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    • 5. 发明授权
    • Diamond-anvil high-pressure cell with improved X-ray collimation system
    • 具有改进的X射线准直系统的金刚石 - 砧座高压电池
    • US4602377A
    • 1986-07-22
    • US595013
    • 1984-03-30
    • David SchiferlBarton W. OlingerRobert W. Livingston
    • David SchiferlBarton W. OlingerRobert W. Livingston
    • G01N23/20G21K1/02
    • G01N23/20041G21K1/02
    • An adjustable X-ray collimation system for a diamond-anvil high-pressure cell of the type including a cooperable piston and cylinder and a pair of opposing diamonds located between the head of the piston and the head of the cylinder. The X-ray collimation system includes a tubular insert which contains an X-ray collimator. The insert is engageable in the bore of the piston. The collimator is mounted within the insert by means of an elastomeric O-ring at the end closest the opposed diamonds, and by means of a set of adjustable set screws at the opposite end. By adjustment of the set screws the collimator can be pivoted about the O-ring and brought into alignment with the opposed diamonds and the sample contained therein. In the preferred embodiment there is further provided a set of plugs which are insertable in the bore of the collimator. The plugs have bores of different diameters. By successively inserting plugs of progressively smaller bore diameters and adjusting the alignment of the collimator with each plug, the collimator can be quickly brought into accurate alignment with the diamonds. The collimation system allows alignment of the collimator either before or after the cell has been loaded and pressurized.
    • 一种用于金刚石 - 砧座高压电池的可调X射线准直系统,包括可配合的活塞和气缸以及位于活塞头部和气缸头部之间的一对相对的金刚石。 X射线准直系统包括含有X射线准直仪的管状插入件。 插入件可接合在活塞的孔中。 准直器通过弹性体O形环安装在插入件内,最靠近相对的金刚石的端部,并通过一组相对端的可调定位螺钉安装。 通过调整固定螺钉,准直器可以围绕O形环枢转并与对置的钻石和其中包含的样品对准。 在优选实施例中,还提供了可插入准直器的孔中的一组插头。 插头具有不同直径的孔。 通过连续地插入逐渐变小的孔径的插头并且调整准直器与每个插头的对准,准直器可以被快速地与钻石准确对准。 准直系统允许在电池被加载和加压之前或之后对准准直器。