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1. 发明公开

US20240235147A1 POTASSIUM DIHYDROGEN PHOSPHATE (KDP) FREQUENCY-DOUBLING CRYSTAL STRUCTURE 审中-公开
公开(公告)号：US20240235147A1
公开(公告)日：2024-07-11
申请号：US18395975
申请日：2023-12-26
申请人： Tianshui Normal University
发明人： Weijun LING , Jinfang YANG , Mingxia ZHANG , Yongle ZHU , Yuping WANG , Feiping LU , Xiangbing LI , Limin ZHAO , Yuxiang ZHAO , Lijun ZHANG , Zhong DONG
IPC分类号： H01S3/109 , C30B29/14 , G02F1/37 , H01S3/08
CPC分类号： H01S3/109 , C30B29/14 , G02F1/37 , H01S3/08054
摘要： The present disclosure provides a potassium dihydrogen phosphate (KDP) frequency-doubling crystal structure, including a crystal fixing structure, a KDP crystal, a π polarization tube, and a σ polarization tube; where a π-polarized laser with a central wavelength of 800 nm enters the KDP crystal through the π polarization tube, and the KDP crystal converts the π-polarized laser with a central wavelength of 800 nm into a σ-polarized laser with a central wavelength of 400 nm by frequency doubling and then outputs the σ-polarized laser from the σ polarization tube. Close end bevels of the π polarization tube and the σ polarization tube are designed into a Brewster angle. The KDP crystal is placed in a vacuum-sealed cavity formed by the π polarization tube, the σ polarization tube, and the crystal fixing structure, which eliminates a complicated process of crystal coating and prevents the KDP crystal from deliquescing in air.

2. 发明申请

US20190144291A1 ZEOLITE COMPOSITIONS AND METHODS FOR TAILORING ZEOLITE CRYSTAL HABITS WITH GROWTH MODIFIERS 审中-公开
公开(公告)号：US20190144291A1
公开(公告)日：2019-05-16
申请号：US16183862
申请日：2018-11-08
申请人： University of Houston System
发明人： Jeffrey D. Rimer , Manjesh Kumar
IPC分类号： C01B39/54 , B01J29/70 , B01J47/00 , C30B7/14 , C30B29/14 , C01B39/04 , C30B29/34
CPC分类号： C01B39/54 , B01J29/035 , B01J29/06 , B01J29/7015 , B01J29/85 , B01J35/002 , B01J35/0033 , B01J35/023 , B01J47/00 , B01J2229/62 , C01B39/04 , C01P2004/03 , C01P2004/20 , C01P2004/38 , C01P2004/60 , C30B7/14 , C30B29/14 , C30B29/34 , C30B29/60
摘要： Embodiments of the invention generally provide compositions of crystalline zeolite materials with tailored crystal habits and the methods for forming such crystalline zeolite materials. The methods for forming the crystalline zeolite materials include binding one or more zeolite growth modifiers (ZGMs) to the surface of a zeolite crystal, which results in the modification of crystal growth rates along different crystallographic directions, leading to the formation of zeolites having a tailored crystal habit. The improved properties enabled by the tailored crystal habit include a minimized crystal thickness, a shortened internal diffusion pathlength, and a greater step density as compared to a zeolite having the native crystal habit prepared by traditional processes. The tailored crystal habit provides the crystalline zeolite materials with an aspect ratio of about 4 or greater and crystal surfaces having a step density of about 25 steps/μm2 or greater.

3. 发明授权

US10240252B2 Epitaxial quartz homeotypes crystal growth on beta quartz for pressure sensors and accelerometers 有权
公开(公告)号：US10240252B2
公开(公告)日：2019-03-26
申请号：US15530412
申请日：2017-01-10
申请人： Daniel Smith
发明人： Daniel Smith
IPC分类号： C30B19/12 , C30B19/08 , C30B7/10 , C30B19/02 , C30B25/18 , C30B29/18 , C30B29/14 , C30B29/22 , C30B23/02 , H01L41/187 , H01L41/316 , H01L41/317
摘要： The purpose of quartz homeotypes grown epitaxially on beta quartz for use in pressure sensors or accelerometers is to be able to drastically cut down production costs on otherwise expensive or time-consuming to grow crystals that are necessary in various industrial applications. This is done via epitaxial growth of quartz homeotypes across the whole surface of a sample of beta quartz, an easily accessible and high temperature capable crystal. This invention also applies to the epitaxial application of piezoelectric material atop a piezoelectric crystal for the purpose of altering its piezoelectric coefficient and the epitaxial application of a piezoelectric crystal atop a host crystal for the purpose of increasing its insulation resistance.

4. 发明授权

US09957162B2 Ternary inorganic compound crystal and preparation method and application thereof 有权
公开(公告)号：US09957162B2
公开(公告)日：2018-05-01
申请号：US15188964
申请日：2016-06-21
申请人： SHENZHEN UNIVERSITY
发明人： Feng Xing , Ning Zhang , Zhu Ding , Biao Liu , Ningxu Han , Weilun Wang , Dawang Li , Wujian Long , Biqin Dong , Xiaodong Wang
IPC分类号： C01B25/45 , C04B35/624 , C30B1/02 , C30B29/14 , C30B29/22 , C04B35/447 , C04B28/02 , C04B35/645 , C30B1/04 , C30B1/10 , C04B103/44
CPC分类号： C01B25/45 , C01B25/32 , C01B25/34 , C01B37/065 , C04B12/02 , C04B28/02 , C04B35/447 , C04B35/624 , C04B35/6455 , C04B2103/445 , C04B2235/3208 , C04B2235/3217 , C04B2235/447 , C04B2235/6567 , C04B2235/661 , C30B1/02 , C30B1/04 , C30B1/10 , C30B29/14 , C30B29/22 , C04B22/16 , C04B18/023
摘要： Provided is a ternary inorganic compound crystal having a molecular formula of Ca8Al12P2O31, and a preparation method thereof comprising the following steps: weighing calcium salts, aluminum salts and phosphate respectively according to the molar ratio of calcium, aluminum and phosphorus in the molecular formula Ca8Al12P2O31; calcining at 1550˜1570° C., cooling, and grinding to obtain the ternary inorganic compound crystal. Also provided is an application of the ternary inorganic compound in gelling materials and molecular sieves, nonlinear optical crystals, and photochromic materials.

5. 发明授权

US09909229B2 Rubidium uranium fluoride-based crystals and methods of fabrication 有权
公开(公告)号：US09909229B2
公开(公告)日：2018-03-06
申请号：US15077317
申请日：2016-03-22
申请人： The United States of America as Represented by the Secretary of the Air Force
发明人： James M Mann , Eric Hunt
IPC分类号： C30B7/10 , C01B25/45 , C09K11/77 , C30B29/14 , C01G43/025 , C30B7/14 , C30B29/16 , C01G43/00 , C01G43/06 , C30B29/12 , C01B25/455 , C09K11/04
CPC分类号： C30B7/10 , C01B25/45 , C01B25/455 , C01G43/006 , C01G43/025 , C01G43/06 , C01P2002/72 , C01P2002/76 , C01P2002/77 , C01P2006/60 , C09K11/04 , C09K11/7709 , C30B7/14 , C30B29/12 , C30B29/14 , C30B29/16
摘要： A method of synthesizing rubidium uranium fluoride crystals. The method includes combining uranium-based feedstock with a mineralizer solution that includes a rubidium fluoride. The feedstock and mineralizer solution are pressurized and a thermal gradient applied thereto such that a first portion of the feedstock and the mineralizer solution is heated to a temperature that is greater than a temperature of a second portion of the feedstock and the mineralizer solution. Uranium nutrient enters the mineralizer solution from the feedstock in the first portion and uranium nutrient precipitates to spontaneously form crystals in the second portion.

6. 发明授权

US09377464B2 Metal sulfide and rare-earth phosphate nanostructures and methods of making same 有权
标题翻译：金属硫化物和稀土磷酸盐纳米结构及其制备方法
公开(公告)号：US09377464B2
公开(公告)日：2016-06-28
申请号：US14243418
申请日：2014-04-02
申请人： The Research Foundation for the State University of New York
发明人： Stanislaus Wong , Fen Zhang
IPC分类号： G01N33/58 , C30B7/14 , B82Y30/00 , B82Y40/00 , C01B17/20 , C01B25/37 , C01G3/12 , C01G9/08 , C01G11/02 , C01G21/21 , C09K11/08 , C09K11/58 , C09K11/66 , C09K11/77 , C30B29/14 , C30B29/46 , C30B29/50
CPC分类号： G01N33/58 , B82Y30/00 , B82Y40/00 , C01B17/20 , C01B25/37 , C01G3/12 , C01G9/08 , C01G11/02 , C01G21/21 , C01P2002/72 , C01P2004/03 , C01P2004/04 , C01P2004/13 , C09K11/0811 , C09K11/582 , C09K11/661 , C09K11/7777 , C30B7/14 , C30B29/14 , C30B29/46 , C30B29/50
摘要： The present invention provides a method of producing a crystalline rare earth phosphate nanostructure. The method comprising: providing a rare earth metal precursor solution and providing a phosphate precursor solution; placing a porous membrane between the metal precursor solution and the phosphate precursor solution, wherein metal cations of the metal precursor solution and phosphate ions of the phosphate precursor solution react, thereby producing a crystalline rare earth metal phosphate nanostructure.
摘要翻译：本发明提供一种生产结晶稀土磷酸盐纳米结构体的方法。该方法包括：提供稀土金属前体溶液并提供磷酸盐前体溶液; 在金属前体溶液和磷酸盐前体溶液之间放置多孔膜，其中金属前体溶液的金属阳离子和磷酸盐前体溶液的磷酸根离子反应，从而产生结晶稀土金属磷酸盐纳米结构。

7. 发明授权

US09083135B2 Method and system for suppression of stimulated Raman scattering in laser materials 有权
标题翻译：激光材料中受激拉曼散射抑制的方法和系统
公开(公告)号：US09083135B2
公开(公告)日：2015-07-14
申请号：US14055602
申请日：2013-10-16
申请人： LAWRENCE LIVERMORE NATIONAL SECURITY, LLC
发明人： John A. Caird , Andrew J. Bayramian , Christopher A. Ebbers
IPC分类号： H01S3/10 , H01S3/00 , G02F1/355 , G02B1/00 , F21V9/00 , G02B5/02 , G02C7/10 , G02F1/361 , G03B11/00 , H01S3/30 , H01S3/16 , C30B7/00 , C30B17/00 , C30B29/14 , C30B29/22 , G02F1/37 , G02F1/35
CPC分类号： H01S3/005 , C30B7/00 , C30B17/00 , C30B29/14 , C30B29/22 , G02B1/005 , G02F1/3551 , G02F1/37 , G02F2001/354 , H01S3/163 , H01S3/1643 , H01S3/1645 , H01S3/1685 , H01S2301/03
摘要： A composition of matter is provided having the general chemical formula K(H,D)2P(16Ox,18Oy)4, where x 0.002, and x+y≈1. Additionally, a method of fabricating an optical material by growth from solution is provided. The method includes providing a solution including a predetermined percentage of (H,D)216O and a predetermined percentage of (H,D)218O, providing a seed crystal, and supporting the seed crystal on a platform. The method also includes immersing the seed crystal in the solution and forming the optical material. The optical material has the general chemical formula K(H,D)2P(16Ox,18Oy)4, where x 0.002, and x+y≈1.
摘要翻译：提供具有一般化学式K（H，D）2P（160x，180y）4的物质组成，其中x <0.998或y> 0.002，x +y≈1。另外，提供了通过从溶液生长制造光学材料的方法。该方法包括提供包含（H，D）216O的预定百分比和（H，D）218O的预定百分比的溶液，提供晶种，并将晶种支撑在平台上。该方法还包括将晶种浸入溶液中并形成光学材料。光学材料具有一般化学式K（H，D）2P（160x，180y）4，其中x <0.998或y> 0.002，x +y≈1。

8. 发明申请

US20140099718A1 SINGLE-CRYSTAL APATITE NANOWIRES SHEATHED IN GRAPHITIC SHELLS AND SYNTHESIS METHOD THEREOF 有权
标题翻译：单晶玻璃中的单晶APATITE NANOWIRES及其合成方法
公开(公告)号：US20140099718A1
公开(公告)日：2014-04-10
申请号：US14076378
申请日：2013-11-11
申请人： KOREA INSTITUTE OF ENERGY RESEARCH
发明人： Nam Jo JEONG , Jung Hoon LEE
IPC分类号： A61L31/12 , C12N5/00 , C30B29/22 , C30B25/00 , C30B29/14 , B01J27/18 , C30B29/62
CPC分类号： A61L31/123 , B01J27/1806 , B82Y30/00 , B82Y40/00 , C12N5/0068 , C30B25/00 , C30B25/005 , C30B29/14 , C30B29/22 , C30B29/60 , C30B29/62 , H01L21/02603 , Y10T428/13 , Y10T428/24355 , Y10T428/292 , Y10T428/2991 , Y10T442/10
摘要： Heterogeneous nanowires having a core-shell structure consisting of single-crystal apatite as the core and graphitic layers as the shell and a synthesis method thereof are provided. More specifically, provided is a method capable of producing large amounts of heterogeneous nanowires, composed of graphitic shells and apatite cores, in a reproducible manner, by preparing a substrate including an element corresponding to X of X5(YO4)3Z is a chemical formula for apatite, adding to the substrate a gaseous source containing an element corresponding to Y of the chemical formula, adding thereto a gaseous carbon source, and allowing these reactants to react under optimized synthesis conditions using chemical vapor deposition (CVD), and to a method capable of freely controlling the structure and size of the heterogeneous nanowires and also to heterogeneous nanowires synthesized thereby.
摘要翻译：提供了具有以单晶磷灰石为核心的核 - 壳结构和作为壳的石墨层的非均相纳米线及其合成方法。更具体地说，提供了一种能够通过制备包含对应于X5（YO4）3的X的元素的基板，以可再现的方式产生大量由石墨壳和磷灰石核心组成的多种不均匀的纳米线的方法。化学式为磷灰石，向基材中加入含有对应于化学式Y的元素的气态源，向其中加入气态碳源，并使用化学气相沉积（CVD）在优化的合成条件下使这些反应物反应，并且使得能够自由地控制非均相纳米线的结构和尺寸，以及由其合成的异质纳米线。

9. 发明申请

US20050268820A1 Tetracalcium phosphate (TTCP) having calcium phosphate whisker on surface 审中-公开
标题翻译：表面具有磷酸钙晶须的磷酸四钙（TTCP）
公开(公告)号：US20050268820A1
公开(公告)日：2005-12-08
申请号：US11131891
申请日：2005-05-18
申请人： Jiin-Huey Lin , Chien-Ping Ju , Wen-Cheng Chen
发明人： Jiin-Huey Lin , Chien-Ping Ju , Wen-Cheng Chen
IPC分类号： A61C5/00 , A61K33/42 , A61L24/00 , A61L24/02 , A61L27/12 , A61L27/50 , C04B12/02 , C04B28/34 , C04B35/00 , C30B7/00 , C30B29/14 , C30B29/62
CPC分类号： A61L24/001 , A61L24/02 , A61L27/12 , A61L27/50 , C04B12/02 , C04B12/025 , C04B28/344 , C04B28/346 , C04B2111/00086 , C04B2111/00206 , C04B2111/0025 , C04B2111/00836 , C30B7/00 , C30B29/14 , C30B29/62 , Y10T428/2991 , Y10T428/2993 , C04B22/126 , C04B22/064 , C04B20/008 , C04B40/0082 , C04B40/0259 , C04B14/383
摘要： A tetracalcium phosphate (TTCP) particle for use in preparing a fast-setting, bioresorbable calcium phosphate cement is disclosed. The TTCP particle has a basic calcium phosphate whiskers or fine crystals on a surface thereof, the basic calcium phosphate whiskers or fine crystals having a Ca/P molar ratio greater than 1.33, and having a length up to about 5000 nm and a width up to about 500 nm.
摘要翻译：公开了一种用于制备快速凝固的生物可再吸收的磷酸钙水泥的四磷酸钙（TTCP）颗粒。 TTCP颗粒在其表面上具有碱性磷酸钙晶须或细晶体，碱式磷酸钙晶须或Ca / P摩尔比大于1.33的细晶体，并且具有高达约5000nm的长度和宽度直到约500nm。

10. 发明授权

US5394420A Multiform crystal and apparatus for fabrication 失效
标题翻译：多晶体和制造装置
公开(公告)号：US5394420A
公开(公告)日：1995-02-28
申请号：US190347
申请日：1994-01-27
申请人： Robert H. Senn , Loren E. Record
发明人： Robert H. Senn , Loren E. Record
IPC分类号： C30B29/10 , C30B29/12 , C30B29/14 , C30B29/22 , C30B29/42 , C30B29/48 , C30B33/00 , H01L31/10 , H01S3/07 , H01S3/08 , H01S3/16 , H01S3/14
CPC分类号： C30B29/40 , C30B29/14 , C30B29/48 , C30B33/00 , H01S3/07 , H01S3/0612 , H01S3/16
摘要： A multiform crystal 10 suitable for laser applications is described. The multiform crystal 10 comprises at least two single crystal segments 12 fused together with a joint 14 therebetween, the joint being substantially optically transparent to light propagating through the crystal 10. The multiform crystal 10 is formed by polishing two single crystal segments 12 to form at least one optically flat face on each segment. The polished faces are cleaned and contacted against one another to form a joint 14 between the crystal segments 12. Substantially all the oxygen in the joint 14 is removed. The joint 14 is maintained at a sufficiently high temperature and pressure to join the segments 12 together at the joint forming the substantially optically transparent joint 14. Mounting fixtures suitable for holding the crystal segments 12 firmly against one another in a furnace, without causing undesirable thermal expansive forces to be exerted on the segments 12, are also described. The temperature cycle used to fuse crystal segments can also be used to heat treat laser single crystals to remove substantially all the contaminants and lattice defects in the crystal, providing higher light amplification properties in the crystal.
摘要翻译：描述适用于激光应用的多晶体10。多晶体10包括至少两个与其间的接头14熔合在一起的单晶片段12，该接合部对于通过晶体10传播的光基本上是光学透明的。多晶体10通过抛光两个单晶片段12而形成每个片段上至少有一个光学平面。抛光的表面被清洁并彼此接触以在晶体段12之间形成接头14.基本上所有的接头14中的氧被去除。接头14保持在足够高的温度和压力下，以在形成基本上光学透明的接头14的接头处将节段12连接在一起。安装固定件适于将晶体段12牢固地保持在炉中彼此之间，而不引起不期望的热还描述了施加在段12上的膨胀力。用于熔合晶体段的温度循环也可以用于热处理激光单晶，以消除晶体中的基本上所有的污染物和晶格缺陷，从而在晶体中提供较高的光放大特性。

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