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1. 发明授权

US06541068B1 Method for the flame-retardant processing of textile materials 失效
标题翻译：纺织材料阻燃加工方法
公开(公告)号：US06541068B1
公开(公告)日：2003-04-01
申请号：US09601395
申请日：2000-09-12
申请人： Leonid Semenovich Galbraikh , Nina Sergeevna Zubkova , Nataliya Grigorievna Butylkina , Alexandr Alexandrovich Berlin , Nikolai Alexandrovich Khalturinsky
发明人： Leonid Semenovich Galbraikh , Nina Sergeevna Zubkova , Nataliya Grigorievna Butylkina , Alexandr Alexandrovich Berlin , Nikolai Alexandrovich Khalturinsky
IPC分类号： D06M13364
CPC分类号： C09D161/28 , D06M13/425 , D06M13/447 , D06M15/423 , D06M15/432 , D06M15/643 , D06M15/6436 , D06M15/693 , D06M2200/30
摘要： A process is proposed for the fireproofing treatment of textile materials by impregnating them initially with a melamine-formaldehyde resin or organosilicon substances, and then with a solution of a complex compound of the ammonia salt of amidoalkylphosphonic acid with ammonium chloride. Materials treated in accordance with the invention have reduced combustibility and low toxicity of the gases given off during combustion.
摘要翻译：提出了一种通过先用三聚氰胺 - 甲醛树脂或有机硅物质浸渍纺织材料进行防火处理的方法，然后用酰氨基烷基膦酸的氨盐与氯化铵的络合物的溶液进行浸渍。根据本发明处理的材料在燃烧期间释放的气体的可燃性和低毒性降低。

2. 发明授权

US5320785A Compositions containing phosphono compounds and organic acids as flameproofing agents 失效
标题翻译：含有膦酰基化合物和有机酸作为防火剂的组合物
公开(公告)号：US5320785A
公开(公告)日：1994-06-14
申请号：US736679
申请日：1991-07-26
申请人： Salman Dermeik
发明人： Salman Dermeik
IPC分类号： C07F9/38 , C09K21/12 , D06M13/02 , D06M13/184 , D06M13/188 , D06M13/192 , D06M13/203 , D06M13/244 , D06M13/322 , D06M13/35 , D06M13/355 , D06M13/358 , D06M13/402 , D06M13/432 , D06M13/447 , D06M15/432 , D06M101/00 , D06M101/02 , D06M101/06 , D06M101/08 , C09K21/10 , D06M13/00
CPC分类号： D06M13/192 , D06M13/447 , D06M15/432
摘要： The permanence of the flame-resistant finish of fibre materials, in particular those based on cellulose, is improved if a phosphono compound which contains an N-methylol group. is used together with an organic carboxylic acid as the finishing agent. If oxalic acid in particular is used as the carboxylic acid, the finished fibre material can be stored in a damp environment for a prolonged period of time without intermediate washing being necessary. The tendency of the finish to hydrolyse in a damp atmosphere is reduced by using the organic carboxylic acid instead of a mineral acid.
摘要翻译：如果含有N-羟甲基的膦酰基化合物，纤维材料的阻燃整理剂，特别是基于纤维素的耐火漆的耐久性得到改善。与有机羧酸一起用作整理剂。如果特别使用草酸作为羧酸，则成品纤维材料可以在潮湿环境中长时间储存，而不需要中间洗涤。通过使用有机羧酸代替无机酸，降低了在潮湿气氛中水解的趋势。

3. 发明授权

US4063883A Manufacture of flame-retardant regenerated cellulose fibres 失效
标题翻译：制造阻燃再生纤维素纤维
公开(公告)号：US4063883A
公开(公告)日：1977-12-20
申请号：US604489
申请日：1975-08-14
申请人： Johann Hupfl , Manfred Czermak , Helmut Teichmann , Josef Paul
发明人： Johann Hupfl , Manfred Czermak , Helmut Teichmann , Josef Paul
IPC分类号： C08K3/32 , C08K5/00 , D01F2/10 , D01F11/02 , D06M11/68 , D06M11/70 , D06M13/285 , D06M13/292 , D06M13/44 , D06M15/431 , D06M15/432 , D06M15/673 , D01F2/08
CPC分类号： D06M15/673 , C08K3/32 , C08K5/0066 , C08K5/49 , D01F2/10 , D06M11/68 , D06M11/70 , D06M13/285 , D06M13/292 , D06M15/431 , D06M15/432
摘要： Manufacture of flame-retardant regenerated cellulose fibres by adding one or more flame-retardant phosphorus comounds to viscose, extruding the viscose-containing mixture thus obtained into a spinning bath, stretching and after treating the resulting filaments or staple fibres. The flame-retardant fibres are made by using as the flame-retardant agent a combination of compounds of the general formula:PN.sub.x O.sub.yin which x stands for a number between 0.09 and 1.7 and y stands for a number between 1.2 and 0, preferably approaching zero as the values of x increase towards 1.7 (component A), with compounds which are selected from phosphoric acid alkylesters, preferably halogen-containing phosphoric acid alkylesters; cyclophosphazenes, polyphosphazenes; tetrakis-(oxymethyl)-phosphonium chloride or hydroxide or its condensation products with ammonia, oxymethylamine, urea or other amines or amides, vinyl compounds containing halogen, phosphonitrogen or phosphorus; and tris-(1-aziridinyl)-phosphine oxide or N-(oxymethyl)-3-phosphonopropionamide, if desired in further combination with a condensation resin (component B).
摘要翻译：通过向粘胶加入一种或多种阻燃磷化合物制造阻燃再生纤维素纤维，将由此获得的含粘胶混合物挤出到纺丝浴中，拉伸和处理所得到的长丝或短纤维。阻燃纤维是通过使用以下通式的化合物作为阻燃剂来制备的：

4. 发明授权

US3647734A Preparation of flame retardant composition for cellulosic material 失效
标题翻译：阻燃剂组合物的制备用于纤维素材料
公开(公告)号：US3647734A
公开(公告)日：1972-03-07
申请号：US3647734D
申请日：1970-03-26
申请人： LOWENSTEIN & SONS M
发明人： HARDWICKE JAMES E , SCHEFFLER BERNARD , WEISZ HERMAN S
IPC分类号： D06M15/432 , C08G51/24 , C08G37/32
CPC分类号： D06M15/432
摘要： A COMPOSITION FOR RENDERING COLLULOSIC MATERIAL FLAME RETARTDANT IS PREPARED BY MAINTAINING THE INTERMEDIATE REACTION PROUCT 3-(DI-ISOPROPYLPHOSPHONO) PROPRIONAMIDE IN AQUEOUS SOLUTION BELOW ITS MELTING POINT FOR METHYLOLATION WITH FORMALDEHYDE TO FORM THE N-HYDROXYMETHYL DERIVATIVE, AND THEN FORMULATING THIS DERIVATIVE WITH AN AQUEOUS METHYOLMELAMINE RESIN SOLUTION AND AN ACID CATALYST FOR PAD-DRY-CURE APPLICATION TO THE CELLULOSIC MATERIAL. CELLULOSIC MATERIAL TREATED WITH THE RESULTING COMPOSITION IS RENDERED SELF-EXTINGUISHING AND RETANS THIS CHARACTERISTIC AFTER FIFTY WASHINGS.

5. 发明授权

US4370442A Fire retardant compositions 失效
标题翻译：阻燃组合物
公开(公告)号：US4370442A
公开(公告)日：1983-01-25
申请号：US214017
申请日：1980-12-05
申请人： Glenn A. Pearson
发明人： Glenn A. Pearson
IPC分类号： C08G12/40 , D06M15/432 , C08L61/20
CPC分类号： D06M15/432 , C08G12/40
摘要： A method of preparing an aqueous resinous system, and the resinous system produced by the method is described wherein about 75-100 parts of an aldehyde such as formaldehyde, about 100-125 parts of phosphoric acid, about 15-25 parts of an alkanolamine such as triethanolamine, about 30-50 parts of urea, and about 20-40 parts of melamine, based on 100-200 parts of water, are reacted to provide an aqueous resinous solution which will cure at room temperature or upon application of heat, permitting its use as a flexible, pliable, waterproof, nonburning coating, especially for textiles and paper containing materials. The solution may be applied by impregnation or as a coating to the fabric or an underlayer to the fabric. In a special embodiment, there is provided a method for providing fire retardancy to a textile fabric applied over an underlayer such as muslin, by applying a fire retardant solution to the underlayer. There is also provided a fire retardant spray solution.
摘要翻译：描述了一种制备水性树脂体系的方法和通过该方法制备的树脂体系，其中约75-100份醛如甲醛，约100-125份磷酸，约15-25份链烷醇胺如作为三乙醇胺，约30-50份尿素和约20-40份三聚氰胺（基于100-200份水）反应，以提供在室温或加热下固化的水性树脂溶液，允许其用作柔性，柔韧，防水，不燃涂层，特别适用于纺织和含纸材料。溶液可以通过浸渍或作为涂层施加到织物或底层到织物上。在一个特殊的实施方案中，提供了一种通过将阻燃溶液施加到底层上来为施加在诸如细棉布的底层上的织物提供阻燃性的方法。还提供了阻燃喷雾溶液。

6. 发明授权

US4280812A Method of imparting smolder resistance to cotton-containing textiles 失效
标题翻译：对含棉纺织品施加闷热阻力的方法
公开(公告)号：US4280812A
公开(公告)日：1981-07-28
申请号：US132594
申请日：1980-03-21
申请人： Darrell J. Donaldson , Robert J. Harper, Jr.
发明人： Darrell J. Donaldson , Robert J. Harper, Jr.
IPC分类号： D06M11/82 , D06M15/432 , D06M1/00
CPC分类号： D06M15/432 , D06M11/82
摘要： Smolder resistance is imparted to cotton and cotton-containing fabrics by applying a certain boron-nitrogen-phosphorus system to the fabric, employing conventional equipment. An inorganic boron compound is placed in solution with a phosphorus-containing compound, then a nitrogen-containing compound is added. The aqueous mixture is applied using conventional textile equipment, dried, and cured by standard methods.
摘要翻译：使用常规设备，通过向织物施加一定的硼 - 氮 - 磷体系，对棉和含棉织物施加锑阻力。将无机硼化合物与含磷化合物一起放入溶液中，然后加入含氮化合物。使用常规纺织设备施加含水混合物，干燥并通过标准方法固化。

7. 发明授权

US4028053A Fire retardant fabrics and method for preparation thereof 失效
标题翻译：阻燃织物及其制备方法
公开(公告)号：US4028053A
公开(公告)日：1977-06-07
申请号：US550295
申请日：1975-02-18
申请人： Marshall W. Duke
发明人： Marshall W. Duke
IPC分类号： D06M15/432 , D06M1/00
CPC分类号： D06M15/432 , Y10S428/921
摘要： A process for rendering cellulose and cellulose containing fabrics fire resistant by first impregnating the fibers with a solution of an aminoplast resin, an acid and an effective amount of a dialkyl phosphono methylol alkylamide to produce fire retardancy in the resulting fabric having the formula ##STR1## wherein R is lower alkyl having 1 to 6 carbon atoms and x is an integer from 1 to 3 and polymerizing the resin while the fibers are wet and swollen. The fabric is then cured, washed and dried. The fabric obtained from this process possesses high fire-retardancy values, soft hand, and tensile values similar to that of the untreated fabric.
摘要翻译：通过首先用氨基塑料树脂，酸和有效量的二烷基膦酰羟甲基烷基酰胺浸渍纤维来使纤维素和含纤维素的织物呈现耐火性的方法，以在具有下式的所得织物中产生阻燃性：（I）其中R是具有1至6个碳原子的低级烷基，x是1至3的整数，并且在纤维湿润和溶胀时使树脂聚合。然后将织物固化，洗涤和干燥。从该方法获得的织物具有与未处理织物相似的高阻燃性值，柔软的手感和拉伸值。

8. 发明授权

US3832227A Use of triazinylaminoalkyl phosphonates for the flameproofing of textiles 失效
标题翻译：三苯甲酰氨基磷酸酯用于纺织品的使用
公开(公告)号：US3832227A
公开(公告)日：1974-08-27
申请号：US29397372
申请日：1972-10-02
申请人： STAUFFER CHEMICAL CO
发明人： WEIL E , FEARING R
IPC分类号： C07F9/6521 , C08G12/40 , C08G59/40 , D06M13/288 , D06M15/432 , C09D5/18
CPC分类号： C08G59/4071 , C07F9/65217 , C08G12/40 , D06M13/288 , D06M15/432
摘要： A PROCESS FOR THE FLAMEPROOFING OF TEXTILES BY TREATING THE TEXTILE WITH A NOVEL CLASS OF TRIAZINYLAMINOALKYL PHOSPHONATES AND THE CROSSLINKING OF THE PHOSPHONATES TO YIELD A FIRE RETARDANT FINISHED FOR THE TEXTILE IS DISCLOSED. THESE TRIAZINYLAMINOALKYL PHOSPHONATES ARE FOUND TO BE LOW IN COST AND OF MINIMAL TOXICITY AND THEIR USE OF THE FLAMEPROOFING OF TEXTILES PROVIDES HIGHLY DURABLE FINISHES.

9. 发明授权

US3746572A Process for flame retarding fabrics 失效
标题翻译：阻燃织物的工艺
公开(公告)号：US3746572A
公开(公告)日：1973-07-17
申请号：US3746572D
申请日：1971-02-23
申请人： STAUFFER CHEMICAL CO
发明人： WEIL E , FEARING R , EISENBERG B
IPC分类号： D06M15/432 , C09D5/18
CPC分类号： D06M15/432 , Y10S428/921 , Y10T442/268
摘要： THE PRESENT INVENTION A PROCESS FOR FLAME RETARDING TEXTILES WHICH COMPRISES: (1) APPLYING TO A TEXTILE AN AQUEOUS SOLUTION CONSISTING OF (A) A PHOSPHONATE HAVING AT LEAST ONE CARBON-BONDED PRIMARY ALCOHOL GROUP, (B) DIMETHYLOLDIHYDROXYETHYLENE UREA, AND (C) A CURING CATALYST; AND (2) CURING THE PHOSPHONATE AND UREA ON THE TEXTILE AND THEREBY RENDERING THE TEXTILE FLAME RETARDANT.

10. 发明申请

US20170152379A1 PHOSPHOROUS-ACID MONOMER CONTAINING EMULSION POLYMER MODIFIED UREA-FORMALDEHYDE RESIN COMPOSITIONS FOR MAKING FIBERGLASS PRODUCTS 审中-公开
公开(公告)号：US20170152379A1
公开(公告)日：2017-06-01
申请号：US15320519
申请日：2015-06-10
申请人： Rohm and Haas Company
发明人： James C. Bohling , Arnold S. Brownell , Michael D. Kelly
IPC分类号： C08L61/24 , D06M15/432 , D04H1/587 , D04H1/64 , C08F220/18 , D04H1/4218
CPC分类号： C08L61/24 , C08F2/001 , C08F2/24 , C08F2/26 , C08F30/02 , C08F36/20 , C08F220/18 , C08F290/00 , C08F2220/1825 , C08L43/02 , C08L61/06 , C08L2201/52 , C08L2201/54 , C09J161/24 , D04H1/4218 , D04H1/587 , D04H1/64 , D06M15/432 , D10B2101/06 , C08F212/08 , C08F220/06 , C08F212/14 , C08F2230/085
摘要： The present invention provides polymer modified aqueous urea formaldehyde resin (UF resin) binder compositions useful in making a treated glass mat, e.g., for roofing shingles, wherein the polymer modifier is an multistage aqueous emulsion acorn copolymer comprising one protuberant polymer stage containing phosphorous acid groups and one or more other polymer stage comprising an addition copolymer incompatible with the protuberant polymer stage, wherein the multistage aqueous emulsion copolymer has a measured Tg of from −60 to 25° C., or, preferably from 31 30 to 12° C. and, further wherein the weight ratio of the total of monomers used to make the one or more other polymer stage to the total amount of monomers used to make the protuberant polymer stage ranges from 3:1 to 50:1, or, preferably, from 3:1 to 30:1 or, more preferably, from 3:1 to 20:1, or, even more preferably, from 8:1 to 12:1.

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