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11. 发明申请

WO2008115261A1 PREPARATION AND PROVISION OF HIGH ASSAY DECABROMODIPHENYLETHANE 审中-公开
标题翻译：高分析十溴二苯醚的制备与提供
公开(公告)号：WO2008115261A1
公开(公告)日：2008-09-25
申请号：PCT/US2007/076183
申请日：2007-08-17
申请人： ALBEMARLE CORPORATION , HUSSAIN, Saadat , MACK, Arthur, G.
发明人： HUSSAIN, Saadat , MACK, Arthur, G.
IPC分类号： C07C17/12 , C07C25/18 , C08K5/03
CPC分类号： C07C1/26 , C07C17/10 , C07C2529/40 , C08K5/03 , C07C9/00 , C07C19/075
摘要： High assay, reaction-derived decabromodiphenylethane product is prepared by feeding (i) diphenylethane or (ii) partially brominated diphenylethane having an average bromine number less than about two, or (iii) both of (i) and (ii), into the liquid confines of a reaction mixture. Such reaction mixture is (a) formed from components comprised of excess liquid bromine and aluminum-based Lewis acid bromination catalyst, and (b) maintained at one or more elevated reaction temperatures of from about 45°-90°C, and at least when elevated pressure is needed to keep a liquid state in the reaction mixture at the temperature(s) used, the reaction mixture is at such an elevated pressure, whereby arbromination occurs. The feeding is conducted at a rate slow enough to form high assay reaction-derived decabromodiphenylethane product, which is an effective flame retardant.
摘要翻译：通过将（i）二苯基乙烷或（ii）平均溴数小于约2的部分溴化二苯基乙烷或（iii）（i）和（ii）两者的部分溴化二苯基乙烷进料到液体中来制备高分离反应衍生的十溴二苯乙烷产物反应混合物的限制。这种反应混合物是（a）由过量的液体溴和铝基路易斯酸溴化催化剂组成的组分形成的，和（b）保持在一个或多个升高的反应温度为约45℃-90℃，需要提高压力以在所用温度下保持反应混合物中的液体状态，反应混合物处于如此高的压力下，由此发生溴化。以足够慢的速度进行进料以形成高分析反应衍生的十溴二苯乙烷产物，其是有效的阻燃剂。

12. 发明申请

WO2011123389A1 PROCESS FOR PREPARATION OF DOPO-DERIVED COMPOUNDS AND COMPOSITIONS THEREOF 审中-公开
标题翻译：制备DOPO衍生化合物的方法及其组合物
公开(公告)号：WO2011123389A1
公开(公告)日：2011-10-06
申请号：PCT/US2011/030183
申请日：2011-03-28
申请人： ALBEMARLE CORPORATION , YAO, Qiang , MACK, Arthur, G. , JUNZUO, Wang
发明人： YAO, Qiang , MACK, Arthur, G. , JUNZUO, Wang
IPC分类号： C07F9/6571 , C08K5/5313
CPC分类号： C07F9/657163 , B01J27/138 , B01J31/0225 , C07B2200/07 , C07F9/657172 , C07F9/65746 , C08K5/5313
摘要： This invention relates to a process for producing compounds derived from 9,10- Dihydro-9-Oxa-10-Phosphaphenantrene-10-oxide (DOPO). In particular, the invention relates to producing DOPO-derived compounds by reacting DOPO with diol compounds in the presence of a catalyst. This invention also relates to DOPO derived composition containing a high melting point diastereomer. The DOPO derived compounds may be useful as flame-retardants.
摘要翻译：本发明涉及一种生产衍生自9,10-二氢-9-氧杂-10-磷杂蒽-10-氧化物（DOPO）的化合物的方法。特别地，本发明涉及通过在催化剂存在下使DOPO与二醇化合物反应制备DOPO衍生的化合物。本发明还涉及含有高熔点非对映异构体的DOPO衍生组合物。 DOPO衍生的化合物可用作阻燃剂。

13. 发明申请

WO2010127072A1 PELLETIZED LOW MOLECULAR WEIGHT BROMINATED AROMATIC POLYMER COMPOSITIONS 审中-公开
标题翻译：低分子量分子量的芳族聚合物组合物
公开(公告)号：WO2010127072A1
公开(公告)日：2010-11-04
申请号：PCT/US2010/032905
申请日：2010-04-29
申请人： ALBEMARLE CORPORATION , KUMAR, Govindarajulu , MACK, Arthur, G. , LIU, Bo , LAYMAN, William, J. , LUTHER, Douglas, W.
发明人： KUMAR, Govindarajulu , MACK, Arthur, G. , LIU, Bo , LAYMAN, William, J. , LUTHER, Douglas, W.
IPC分类号： C08F6/00 , C08F8/00
CPC分类号： C08F6/28 , C08K5/1345 , C08L23/08 , C08L25/06 , C08L25/18 , C08L2666/04
摘要： Novel polymer compositions of specified formula are converted into pellets of this invention by process technology provided by this invention. By forming a melt blend of a polymer of such polymer compositions together with a modest amount of at least one thermoplastic polymer of at least one monoolefinic monomer having 2-12 carbon atoms per molecule, and converting the melt blend into pellets as described herein, pellets can be formed produce during production, handling, and use, almost no "fines" or air-entrainable dusts. The pellets have an array of additional superior properties and characteristics.
摘要翻译：通过本发明提供的工艺技术将具有特定配方的新型聚合物组合物转化为本发明的颗粒。通过将这种聚合物组合物的聚合物与适量的至少一种至少一种每分子具有2-12个碳原子的单烯属单体的热塑性聚合物一起形成熔体共混物，并将熔融共混物转化成如本文所述的颗粒，将颗粒可以在生产，处理和使用过程中形成产品，几乎没有“细粉”或空气夹带的粉尘。颗粒具有额外的优异性能和特性的阵列。

14. 发明申请

WO2008134733A1 OLIGOMERIC PHOSPHONATE COMPOSITIONS, THEIR PREPARATION AND USES 审中-公开
标题翻译：低分子磷酸盐组合物，其制备和用途
公开(公告)号：WO2008134733A1
公开(公告)日：2008-11-06
申请号：PCT/US2008/062037
申请日：2008-04-30
申请人： ALBEMARLE CORPORATION , MACK, Arthur, G. , TSAO, Techen , SAUER, Anne, M.
发明人： MACK, Arthur, G. , TSAO, Techen , SAUER, Anne, M.
IPC分类号： C07F9/40
CPC分类号： C07F9/4075 , C07F9/4081
摘要： This invention provides oligomeric hydrogen phosphonates represented by the formula (I) where R is an alkyl group having one to about six carbon atoms; R' is a linear or branched hydrocarbylene group or an oxygen-containing hydrocarbylene group having two to about twenty carbon atoms or a hydrocarbylene group having at least one cycloaliphatic or aromatic ring, where at least one of R' is a linear or branched hydrocarbylene group or an oxygen-containing hydrocarbylene group and at least one of R' is a hydrocarbylene group having at least one cycloaliphatic or aromatic ring; and n is a number from 2 to about 20. Also provided are processes for making these oligomeric hydrogen phosphonates, oligomeric organophosphonate compositions, and processes for making these oligomeric organophosphonate compositions.
摘要翻译：本发明提供由式（I）表示的低聚氢膦酸盐，其中R是具有1至约6个碳原子的烷基; R'是具有2至约20个碳原子的直链或支链亚烃基或含氧亚烃基或具有至少一个脂环族或芳族环的亚烃基，其中至少一个R'是直链或支链亚烃基或含氧亚烃基，并且R'中的至少一个是具有至少一个脂环族或芳族环的亚烃基; 并且n是2至约20的数。还提供了制备这些低聚氢膦酸盐，低聚有机膦酸盐组合物的方法以及制备这些低聚有机膦酸盐组合物的方法。

15. 发明申请

WO2007118089A1 FLAME RETARDANT ADDITIVE COMPOSITIONS AND USE THEREOF 审中-公开
标题翻译：阻燃剂添加剂组合物及其用途
公开(公告)号：WO2007118089A1
公开(公告)日：2007-10-18
申请号：PCT/US2007/065879
申请日：2007-04-03
申请人： ALBEMARLE CORPORATION , MACK, Arthur, G. , CHEW, Hoover, B.
发明人： MACK, Arthur, G. , CHEW, Hoover, B.
IPC分类号： C08K5/12 , C08K5/523 , C08K5/5357 , C08L75/00 , C09K21/14 , C08L101/00
CPC分类号： C09K21/12 , C08G18/4607 , C08G2101/0008 , C08K5/12 , C08K5/523 , C08K5/5357
摘要： Improved flame retardant additives are formed from (A) at least one bis(alkanoic acid ester) of a ring-brominated aromatic diester diol; (B) liquid alkylated triphenyl phosphate having an approximate average formula (R x PhO) 3 P=O) in which each R is, independently, a hydrogen atom or a C 14 alkyl group and x is an average number in the range of about 0.2 to 3; and (C) at least one alicyclic phosphonate ester having 1, 2 or 3 phosphorus atoms in the molecule, at least one of which is part of an alicyclic ring system, and having a phosphorus content of at least about 15 wt%. Combinations of these components are well- suited for use in various polymers or resins, especially polyurethanes.
摘要翻译：改进的阻燃添加剂由（A）至少一种环 - 溴化芳族二酯二醇的双（链烷酸酯）形成; （B）具有近似平均式（R x x P Ph）3 P = O的液体烷基化三苯基磷酸酯，其中每个R独立地是氢原子或C 14个烷基，x是约0.2-3的平均数; 和（C）至少一种在分子中具有1,2或3个磷原子的脂环族膦酸酯，其中至少一种是脂环族体系的一部分，并且具有至少约15重量％的磷含量。这些组分的组合非常适用于各种聚合物或树脂，特别是聚氨酯。

16. 发明申请

WO2008118695A1 USE OF LOW TRIPHENYLPHOSPHATE, HIGH PHOSPHOROUS CONTENT ISOPROPYL PHENYL PHOSPHATES AS FLAME RETARDANTS IN RESINS 审中-公开
标题翻译：低三磷酸磷酸盐，高磷酸盐异丙基苯酚磷酸盐作为树脂中的阻燃剂使用
公开(公告)号：WO2008118695A1
公开(公告)日：2008-10-02
申请号：PCT/US2008/057395
申请日：2008-03-19
申请人： ALBEMARLE CORPORATION , LAYMAN, JR., William, J. , MACK, Arthur, G. , TSAO, Techen , APLIN, Jeffrey, T. , LUTHER, Douglas, W.
发明人： LAYMAN, JR., William, J. , MACK, Arthur, G. , TSAO, Techen , APLIN, Jeffrey, T. , LUTHER, Douglas, W.
IPC分类号： C08K5/523 , C08L27/06 , C07F9/12
CPC分类号： C08K5/523 , C07F9/12
摘要： The present invention relates to the use of low triphenyl phosphate, high phosphorous content aryl phosphates with high ortho alkylation as flame retardant compositions.
摘要翻译：本发明涉及具有高邻苯基烷基化作用的低磷酸三苯酯，高含磷芳基磷酸酯作为阻燃剂组合物的用途。

17. 发明申请

WO2008073871A1 ORGANOPHOSPHONATE OLIGOMERS AND MIXTURES THEREOF USEFUL AS FLAME RETARDANTS 审中-公开
标题翻译：有机磷酸酯低聚物及其混合物有用于阻燃剂
公开(公告)号：WO2008073871A1
公开(公告)日：2008-06-19
申请号：PCT/US2007/086932
申请日：2007-12-10
申请人： ALBEMARLE CORPORATION , SAUER, Anne, M. , MACK, Arthur, G. , TSAO, Techen , APLIN, Jeffrey, Todd
发明人： SAUER, Anne, M. , MACK, Arthur, G. , TSAO, Techen , APLIN, Jeffrey, Todd
IPC分类号： C07F9/38 , C07F9/40 , C08K5/5317 , C08K5/5333 , C08G18/38
CPC分类号： C08G79/04 , C07F9/4075 , C08G18/4829 , C08G2101/0008 , C08K5/5333 , C08L75/04 , C08L2666/22
摘要： Organophosphonate oligomers, and mixtures thereof, useful as flame retardants.
摘要翻译：有机膦酸酯低聚物及其混合物，可用作阻燃剂。

18. 发明申请

WO2008011477A2 PROCESS TECHNOLOGY FOR RECOVERING BROMINATED STYRENIC POLYMERS FROM REACTION MIXTURES IN WHICH THEY ARE FORMED AND/OR CONVERTING SUCH MIXTURES INTO PELLETS OR INTO GRANULES OR PASTILLES 审中-公开
标题翻译：从反应混合物中回收溴化的聚苯乙烯聚合物的工艺技术，在这些反应混合物中形成和/或将这种混合物转化为球形或颗粒或浆料
公开(公告)号：WO2008011477A2
公开(公告)日：2008-01-24
申请号：PCT/US2007/073805
申请日：2007-07-18
申请人： ALBEMARLE CORPORATION , KOLICH, Charles, H. , BALHOFF, John, F. , LUTHER, Douglas, W. , HERNDON, Jr., Robert, C. , LIN, Ronny, W. , PETERS, Bruce, C. , MACK, Arthur, G. , LEE, David, A.
发明人： KOLICH, Charles, H. , BALHOFF, John, F. , LUTHER, Douglas, W. , HERNDON, Jr., Robert, C. , LIN, Ronny, W. , PETERS, Bruce, C. , MACK, Arthur, G. , LEE, David, A.
CPC分类号： C08F6/02 , B29C47/0004 , B29C47/0011 , B29C47/30 , B29C47/38 , B29C47/765 , B29C47/92 , B29C2947/92514 , B29C2947/92704 , C08F6/001 , C08F8/20 , Y10T428/2982 , C08L25/18 , C08F12/08
摘要： Brominated styrenic polymer is recovered from solution in a vaporizable solvent by converting the solution in a devolatilization extruder into a brominated styrenic polymer melt or flow and a separate vapor phase comprised predominately of vaporizable solvent, recovering the melt or flow from the devolatilization extruder, and allowing or causing the melt or flow to solidify. The solidified brominated styrenic polymer can be subdivided into a powder or pelletized form. Pellets so made have improved hardness and/or crush strength properties along with reduced formation of fines. Brominated anionic styrenic polymer is preferably used in the process.
摘要翻译：通过将脱挥发分挤出机中的溶液转化成溴化苯乙烯类聚合物熔体或流动物和单独的气相主要包含可蒸发溶剂，从溶剂中回收溴化苯乙烯类聚合物，回收熔融物或从脱挥发分挤出机流出，并使熔体或流动固化。固化的溴化苯乙烯聚合物可以细分成粉末或颗粒形式。如此制成的粒料具有改善的硬度和/或抗碎强度性能以及减少的细粒形成。溴化阴离子苯乙烯聚合物优选用于该方法中。

19. 发明申请

WO2005023927A1 FLAME RETARDANTS WITH HIGH HALOGEN CONTENT AND LOW VISCOSITY 审中-公开
标题翻译：具有高含量和低粘度的阻燃剂
公开(公告)号：WO2005023927A1
公开(公告)日：2005-03-17
申请号：PCT/US2004/026826
申请日：2004-08-19
申请人： ALBEMARLE CORPORATION , FESKE, Elbert, F. , CLARK, Nelson, E. , MACK, Arthur, G. , APLIN, Jeffrey, Todd
发明人： FESKE, Elbert, F. , CLARK, Nelson, E. , MACK, Arthur, G. , APLIN, Jeffrey, Todd
IPC分类号： C08K5/12
CPC分类号： C08K5/1539 , C08G2101/00 , C08K5/0066 , C08K5/053 , C08K5/11 , C08K5/1515
摘要： A flame retardant formulation which is the combination of at least (1) at least one bromine-containing polyol flame retardant formed from the reaction of (a) tetrabromophthalic anhydride, (b) an aliphatic polyol, and (c) an epoxide, and (2) at least one aliphatic diester of an alkane dicarboxylic acid, with the proviso that the formulation has a viscosity at 25°C of about 20,000 cps or less, and a bromine content of at least about 40 wt%. A flame retardant compound formed from A) tetrabromophthalic anhydride; B) diethylene glycol; C) at least one alpha-omega alkane diol, or at least one alpha-omega alkane diol and at least one aliphatic monool; and D) at least one alkylene oxide; with the proviso that the compound has a viscosity at 25°C of about 60,000 cps or less, and a bromine content of at least about 43 wt%. Polymer compositions formed from (a) a polyurethane or a polyisocyanurate and (b) a formulation of the invention. One process to make a formulation involves heating a mixture of (a), (b), and at least one liquid aliphatic diester of a alkane dicarboxylic acid to form an intermediate composition; and then the intermediate is contacted one or more times with (c) thereby producing the formulation. Optionally, excess (c) is removed.
摘要翻译：阻燃剂组合物，其是由（a）四溴邻苯二甲酸酐，（b）脂族多元醇和（c）环氧化物的反应形成的至少（1）至少一种含溴多元醇阻燃剂和（c） 2）烷烃二羧酸的至少一种脂族二酯，条件是制剂在25℃下的粘度为约20,000cps或更低，溴含量为至少约40重量％。由A）四溴邻苯二甲酸酐形成的阻燃化合物; B）二甘醇; C）至少一种α-ω链烷二醇，或至少一种α-ω链烷二醇和至少一种脂族一元醇; 和D）至少一种环氧烷; 条件是该化合物在25℃下的粘度为约60,000cps或更低，溴含量为至少约43重量％。由（a）聚氨酯或聚异氰尿酸酯和（b）本发明的制剂形成的聚合物组合物。制备制剂的一个方法包括加热（a），（b）和至少一种烷烃二羧酸的液体脂族二酯的混合物以形成中间体组合物; 然后将中间体与（c）一次或多次接触，从而制备制剂。任选地，除去过量（c）。

20. 发明申请

WO2014179688A1 BUTADIEN2,3-DIYL LINKED DI-DOPO DERIVATIVES AS FLAME RETARDANTS 审中-公开
标题翻译：丁二烯-2,3-二氢吲哚衍生物作为阻燃剂
公开(公告)号：WO2014179688A1
公开(公告)日：2014-11-06
申请号：PCT/US2014/036579
申请日：2014-05-02
申请人： ALBEMARLE CORPORATION , ANGELL, Scott, Edward , WHITE, Kimberly, A. , ANGLELL, Yu, Li , MACK, Arthur, G.
发明人： ANGELL, Scott, Edward , WHITE, Kimberly, A. , ANGLELL, Yu, Li , MACK, Arthur, G.
IPC分类号： C07F9/6571 , A62D1/00 , C09K21/12 , C08K5/5313
CPC分类号： C07F9/657172 , C08K5/5313 , C09K21/12
摘要： Disclosed are novel, halogen-free flame-retardants derived from 9,10-Dihydro-9-Oxa-10-Phosphaphenantrene-10-oxide (DOPO) of the structure below: This invention also relates to the use of the halogen free DOPO derived compositions as flame-retardants in polymers, and a process of preparing the above compounds by reacting a formula A compound with a formula B compound:
摘要翻译：公开了衍生自以下结构的9,10-二氢-9-氧杂-10-磷杂蒽-10-氧化物（DOPO）的新型无卤素阻燃剂：本发明还涉及使用无卤素的DOPO衍生物组合物作为聚合物中的阻燃剂，以及通过使式A化合物与式B化合物反应来制备上述化合物的方法：

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