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1. 发明授权

US4791229A Preparation of aryl cyanamides from arylamines and cyanogen chloride 失效
标题翻译：从芳基胺和氯化氰制备芳基腈
公开(公告)号：US4791229A
公开(公告)日：1988-12-13
申请号：US922635
申请日：1986-10-24
申请人： Rudolf Fauss , Hans-Jochem Riebel
发明人： Rudolf Fauss , Hans-Jochem Riebel
IPC分类号： C07C67/00 , C07C233/00 , C07C239/00 , C07C261/04 , C07D307/91 , C07C125/08 , C07C147/12
CPC分类号： C07D307/91 , C07C233/00
摘要： A process for the preparation of an aryl cyanamide comprising reacting an arylamine of the formula ##STR1## in which Ar is aryl,R is hydrogen or alkyl, andn is 1, 2 or 3,(excepting 2-nitroaniline, 4-nitroaniline and arylamines having a nucleophilic character equal to or lower than 2-nitroaniline and 4-nitroaniline), with cyanogen chloride in 1-2 times the molar amount per mole of amino group of the arylamine initially in a homogeneous liquid phase using as reaction medium acetic acid (which is optionally diluted with water and/or a water-miscible, organic auxiliary solvent) in the presence of 1-1.5 molar equivalents of an auxiliary base for each amino group of the arylamine, there being more cyanogen chloride than equivalents of auxiliary base present in the reaction mixture at any point in time of the reaction, the pH of the reaction mixture being maintained below 7.
摘要翻译：一种制备芳基氨酰胺的方法，包括使式（I）的芳胺，其中Ar为芳基，R为氢或烷基，n为1,2或3（除2-硝基苯胺，4-硝基苯胺和具有等于或低于2-硝基苯胺和4-硝基苯胺的亲核性质的芳基胺），其中氯化氰为最初在均相液相中的芳基胺的每摩尔氨基摩尔量的1-2倍，使用反应介质乙酸（其任选地用水和/或水混溶性有机辅助溶剂稀释）在芳基胺的每个氨基的1-1.5摩尔当量辅助碱存在下，存在比辅助碱的当量更多的氯化氰存在于反应混合物的任何反应时间点，反应混合物的pH值保持在7以下。

2. 发明授权

US4595782A Process for the preparation of alkali metal salts of acyl cyanamides 失效
标题翻译：制备酰基氰胺的碱金属盐的方法
公开(公告)号：US4595782A
公开(公告)日：1986-06-17
申请号：US671179
申请日：1984-11-14
申请人： Christian Hase , Horst Baumann , Franz-Josef Carduck , Hubert Pawelczyk
发明人： Christian Hase , Horst Baumann , Franz-Josef Carduck , Hubert Pawelczyk
IPC分类号： C07C261/04 , C07C67/00 , C07C239/00 , C07C125/08
CPC分类号： C07C261/04
摘要： The present invention is for a process for the preparation of alkali metal salts of acyl cyanamides, especially those of aliphatic carboxylic acids by reacting carboxylic acid esters of lower alcohols with monoalkali metal cyanamides. The reaction results in a process which is simple and efficient and one which can be used in commercial scale batch or continuous operations.
摘要翻译：本发明涉及通过使低级醇的羧酸酯与单碱金属氨基氰反应来制备酰基氰胺的碱金属盐，特别是脂族羧酸的碱金属盐的方法。反应产生简单有效的方法，可以在商业规模的批量或连续操作中使用。

3. 发明授权

US4298544A Manufacturing process for preparing disubstituted (N-cyanoimido) carbonates 失效
标题翻译：二取代（N-氰基亚氨基）碳酸酯的制备方法
公开(公告)号：US4298544A
公开(公告)日：1981-11-03
申请号：US118066
申请日：1980-01-24
申请人： Graham E. Robinson
发明人： Graham E. Robinson
IPC分类号： C07C233/00 , C07C125/08 , C07D317/10 , C07D319/04
CPC分类号： C07C233/00
摘要： A process for the manufacture of disubstituted (N-cyanoimido)carbonate of the formula: ##STR1## in which R.sup.1 and R.sup.2 are the same and are alkyl radicals of 1 to 6 carbon atoms or phenyl radicals, or R.sup.1 and R.sup.2 are joined to form an ethylene or propylene chain which is optionally substituted by 1 or 2 alkyl radicals each of 1 to 3 carbon atoms, by reaction of a disubstituted imidocarbonate of the formula: ##STR2## with cyanamide, characterized in that the reaction is conducted in a two phase system containing water and a water-immiscible organic solvent.
摘要翻译：制备下式的二取代（N-氰基亚氨基）碳酸酯的方法：其中R 1和R 2相同并且是1至6个碳原子的烷基或苯基，或者R 1和R 2连接到形成乙烯或丙烯链，其任选被1或2个具有1至3个碳原子的烷基取代，通过下式的二取代的亚氨基碳酸酯与氨基氰反应，其特征在于反应在含有水和与水不混溶的有机溶剂的两相体系。

4. 发明授权

US4171325A Chemical process 失效
标题翻译：化学工艺
公开(公告)号：US4171325A
公开(公告)日：1979-10-16
申请号：US878194
申请日：1978-02-16
申请人： Thomas H. Brown , Graham J. Durant , John C. Emmett , Charon R. Ganellin
发明人： Thomas H. Brown , Graham J. Durant , John C. Emmett , Charon R. Ganellin
IPC分类号： C07C323/44 , C07C125/08 , C07C133/10
CPC分类号： C07C323/44
摘要： Process for preparing heterocyclicalkylthioalkyl-N-cyanoguanidines and thioureas by treating a heterocyclicalkyl derivative with a mercaptoalkyl-N-cyanoguanidine or thiourea. Two specific products are N-cyano-N'-methyl-N"-[2-((5-methyl-4-imidazolyl)methylthio)ethyl]guanidine and N-methyl-N'-[2-((5-methyl-4-imidazolyl)methylthio)ethyl]thiourea, both useful as histamine H.sub.2 -antagonists.
摘要翻译：通过用巯基烷基-N-氰基胍或硫脲处理杂环烷基衍生物来制备杂环烷基硫代烷基-N-氰基胍和硫脲的方法。两个具体产物是N-氰基-N'-甲基-N“ - [2 - （（5-甲基-4-咪唑基）甲硫基）乙基]胍和N-甲基-N' - [2 - （（5 甲基-4-咪唑基）甲硫基）乙基]硫脲，均可用作组胺H2拮抗剂。

5. 发明授权

US3978121A 5H Dibenzo[a,d]cycloheptene derivatives 失效
标题翻译： 5H二苯并（A，D）环己基衍生物
公开(公告)号：US3978121A
公开(公告)日：1976-08-31
申请号：US567165
申请日：1975-04-11
申请人： Edward L. Engelhardt
发明人： Edward L. Engelhardt
IPC分类号： C07D209/48 , C07C125/08
CPC分类号： C07D209/48 , C07C2103/32
摘要： Compounds of 5H dibenzo[a,d]-cycloheptenes and 10,11-dihydro-5H-dibenzo[a,d]cycloheptenes which are substituted at their 5-carbon atom with an N-cyanoaminopropyl or an N-cyanoaminopropylidene radical.

6. 发明授权

US4394129A Process for the finishing of fibrous materials: sulfonyl- or carbonyl-cyanamides of dyestuffs 失效
标题翻译：纤维材料的整理方法：染料的磺酰基或羰基 - 氰胺
公开(公告)号：US4394129A
公开(公告)日：1983-07-19
申请号：US296469
申请日：1981-08-26
申请人： Hartmut Springer
发明人： Hartmut Springer
IPC分类号： C09B69/00 , C09B1/32 , C09B1/34 , C09B5/14 , C09B19/02 , C09B29/00 , C09B33/153 , C09B35/215 , C09B47/26 , C09B57/12 , D06M13/345 , D06M13/402 , D06M13/438 , D06P1/00 , D06P1/18 , C07C125/08 , D06P1/16
CPC分类号： C09B5/14 , C09B1/325 , C09B1/343 , C09B19/02 , C09B29/00 , C09B33/153 , C09B35/215 , C09B47/26 , C09B57/12 , D06M13/345 , D06M13/402 , D06M13/438 , D06P1/0048 , Y10S8/917 , Y10S8/918 , Y10S8/924
摘要： Fibrous materials of any kind is finished with an organic compound having fiber-finishing properties and containing one or several groups of the formula ##STR1## in which X is sulfonyl or carbonyl and A represents hydrogen or one equivalent of a mono-, bi- or trivalent metal or an ammonium group, is applied onto the fibrous material in the form of an aqueous or organo-aqueous solution or dispersion, and the fibrous material thus treated is then subjected, if necessary, to a heat treatment for the fixation of this organic compound onto the fibrous material. Organic fiber-finishing compounds containing the above-mentioned group may be for example dyestuffs, optical brighteners or compounds increasing the crease resistance.
摘要翻译：任何类型的纤维材料用具有纤维整理性质的有机化合物完成，并含有一个或几个式（IMAGE）的基团，其中X是磺酰基或羰基，A代表氢或一个当量的单，双或三价金属或铵基以水溶液或有机水溶液或分散体的形式施加到纤维材料上，然后如果需要，将如此处理的纤维材料进行热处理以固定该有机物复合到纤维材料上。含有上述基团的有机纤维整理化合物可以是例如增加抗折皱性的染料，荧光增白剂或化合物。

7. 发明授权

US4332822A Guanidine derivatives 失效
标题翻译：胍衍生物
公开(公告)号：US4332822A
公开(公告)日：1982-06-01
申请号：US229902
申请日：1981-01-30
申请人： Terence J. Ward
发明人： Terence J. Ward
IPC分类号： C07C279/28 , C07C125/08 , A61K31/165 , A61K31/40 , C07D207/30
CPC分类号： C07C279/28
摘要： Novel cyanoguanidine derivatives having the formula ##STR1## wherein Ar is a phenyl or pyrrol-1-yl group substituted by one or more substituents selected from halogen, trifluoromethyl, lower alkyl, lower alkoxy and nitro and R.sub.1, R.sub.2, R.sub.3, R.sub.4 and R.sub.5 are each independently hydrogen or lower alkyl or R.sub.1 and R.sub.2 taken together form dimethylene or trimethylene, lower blood pressure and, in some cases are also anti-ulcer agents.
摘要翻译：具有下式的新的氰基胍衍生物其中Ar是被一个或多个选自卤素，三氟甲基，低级烷基，低级烷氧基和硝基的取代基取代的苯基或吡咯-1-基，R1，R2，R3，R4和R5 各自独立地为氢或低级烷基，或者R 1和R 2一起形成二亚甲基或三亚甲基，降低血压，并且在一些情况下也是抗溃疡剂。

8. 发明授权

US4250092A Derivatives of N-cyano-azomethines and process for their preparation 失效
标题翻译： N-氰基偶氮甲碱的衍生物及其制备方法
公开(公告)号：US4250092A
公开(公告)日：1981-02-10
申请号：US38838
申请日：1979-05-14
申请人： Franjo Kajfez
发明人： Franjo Kajfez
IPC分类号： C07C261/04 , C07C20060101 , C07C67/00 , C07C239/00 , C07C253/30 , C07C255/61 , C07C313/00 , C07C323/25 , C07C323/45 , C07D203/12 , C07D203/20 , C07D233/64 , C07C125/08
CPC分类号： C07D203/12
摘要： N-Cyano-azomethines, useful as intermediates for the production of antihistamines are described. They are produced by reaction of ##STR1## where R.sub.3 is a thiomethyl group, an alkylamino group or N-1-amino-.omega.-alkylthiomethyl group, with primary or secondary alkyl- or hydroxyalkyl-amines or with ethylenimine.
摘要翻译：描述了可用作生产抗组胺剂的中间体的N-氰基 - 偶氮甲碱。它们通过＆lt; IMAGE＆gt;其中R3是硫代甲基，烷基氨基或N-1-氨基-ω-烷基硫代甲基与伯或仲烷基 - 或羟基烷基 - 胺或与亚乙基亚胺反应制备。

9. 发明授权

US4235928A Substituted cyanamides and their use as fungicides 失效
标题翻译：取代的氰胺及其作为杀真菌剂的用途
公开(公告)号：US4235928A
公开(公告)日：1980-11-25
申请号：US99017
申请日：1979-11-30
申请人： Karl Eicken , Peter Plath , Ernst-Heinrich Pommer
发明人： Karl Eicken , Peter Plath , Ernst-Heinrich Pommer
IPC分类号： A01N47/40 , A01N53/12 , C07C67/00 , C07C233/00 , C07C239/00 , C07C255/58 , C07C261/04 , C07C313/00 , C07C323/60 , C07C325/00 , C07C333/02 , C07C333/08 , C07D213/81 , C07D261/18 , C07D263/34 , C07D271/10 , C07D277/56 , C07D285/12 , C07D307/24 , C07D307/46 , C07D307/68 , C07D333/38 , C07D333/40 , A01N47/12 , C07C121/78 , C07C125/08
CPC分类号： C07D263/34 , A01N47/40 , C07C255/00 , C07D261/18 , C07D271/10 , C07D277/56 , C07D285/12 , C07D307/68 , C07D333/38
摘要： New, substituted cyanamides, processes for the manufacture thereof, and fungicides containing these compounds.
摘要翻译：新的取代的氰酰胺，其制备方法和含有这些化合物的杀真菌剂。

10. 发明授权

US3994971A Phosphorus-containing condensation products 失效
标题翻译：含磷缩合产物
公开(公告)号：US3994971A
公开(公告)日：1976-11-30
申请号：US604411
申请日：1975-08-13
申请人： Hermann Nachbur , Arthur Maeder
发明人： Hermann Nachbur , Arthur Maeder
IPC分类号： B27K3/15 , B27K3/50 , C07F9/54 , C08L61/32 , D06M15/431 , D06M15/667 , D06M15/673 , C07C125/08 , C07F9/22 , C09K3/28
CPC分类号： D06M15/673 , C07F9/5407 , C08L61/32 , D06M15/431 , D06M15/667 , B27K2240/30 , B27K3/15 , Y10T442/268
摘要： The subject of the invention is a process for the manufacture of water-soluble condensation products of hydroxymethylphosphonium compounds and cyanamide, characterized in that (a) one mol of a tetrakis-(hydroxymethyl)-phosphonium compound is condensed with (b) 0.02 to 0.5 mol, preferably 0.1 to 0.3 mol, of cyanamide at 40.degree. to 120.degree. C, optionally in the presence of formaldehyde or a formaldehyde-donating agent and optionally in the presence of an inert organic solvent, and optionally subsequently further condensed at temperatures of 100.degree. to 150.degree. C and, if appropriate, free hydroxyl groups are at least partially etherified with at least one alkanol with 1 to 4 carbon atoms and if appropriate the salts of the condensation products are converted into the corresponding hydroxides.
摘要翻译：本发明的主题是制备羟甲基鏻化合物和氨腈的水溶性缩合产物的方法，其特征在于（a）一摩尔四（羟甲基）鏻化合物与（b）0.02至0.5 mol，优选0.1至0.3mol氰氨腈，任选在甲醛或甲醛供体剂存在下，任选在惰性有机溶剂存在下，任选地随后在100℃的温度下进一步冷凝如果合适，游离羟基至少部分用至少一个具有1至4个碳原子的链烷醇醚化，如果合适，则缩合产物的盐转化为相应的氢氧化物。

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