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121. 发明申请

WO99051561A1 NEW PROCESSES FOR THE PREPARATION OF 3-BROMOANISOLE AND 3-BROMONITROBENZENE 审中-公开
标题翻译：制备三硼和三溴代苯并噻吩的新工艺
公开(公告)号：WO99051561A1
公开(公告)日：1999-10-14
申请号：PCT/IL1999/000161
申请日：1999-03-22
IPC分类号： C07C41/01 , C07C43/225 , C07C201/12 , C07C205/12
CPC分类号： C07C41/01 , C07C201/12 , C07C205/12 , C07C43/225
摘要： Process for the preparation of 3-bromoanisole comprising methoxydenitrating 3-bromonitrobenzene in the presence of a phase-transfer catalyst (PTC), and the preparation of 3-bromonitrobenzene by the bromination of nitrobenzene with bromine in oleum. The methoxydenitration reagent is an alkali metal methoxide, which is selected from sodium methoxide and potassium methoxide. The amount of methoxide used is 1-1.5 mol per mol of 3-bromonitrobenzene. The alkali methoxide can be a pre-prepared solid or it can be prepared in situ, by the reaction of the corresponding alkali hydroxide and methanol. In the case when pre-prepared solid methoxide is used, the effective amount of alkali hydroxide is between 1.2-1.7 mol per mol of 3-bromonitrobenzene. The reaction temperatures are between about 40 to 80 DEG C, with preference to reaction temperatures of 50 to 55 DEG C. In the case in which methoxide is prepared in situ, the effective amount of alkali hydroxide is between 2.2-2.4 mol per mol of 3-bromonitrobenzene. The reaction temperatures are between about 50 to 80 DEG C with preference to reaction temperatures of 55 to 65 DEG C.
摘要翻译：在相转移催化剂（PTC）的存在下，制备3-溴苯甲醚的方法，其中包括使3-溴硝基苯甲氧基过氧化，通过在发烟硫酸中用溴溴化硝基苯来制备3-溴硝基苯。甲氧基浓缩试剂是碱金属甲醇钠，其选自甲醇钠和甲醇钾。所用的甲氧化物的量为每摩尔3-溴硝基苯为1-1.5摩尔。碱金属甲醇盐可以是预制的固体，也可以通过相应的碱金属氢氧化物和甲醇的反应在原位制备。在使用预制的固体甲醇钠的情况下，碱金属氢氧化物的有效量为每摩尔3-溴硝基苯1.2-1.7摩尔。反应温度在约40至80℃之间，优选反应温度为50至55℃。在原位制备甲醇盐的情况下，碱金属氢氧化物的有效量为每摩尔2.2-2.4摩尔 3溴硝基苯。反应温度在约50至80℃之间，优选的反应温度为55至65℃。

122. 发明申请

WO99023074A1 FLUORINATED NAPHTHALENE DERIVATIVES AND THEIR USE IN LIQUID CRYSTAL MIXTURES 审中-公开
标题翻译：氟化萘衍生物和它们在的液晶混合物
公开(公告)号：WO99023074A1
公开(公告)日：1999-05-14
申请号：PCT/EP1998/006938
申请日：1998-11-03
IPC分类号： C07C43/225 , C07C69/017 , C07C69/63 , C07C69/75 , C07D213/30 , C07D213/64 , C07D239/34 , C07D405/12 , C07F7/08 , C09K19/32 , C09K19/34 , C09K19/40 , C07C69/635
CPC分类号： C07D213/30 , C07C43/225 , C07C69/017 , C07C69/63 , C07C69/75 , C07C2602/10 , C07D213/64 , C07D239/34 , C07D405/12 , C07F7/0812 , C07F7/0818 , C09K19/322 , C09K19/3444 , C09K19/3458 , C09K19/3466 , C09K19/3469 , C09K19/406 , C09K2019/325 , Y10T428/10
摘要： The invention relates to fluorinated naphthalene derivatives of formula (I) R (-A -M )a(-A -M )b-B(-M -A )c(-M -A )d-R , wherein B is (II) having the meaning (III), (IV) or (V) or is (VI) and R (-A -M )a(-A -M ) and (-M -A )(-M -A )R stand for mesogene radicals. Said derivatives can be used as constituents for liquid crystal mixtures, more particularly for ferroelectric liquid crystal mixtures.
摘要翻译：（ - A <1> -M <1>）一个（-A <2> -M <2>）BB（-M <3> -A <3的式（I）中，R <1>的氟化萘衍生物 >）C（-M <4> -A <4>）的dR <2>，其中B（II），（III的含义），（IV），（V）或（VI），并且R <1 >（ - A <1> -M <1>）一个（-A <2> -M <2>）和（-M <3> -A <3>）（ - 中号<4> -A <4> ）R <2>介晶残基是适合作为组分，尤其是铁电液晶的混合物。

123. 发明申请

WO99019420A2 5-ARYLINDANE DERIVATIVES AND FERROELECTRIC LIQUID CRYSTAL MIXTURE CONTAINING SAME 审中-公开
标题翻译：衍生物5 ARYLINDANE与混合液晶铁电含其
公开(公告)号：WO99019420A2
公开(公告)日：1999-04-22
申请号：PCT/EP1998/006415
申请日：1998-10-08
IPC分类号： G02F1/13 , C07C25/22 , C07C25/24 , C07C43/225 , C07D213/02 , C07D239/02 , C07D239/26 , C09K19/02 , C09K19/32 , C09K19/34 , C09K19/42
CPC分类号： C07D239/26 , C07C25/22 , C07C25/24 , C07C43/225 , C07C2602/08 , C09K19/0225 , C09K19/32 , C09K19/34 , C09K19/3444 , C09K19/42 , C09K2019/327 , Y10T428/10
摘要： A ferroelectric liquid crystal mixture, especially useful for operation in the tau Vmin-mode, comprises a 5-Arylindane derivative of formula (I), wherein Y is CH, CF or N and R (-A -M )a(-A -M )b-, (M -A -)cR are mesogenic groups.
摘要翻译：本发明涉及5-芳基茚满衍生物和含有它的铁电液晶混合物。铁电液晶，在模式的tau Vmin-操作特别有用的混合物包含式（I）的5- arylindane的衍生物; 在式Y表示CH，CF或N和R <1>（ - A <1> -M <1>）一个（-A <2> -M <2>），B（M <3> -A 3） - ）cR 2是介晶基团。

124. 发明申请

WO98050438A1 CHLORIDE LINKER FOR SOLID PHASE ORGANIC SYNTHESIS 审中-公开
标题翻译：用于固相有机合成的氯化物连接器
公开(公告)号：WO98050438A1
公开(公告)日：1998-11-12
申请号：PCT/US1998/009485
申请日：1998-05-08
IPC分类号： C07B61/00 , C07C43/225 , C07C235/06 , C08F8/18 , C08G85/00 , C08F12/08 , C08F112/08 , C08F212/08
CPC分类号： C08F8/18
摘要： This invention relates to a linker for use in solid phase synthesis, its preparation and methods of use. The linker consists essentially of an alkoxy substituted phenyl ring bearing an optionally substituted benzylic chloride. Synthetic components bearing a suitable nucleophile can displace the chlorine atom and form a covalent linkage to the support.
摘要翻译：本发明涉及用于固相合成的接头，其制备方法和使用方法。接头基本上由带有任选取代的苄基氯的烷氧基取代的苯基环组成。具有合适亲核试剂的合成组分可以置换氯原子并与载体形成共价键。

125. 发明申请

WO98035924A1 LIQUID-CRYSTALLINE COMPOUNDS HAVING BICYCLO[1.1.1]PENTANE STRUCTURE, LIQUID-CRYSTAL COMPOSITION, AND LIQUID-CRYSTAL DISPLAY ELEMENT 审中-公开
标题翻译：具有双相结构的液晶化合物[1.1.1] PENTANE结构，液晶组合物和液晶显示元件
公开(公告)号：WO98035924A1
公开(公告)日：1998-08-20
申请号：PCT/JP1998/000602
申请日：1998-02-13
IPC分类号： C07C17/00 , C07C17/26 , C07C17/269 , C07C22/08 , C07C25/18 , C07C25/24 , C07C43/18 , C07C43/184 , C07C43/188 , C07C43/192 , C07C43/225 , C07C45/51 , C07C69/753 , C07C69/757 , C07C69/76 , C09K19/32 , C07C13/36 , C07C25/22 , C07C49/115 , C07C49/215 , C07C69/773 , C07C255/45 , C07C255/50 , C07D239/26 , C07F7/12 , C09K19/42 , G02F1/13
CPC分类号： C07C17/00 , C07C17/263 , C07C17/269 , C07C22/08 , C07C25/18 , C07C25/24 , C07C43/18 , C07C43/184 , C07C43/188 , C07C43/192 , C07C43/225 , C07C45/513 , C07C45/515 , C07C69/753 , C07C69/757 , C07C69/76 , C09K19/32 , C07C23/24 , C07C47/34 , C07C49/417
摘要： Novel liquid-crystalline compounds which can impart desirable properties to liquid-crystal compositions mainly for use in the TFT, STN, and TN display systems, in particular liquid-crystalline compounds having excellent compatibility at low temperatures, capable of low-voltage operation or high-speed response in various display systems according to substituent selection, capable of giving a highly reliable liquid-crystal composition and having a bicyclo[1.1.1]pentane structure represented by general formula (1), a liquid-crystal composition containing the same; and a liquid-crystal display element prepared from the composition.
摘要翻译：可以为主要用于TFT，STN和TN显示系统的液晶组合物提供理想的性能的新型液晶化合物，特别是能够在低温下具有优异的相容性，能够低电压操作或高的液晶化合物根据取代基选择的各种显示系统中的速度响应，能够得到高度可靠的液晶组合物并具有由通式（1）表示的双环[1.1.1]戊烷结构，含有它们的液晶组合物; 和由该组合物制备的液晶显示元件。

126. 发明申请

WO1997037960A1 'alpha','alpha'-DIFLUOROBENZYL ETHER DERIVATIVES, LIQUID CRYSTAL COMPOSITIONS, AND LIQUID CRYSTAL DISPLAY DEVICES 审中-公开
标题翻译： α，α-二氟硼烷醚衍生物，液晶组合物和液晶显示装置
公开(公告)号：WO1997037960A1
公开(公告)日：1997-10-16
申请号：PCT/JP1997001214
申请日：1997-04-09
申请人： CHISSO CORPORATION , MATSUI, Shuichi , KOIZUMI, Yasuyuki , MIYAZAWA, Kazutoshi , SEKIGUCHI, Yasuko , NAKAGAWA, Etsuo
发明人： CHISSO CORPORATION
IPC分类号： C07C43/225
CPC分类号： C07C255/54 , C07C43/225 , C07C255/50 , C07C255/57 , C07C2601/14 , C09K19/3066
摘要： Liquid crystal compounds of general formula (1) which have a low threshold voltage and a low viscosity, keep or lower the dielectric anisotropy when added to liquid crystal compositions, and are excellent in compatibility with other liquid crystal compounds particularly at low temperature; liquid crystal compositions containing the compounds; and liquid crystal display devices made by using the compositions. In said formula R is alkyl or the like; A and B are each 1,4-cyclohexylene or the like; C and D are each 1,4-phenylene or the like; Z , Z and Z are each -CH2CH2- or the like; X is halogeno or the like; Y is hydrogen or halogeno; and 1 and m are each 0 to 1, with the proviso that 1 and m must satisfy the relationship: 1 + m
摘要翻译：具有低阈值电压和低粘度的通式（1）的液晶化合物在添加到液晶组合物时保持或降低介电各向异性，并且与其它液晶化合物，特别是在低温下的相容性优异; 含有这些化合物的液晶组合物; 以及使用该组合物制成的液晶显示装置。在所述式中，R 1是烷基等; A和B各自为1,4-亚环己基等; C和D各自为1,4-亚苯基等; Z 1，Z 2和Z 3各自为-CH 2 CH 2 - 等; X是卤代等; Y是氢或卤素; 且1和m各自为0至1，条件是1和m必须满足关系：1 + m 1。

127. 发明申请

WO1995009827A1 3,4-DIFLUOROBENZENES AND THEIR USE IN LIQUID-CRYSTAL MIXTURES 审中-公开
标题翻译： 3,4-二氟苯及它们在的液晶混合物
公开(公告)号：WO1995009827A1
公开(公告)日：1995-04-13
申请号：PCT/EP1994003125
申请日：1994-09-19
申请人： MERCK PATENT GMBH , SCHLOSSER, Hubert , JUNGBAUER, Dietmar
发明人： MERCK PATENT GMBH
IPC分类号： C07C43/225
CPC分类号： C09K19/3066 , C07C43/225 , C07C2601/14 , C09K19/0403 , C09K2019/0407
摘要： Described are 3,4-difluorobenzenes of formula (I) in which the symbols and indices have the following meanings: R is H, a straight-chain or branched-chain alkyl (with or without an asymmetric C-atom) with 1 to 15 C-atoms, whereby one or two non-adjacent -CH2- groups may be replaced by -O-, -CH=CH-, -CC-, cyclopropane-1,2-diyl or -Si(CH3)2- and one or more H-Atoms in the alkyl group may be substituted by F; A , A and A which may be the same or different, are 1,4-phenylene, pyridine-2,5-diyl, pyrimidine-2,5-diyl in which one or more H-atoms may be replaced by F, trans 1,4-cyclohexylene, 1,3-dioxane-2,5-diyl or naphthalene-2,6-diyl; M and M , which may be the same or different, are -CH2CH2-, -CH=CH-, -CC-, -CH2CH2CH2CH2-, -CH2CH2CH2-O-, -O-CH2CH2CH2-, -CH2CH2-CO-O-, -O-CO-CH2CH2-, -CH2-O-, -O-CH2, -CO-O- or -O-CO-; X is -CH2-O- or -O-CH2-; k, l, m, n, o and p are zero or one, under the condition that k+m+o is greater than zero. The compounds described have particularly low melting points. In mixtures, they improve the properties e.g. reducing the glass-transition temperature. This makes for a low viscosity and a low temperature dependence of the viscosity.
摘要翻译：（I），其中符号和指数具有以下含义的式3,4-二氟苯衍生物，R <1>为H，直链或支链（具有或不具有不对称碳原子），具有1至15个碳原子，其中烷基被-O - ， - CH CH - ， - CC-，环丙烷-1,2-二基或-Si（CH 3）2 =一个或两个非相邻-CH 2 - 基团可以被取代，并且其中一个或多个所述烷基可被F取代的H原子; A <1>，A <2>，A <3>相同或不同的1,4-亚苯基，吡啶-2,5-二基，嘧啶-2,5-二基，其中一个或两个H原子被F取代可更换，反式-1,4-亚环己基，1,3-二恶烷-2,5-二基或萘-2,6-二基; 中号<1>中，M <2>是相同的或不同的-CH 2 CH 2 - ， - CH = CH - ， - CC-，-CH2CH2CH2CH2-，-CH2CH2CH2 - ， - O-CH 2 CH 2，-CH 2 CH 2 CO-O- ，-O-CO-CH 2 CH 2 -CH 2 -O-，-O-CH 2 - ， - CO-O-或-O-CO-; X是-CH2-O-或-O-CH 2 - ; K，L，M，N，O，P是0或1，条件是K + M + O的总和是大于零。该新型物质通过特别低的熔点表征。在混合物中，它们具有有利的效果，例如降低玻璃化转变温度。这是一个低粘度和它们的低温度依赖性良好。

128. 发明申请

WO9103445A3 HALOGENATED BENZENE DERIVATIVES AND LIQUID CRYSTALLINE MEDIUM 审中-公开
标题翻译：卤代苯衍生物和液晶介质
公开(公告)号：WO9103445A3
公开(公告)日：1991-04-18
申请号：PCT/EP9001437
申请日：1990-08-30
申请人： MERCK PATENT GMBH
发明人： HITTICH REINHARD , POETSCH EIKE , REIFFENRATH VOLKER , RIEGER BERNHARD , WAECHTLER ANDREAS , COATES DAVID , PLACH HERBERT
IPC分类号： G02F1/13 , C07C22/08 , C07C25/18 , C07C43/225 , C07C255/50 , C09K19/30 , C09K19/42 , C07C22/04
CPC分类号： C09K19/3028 , C07C22/08 , C07C25/18 , C07C43/225 , C07C255/50 , C07C2601/14 , C09K19/3003 , C09K2019/3021
摘要： New halogenated benzene derivatives of formula (I), where n is 1 to 7, the rings A and B each stand for trans-1,4-cyclohexylene, or one of the rings A and B also stands for 1,4-phenylene or 3-fluor-1,4-phenylene, X F, Cl, -CHF2, -CF3, -CN, -OCF3 or -OCHF2, Y and Z each independently stand for H or F, r = 1 or, if s = 1, B = trans-1,4-cyclohexylene and simultaneously X = -CHF2, -CF3, -OCF3 or -OCHF2 and r = 0, and s = 1 or, if B = 1,4-phenylene or 3-fluor-1,4-phenylene, s = 0.
摘要翻译：本发明涉及式I的新型卤代苯衍生物，其中n为1至7，环A和B各自为反式-1,4-亚环己基或环A和B之一或者是1,4-亚苯基或3-氟-1,4-亚苯基，X是F，Cl，CHF 2，-CF 3，-CN，-OCF 3或-OCHF 2，Y和Z各自彼此独立地是H 或F，r = 1，或者在s = 1的情况下，B =反式-1,4-亚环己基并且同时X = -CHF 2，-CF 3，-OCF 3或-OCHF 2，r是0或s = 1 或者在B = 1,4-亚苯基或3-氟-1,4-亚苯基的情况下，s = 0。

129. 发明申请

WO8905288A3 COMPLETE ETHER CAPPING OF OLIGOMERIC POLYPHENOLS 审中-公开
标题翻译：低聚多元酚的完全封端
公开(公告)号：WO8905288A3
公开(公告)日：1989-08-10
申请号：PCT/US8804140
申请日：1988-11-21
申请人： ALLIED SIGNAL INC
发明人： ZWEIG ANDREW M , CONRAD JEFFREY P
IPC分类号： C07C41/16 , C07C41/38 , C07C43/20 , C07C43/215 , C07C43/225 , H05K1/03 , C07C43/205 , C07C43/21
CPC分类号： C07C41/16 , C07C41/38 , H05K1/0326 , Y10S525/934 , C07C43/215
摘要： A method is presented to prepare totally functionalized ethercapped oligomeric polyphenols without molecular weight fractionation. The products generally are very low in inorganic salts and are characterized by the absence of volatiles leading to void formation in their subsequent curing. The success of the method rests upon conducting the reaction under totally homogenenous conditions throughout.
摘要翻译：提出了一种制备完全官能化的不含分子量分馏的醚封端的低聚多酚的方法。这些产品通常非常低的无机盐，其特征在于不存在挥发性物质，从而导致其随后固化时形成空隙。该方法的成功在于始终在完全均匀的条件下进行反应。

130. 发明申请

WO8705291A3 LIQUID CRYSTAL COMPOUNDS,MIXTURES AND DEVICES 审中-公开
标题翻译：液晶化合物，混合物和装置
公开(公告)号：WO8705291A3
公开(公告)日：1988-02-11
申请号：PCT/GB8700132
申请日：1987-02-20
申请人： SECR DEFENCE BRIT , SHANGHAI INST ORGANIC CHEM
发明人： GRAY GEORGE WILLIAM , LACEY DAVID , TOYNE KENNETH JOHNSON , SCROWSTON RICHARD MICHAEL , HOLMES DAVID , BRADSHAW MADELINE JOAN , SAMRA ANERJIT , HONG JUN SHANGHAI
IPC分类号： C07C1/32 , C07C43/225 , C07C67/00 , C07C69/612 , C07C69/65 , C07C69/734 , C07C69/86 , C07C69/90 , C07C69/92 , C07C69/94 , C07C241/00 , C07C251/24 , C07D239/26 , C07D239/28 , C07D239/34 , C07D239/42 , C09K19/12 , C09K19/20 , C09K19/22 , C09K19/24 , C09K19/26 , C09K19/30 , C09K19/34 , C09K19/46 , G02F1/13
CPC分类号： C07D239/26 , C07C1/326 , C07C255/00 , C09K19/0225 , C09K19/126 , C09K19/2028 , C09K19/3003 , C09K19/3402 , C09K19/3441 , C09K19/3444 , C09K19/3463 , C09K19/3475 , C07C13/28
摘要： Novel compounds suitable for inclusion in a ferroelectric smectic liquid crystal mixture, having formula (I), where the rings are independently phenyl, cyclohexyl or pyrimidyl, n is 0 or 1, m is 1, 2 or 3 (m + n is 1, 2 or 3), A, B, D, E are independently H or F, Z is a linking group or a single bond, R1 is alkyl or alkoxy, R2 is optically alkyl (n=0) or -COOR3 CH(CH3) COOR4 where R3 is optically active alkyl and R4 is n-alkyl (n=1), and a is 1 or 2. Ferroelectric smectic mixtures containing these compounds preferably in a non-optically active or racemic form aree described. Preferably each of the rings is phenyl.

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