题翻译：制备介孔氧化锆基混合氧化物的方法
公开(公告)号：WO2017173018A1
公开(公告)日：2017-10-05
申请号：PCT/US2017/024895
申请日：2017-03-30
申请人： PACIFIC INDUSTRIAL DEVELOPMENT CORPORATION
发明人： BORTUN, Anatoly , SHEPARD, David , LI, Yunkui , WU, Wei , LACHAPELLE, Jeffery
IPC分类号： C01G25/00
摘要： Mesoporous, zirconium-based mixed oxides and a method of making the same comprises: injecting a polyvalent metal-containing solution into an electrolyte solution to form a mother liquor; forming a precipitate; aging the precipitate in the mother liquor to form the mixed oxides; washing the mixed oxides with an aqueous medium; drying and collecting the mixed oxides. The pH of the electrolyte solution exceeds the isoelectric point for zirconium-based mixed oxides. The mixed oxides exhibit a single particle size distribution, improved Ce02 reducibility in the presence of Rhodium, a decrease in surface area after calcination (800-1 100°C) that is not more than 55%, and a tetragonal/cubic structure after calcination. After calcination at 1 100°C for 10 hours in air, the mixed oxides exhibit a surface area > 25 m2/g, a pore volume > 0.20 cm3/g, an average pore size > 30 nm, and an average crystallite size between 8 -15 nm.
摘要翻译：中孔锆基混合氧化物及其制备方法包括：将含多价金属的溶液注入电解质溶液中以形成母液; 形成沉淀物; 老化母液中的沉淀物以形成混合氧化物; 用水介质洗涤混合氧化物; 干燥并收集混合氧化物。电解质溶液的pH超过锆基混合氧化物的等电点。混合氧化物表现出单一粒度分布，在铑存在下提高的CeO 2还原性，煅烧后表面积（800-1100℃）不超过55％的降低，以及煅烧后的四方/立方结构。在空气中在1100℃下煅烧10小时后，混合氧化物表现出> 25平方米/克，孔体积> 0.20厘米3 /克，平均孔径> 30纳米，平均晶粒尺寸在8-15纳米之间。

22. 发明申请

WO2014052691A1 A METHOD OF PREPARING AN STT-TYPE ZEOLITE FOR USE AS A CATALYST IN SELECTIVE CATALYTIC REDUCTION REACTIONS 审中-公开
标题翻译：制备用于选择性催化还原反应的催化剂的STT型沸石的方法
公开(公告)号：WO2014052691A1
公开(公告)日：2014-04-03
申请号：PCT/US2013/062075
申请日：2013-09-27
申请人： PACIFIC INDUSTRIAL DEVELOPMENT CORPORATION
发明人： MANCKA, Manjola , LI, Yunkui , LACHAPELLE, Jeffery , WU, Wei
IPC分类号： C01B37/02 , B01D53/94 , B01J29/70 , B01J29/72 , C01B39/02 , C01B39/48
CPC分类号： B01D53/9418 , B01D53/9431 , B01D2255/50 , B01J29/061 , B01J29/70 , B01J29/7049 , B01J29/72 , B01J29/76 , B01J35/002 , B01J37/08 , B01J37/30 , B01J2229/16 , B01J2229/183 , B01J2229/186 , B01J2229/37 , B01J2229/40 , C01B37/02 , C01B39/026 , C01B39/48
摘要： A method of preparing a crystalline STT-type zeolite, which has a mole ratio greater than about 15:1 of an oxide of a tetravalent element to an oxide of a trivalent element, is disclosed along with a gas treatment system that incorporates the STT-type zeolite and a process for treating a gas using the STT-type zeolite. The method generally comprises forming an aqueous reaction mixture comprising a source of an oxide of the tetravalent element, a source of an oxide of the trivalent element, a source of alkali metal, and an organic structure directing agent comprising N,N,N-trimethyl-1-adamantamonium hydroxide; maintaining the aqueous mixture under crystallization conditions sufficient to crystallize crystals of a STT-type zeolite; and recovering the STT-type zeolite crystals The STT-type zeolite crystals exhibit an x-ray diffraction pattern with 2 theta degree peaks at: 8.26, 8.58, 9.28, 9.54, 10.58, 14.52, 15.60, 16.43, 17.13, 17.74, 18.08, 18.46, 19.01, 19.70, 20.12, 20.38, 20.68, 21.10, 21.56, 22.20, 22.50, 22.78, 23.36, 23.76, 23.99, 24.54, 24.92, 25.16, 25.58, 25.80, 26.12, 26.94, 27.38, 27.92, 28.30, 28.60, 29.24, 29.48, 30.08, 30.64, 31.20, 31.46, 31.80, 32.02, 32.60, 33.60, and 34.43.
摘要翻译：公开了一种制备具有四价元素的氧化物与三价元素的氧化物的摩尔比大于约15:1的结晶STT型沸石的方法，其中包含STT-型沸石的气体处理系统，型沸石和使用STT型沸石处理气体的方法。该方法通常包括形成含有四价元素的氧化物源，三价元素的氧化物源，碱金属源和含有N，N，N-三甲基 -1-金刚烷基氢氧化物; 在足以使STT型沸石的晶体结晶的结晶条件下保持含水混合物; 并回收STT型沸石晶体STT型沸石晶体在8.26,8.58,9.28,9.54,10.58,14.52,15.60,16.43,17.13,17.74,18.08，表明具有2θ度峰的X射线衍射图案， 18.46,19.01,19.70,20.12,20.38,20.68，21.10,21.56,22.20,22.50,22.78,23.36,23.76,29.99,24.54,24.92,25.16,25.58,25.80,26.12,26.94,27.38,27.92,28.30,28.60， 29.24,29.48,30.08,30.64,31.20,31.46,31.80,32.02,32.60,3.60和34.43。

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