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1. 发明授权

US11667541B2 Two-dimensional (2D) bismuth nanocomposite, and preparation method and use thereof 有权
公开(公告)号：US11667541B2
公开(公告)日：2023-06-06
申请号：US17128311
申请日：2020-12-21
申请人： Henan University
发明人： Bingyang Shi , Jiefei Wang , Ping Shangguan , Yong Zhong , Zhongjie Wang , Xiaoyu Chen
IPC分类号： C01G29/00 , C01G55/00 , B82Y30/00 , B82Y40/00
CPC分类号： C01G29/00 , C01G55/00 , B82Y30/00 , B82Y40/00 , C01P2004/04 , C01P2004/24 , C01P2004/64
摘要： The disclosure relates to a two-dimensional (2D) bismuth nanocomposite, and a preparation method and use thereof, and belongs to the field of nanobiotechnology. The 2D bismuth nanocomposite of the disclosure is an ultra-thin bismuth nanosheet that is loaded with platinum nanoparticles and modified with indocyanine green (ICG) and surface targeting polypeptide Ang-2. The 2D bismuth nanocomposite Bi@Pt/ICG-Ang2 of the disclosure can not only realize the targeted photothermal and photodynamic combination therapy for tumors, but also realize the dual-mode imaging combining CT and fluorescence imaging.

2. 发明授权

US09957168B2 Method for synthesis of ruthenium nanoparticles with face-centered cubic and hexagonal close-packed structures 有权
公开(公告)号：US09957168B2
公开(公告)日：2018-05-01
申请号：US15201852
申请日：2016-07-05
申请人： Honda Motor Co., Ltd.
发明人： Avetik Harutyunyan , Nam Hawn Chou
IPC分类号： C01G55/00 , B22F9/24 , B01J23/46 , B01J35/00 , B01J37/04 , B22F1/00 , C22B61/00 , B01J37/03 , B01J37/00
CPC分类号： C01G55/00 , B01J23/462 , B01J35/0013 , B01J35/0046 , B01J35/006 , B01J37/0072 , B01J37/031 , B01J37/04 , B22F1/0044 , B22F9/24 , C22B61/00
摘要： The present disclosure provides for methods for preparing ruthenium nanoparticles characterized by face centered cubic crystallographic structure characterized by small particle size, substantially homogeneous particle size distribution, substantially uniform spherical shape, and substantial high temperature stability. The present disclosure further provides for methods for preparing ruthenium nanoparticles characterized by face hexagonal close packed crystallographic structure characterized by small particle size, substantially homogeneous particle size distribution, substantially uniform spherical shape, and substantial high temperature stability.

3. 发明授权

US09359223B2 Method for producing thin film electrodes 有权
标题翻译：薄膜电极的制造方法
公开(公告)号：US09359223B2
公开(公告)日：2016-06-07
申请号：US13237487
申请日：2011-09-20
申请人： Manoj Narayanan , Beihai Ma , Uthamalingam Balachandran , Stephen Dorris
发明人： Manoj Narayanan , Beihai Ma , Uthamalingam Balachandran , Stephen Dorris
IPC分类号： B05D5/12 , C01G55/00 , H01L49/02
CPC分类号： H05K3/068 , C01G55/00 , C01G55/002 , C01P2004/03 , C01P2006/32 , C01P2006/40 , H01B1/08 , H01L28/65 , H05K1/092 , Y10T428/31678
摘要： The invention provides for A method for producing pure phase strontium ruthenium oxide films, the method comprising solubilizing ruthenium-containing and strontium-containing compounds to create a mixture; subjecting the mixture to a first temperature above that necessary for forming RuO2 while simultaneously preventing formation of RuO2; maintaining the first temperature for a time to remove organic compounds from the mixture, thereby forming a substantially dry film; and subjecting the film to a second temperature for time sufficient to crystallize the film. Also provided is pure phase material comprising strontium ruthenium oxide wherein the material contains no RuO2.
摘要翻译：本发明提供了一种生产纯相锶氧化钌薄膜的方法，该方法包括使含钌和含锶化合物溶解以产生混合物; 使混合物经受高于形成RuO 2所必需的第一温度，同时防止形成RuO 2; 保持第一温度一段时间以从混合物中除去有机化合物，从而形成基本干燥的膜; 并将膜处于第二温度足以使膜结晶的时间。还提供了包含氧化钌的纯相材料，其中该材料不含RuO 2。

4. 发明授权

US09340738B2 Method of making cerium oxide nanoparticles 有权
标题翻译：制造氧化铈纳米粒子的方法
公开(公告)号：US09340738B2
公开(公告)日：2016-05-17
申请号：US14537161
申请日：2014-11-10
申请人： CERION, LLC
发明人： Albert Gary DiFrancesco , Richard K. Hailstone , Kenneth J. Reed , Gary R. Prok
IPC分类号： C01F17/00 , C10L1/12 , B01J13/00 , B82Y30/00 , C01G25/00 , C01G25/02 , C01G49/00 , C01G49/02 , C01G55/00 , C10L1/10 , C10L10/02 , C10L10/06 , C10L1/188
CPC分类号： C10L1/1233 , B01J13/0034 , B01J13/0047 , B82Y30/00 , C01F17/00 , C01F17/0043 , C01G25/00 , C01G25/02 , C01G49/0054 , C01G49/009 , C01G49/02 , C01G55/00 , C01P2002/30 , C01P2002/52 , C01P2002/72 , C01P2004/04 , C01P2004/51 , C01P2004/52 , C01P2004/64 , C01P2006/90 , C10G25/02 , C10L1/10 , C10L1/1881 , C10L10/02 , C10L10/06 , C10L2200/0222 , C10L2200/024 , C10L2200/0245 , C10L2200/0254 , C10L2230/22 , C10L2250/06 , C10L2270/026 , Y10T428/2982
摘要： A process for making cerium-containing oxide nanoparticles includes providing an aqueous reaction mixture containing a source of cerous ion and a source of one or more metal ions (M) other than cerium, a source of hydroxide ion, at least one monoether carboxylic acid nanoparticle stabilizer wherein the molar ratio of said monoether carboxylic acid nanoparticle stabilizers to total metal ions is greater than 0.2, and an oxidant. The cerous ion is oxidized to ceric ion, thereby forming a product dispersion of cerium-containing oxide nanoparticles containing one or more metal ions (M), Ce1-xMxO2-δ, wherein x has a value from about 0.001 to about 0.95 and δ has a value of about 0.0 to about 0.5.
摘要翻译：制备含铈氧化物纳米颗粒的方法包括提供含有铈离子源和除了铈以外的一种或多种金属离子（M）的源的氢氧化物离子源，至少一种单醚羧酸纳米颗粒的含水反应混合物其中所述单醚羧酸纳米颗粒稳定剂与总金属离子的摩尔比大于0.2的稳定剂和氧化剂。铈离子被氧化成铈离子，从而形成含有一种或多种金属离子（M），Ce1-xMxO2-δ的含铈氧化物纳米粒子的产物分散体，其中x具有约0.001至约0.95的值，δ具有约0.0至约0.5的值。

5. 发明授权

US09005555B2 Method for preparing solid ruthenium nitrosyl nitrate 有权
标题翻译：固体硝基硝酸硝基钌的制备方法
公开(公告)号：US09005555B2
公开(公告)日：2015-04-14
申请号：US14475547
申请日：2014-09-02
申请人： Sunshine Kaidi New Energy Group Co., Ltd.
发明人： Li Xu , Bo Lai , Dechen Song , Qianqian Liu , Yiming Han
IPC分类号： C01G55/00 , C22B3/00
CPC分类号： C22B11/048 , C01G55/00 , C01P2006/80 , C22B1/005 , C22B7/009 , Y02P10/214 , Y02P10/234
摘要： A method for preparing solid ruthenium nitrosyl nitrate, including: 1) drying a ruthenium-containing spent catalyst, and calcining the spent catalyst, and cooling to room temperature, whereby yielding a ruthenium-containing solid; 2) grinding the ruthenium-containing solid to yield a powder, introducing the powder to a fluidized bed reactor, aerating the fluidized bed reactor with nitrogen or an inert gas, charging hydrogen, whereby yielding ruthenium metal; 3) contacting a mixed gas of ozone and air with the ruthenium metal, whereby yielding gaseous ruthenium tetroxide; 4) introducing the gaseous ruthenium tetroxide into a three-stage absorption plant, whereby yielding an acid solution including ruthenium nitrate; 5) adding a solid of sodium nitrite to the acid solution, stirring, and heating a resulting solution, whereby yielding a solution of ruthenium nitrosyl nitrate; and 6) extracting the solution of ruthenium nitrosyl nitrate with anhydrous ether.
摘要翻译：一种制备固体硝酸亚硝基硝酸盐的方法，包括：1）干燥含钌废废催化剂，煅烧废催化剂，冷却至室温，由此得到含钌固体; 2）研磨含钌固体产生粉末，将粉末引入流化床反应器，用氮气或惰性气体充气流化床反应器，加入氢气，从而产生钌金属; 3）将臭氧和空气的混合气体与钌金属接触，从而产生四氧化四钌; 4）将气态四氧化钌引入三级吸收装置，从而产生包含硝酸钌的酸溶液; 5）向酸溶液中加入亚硝酸钠固体，搅拌并加热所得溶液，由此得到硝酸亚硝基硝酸钌溶液; 和6）用无水乙醚萃取硝酸亚硝基硝酸钌溶液。

6. 发明授权

US08987165B2 Unsupported and supported non-promoted ruthenium sulfide catalyst with high catalytic activity for hydrocarbon hydrotreatments and its method 有权
标题翻译：不支持和支持的非促进的硫化氢催化剂具有高催化活性的烃加氢处理及其方法
公开(公告)号：US08987165B2
公开(公告)日：2015-03-24
申请号：US13444411
申请日：2012-04-11
申请人： Carlos Elias Ornelas Gutierrez , Lorena Alvarez Contreras , Jose Rurik Farias Mancilla , Alfredo Aguilar Elguezabal
发明人： Carlos Elias Ornelas Gutierrez , Lorena Alvarez Contreras , Jose Rurik Farias Mancilla , Alfredo Aguilar Elguezabal
IPC分类号： B01J27/02 , B01J27/045
CPC分类号： B01J27/045 , B01J35/002 , B01J35/006 , B01J35/1014 , B01J35/1019 , B01J37/0201 , B01J37/031 , B01J37/08 , B01J37/18 , B01J37/20 , B82Y30/00 , C01G55/00 , C01P2002/72 , C01P2004/64 , C01P2006/12 , C01P2006/17 , C10G3/44 , C10G45/04 , Y02P30/20
摘要： The present invention relates to a synthesis method for unsupported and supported ruthenium base (RuS2) catalysts from a ruthenium complex precursor, which is decomposed and activated by a simple activation process; these steps provide a catalyst with very high catalytic activity, in addition the incorporation of ruthenium complex precursor to a support by methods of incipient and wet impregnating is described; the obtained catalytic activities in this invention are in the order of 100 times the molybdenum sulfide catalyst without support and without promoter, 14 times the industrial supported catalyst, and 5 times the activity of the currently most active commercial unsupported catalyst.
摘要翻译：本发明涉及一种通过简单的活化方法分解和活化的来自钌络合物前体的未负载和负载的钌基（RuS 2）催化剂的合成方法; 这些步骤提供具有非常高的催化活性的催化剂，此外，描述了通过初始和湿浸渍方法将钌络合物前体引入载体的方法; 在本发明中获得的催化活性大约是无支撑和无助催化剂的钼硫化物催化剂的100倍，是工业载体催化剂的14倍，是当前最活跃的无载体催化剂活性的5倍。

7. 发明申请

US20150059236A1 CERIUM OXIDE CONTAINING NANOPARTICLES 有权
标题翻译：含氧化铈的纳米颗粒
公开(公告)号：US20150059236A1
公开(公告)日：2015-03-05
申请号：US14537993
申请日：2014-11-11
申请人： Cerion, LLC
发明人： Albert Gary DIFRANCESCO , Richard K. HAILSTONE , Kenneth J. REED , Gary R. PROK
IPC分类号： C10L1/12 , C10L10/06 , C10L10/02
CPC分类号： C10L1/1233 , B01J13/0034 , B01J13/0047 , B82Y30/00 , C01F17/00 , C01F17/0043 , C01G25/00 , C01G25/02 , C01G49/0054 , C01G49/009 , C01G49/02 , C01G55/00 , C01P2002/30 , C01P2002/52 , C01P2002/72 , C01P2004/04 , C01P2004/51 , C01P2004/52 , C01P2004/64 , C01P2006/90 , C10G25/02 , C10L1/10 , C10L1/1881 , C10L10/02 , C10L10/06 , C10L2200/0222 , C10L2200/024 , C10L2200/0245 , C10L2200/0254 , C10L2230/22 , C10L2250/06 , C10L2270/026 , Y10T428/2982
摘要： A process for making cerium-containing oxide nanoparticles includes providing an aqueous reaction mixture containing a source of cerous ion, optionally a source of one or more metal ions (M) other than cerium, a source of hydroxide ion, at least one monoether carboxylic acid nanoparticle stabilizer wherein the molar ratio of said monoether carboxylic acid nanoparticle stabilizers to cerous ions is greater than 0.2, and an oxidant. The cerous ion is oxidized to ceric ion, thereby forming a product dispersion of cerium-containing oxide nanoparticles CeO2-δ, wherein δ has a value of about 0.0 to about 0.5. The nanoparticles may have a mean hydrodynamic diameter from about 1 nm to about 50 nm, and a geometric diameter of less than about 45 nm.
摘要翻译：制备含铈氧化物纳米颗粒的方法包括提供含有铈离子源的水性反应混合物，任选地除了铈以外的一种或多种金属离子（M）的源，氢氧根离子源，至少一种单醚羧酸其中所述单醚羧酸纳米颗粒稳定剂与铈离子的摩尔比大于0.2的纳米颗粒稳定剂和氧化剂。铈离子被氧化成铈离子，从而形成含铈氧化物纳米粒子CeO2-δ的产物分散体，其中δ具有约0.0至约0.5的值。纳米颗粒可以具有约1nm至约50nm的平均流体动力学直径和小于约45nm的几何直径。

8. 发明申请

US20150017513A1 NOVEL COMPOUND, METHOD FOR PREPARATION OF THE SAME, AND LITHIUM SECONDARY BATTERY COMPRISING THE SAME 审中-公开
标题翻译：新化合物，其制备方法和包含其的锂二次电池
公开(公告)号：US20150017513A1
公开(公告)日：2015-01-15
申请号：US14501645
申请日：2014-09-30
申请人： LG CHEM, LTD.
发明人： YoungHwa JUNG , Youngsun CHOI , Seung-Tae HONG
IPC分类号： H01M4/485 , C01G55/00 , H01M10/052
CPC分类号： H01M4/485 , C01G55/00 , C01G55/002 , C01P2002/52 , C01P2002/72 , C01P2002/77 , C01P2006/40 , H01M4/505 , H01M4/525 , H01M10/052 , H01M10/0525 , H01M2220/20 , Y02E60/122 , Y02P70/54 , Y02T10/7011
摘要： Disclosed are a novel compound, a method for preparing the same, and a lithium secondary battery comprising the same. More specifically, disclosed are a compound in which five MO6 octahedrons are bonded to one another around one MO6 octahedron such that the MO6 octahedrons share a vertex, to form hollows and Li cations substituted instead of Na cations using an ion substitution method are present in the hollows, and a crystal structure thereof is not varied even upon intercalation and deintercalation of Li cations, a method for preparing the same, and a lithium secondary battery comprising the same as a cathode active material.
摘要翻译：公开了一种新型化合物，其制备方法和包含该化合物的锂二次电池。更具体地，公开了一种化合物，其中五个MO6八面体围绕一个MO6八面体彼此结合，使得MO6八面体共享顶点，形成中空，并且使用离子取代方法代替Na阳离子的Li阳离子存在于空穴及其晶体结构即使在Li阳离子的嵌入和脱嵌时也不变化，其制备方法，以及包含该阳离子活性物质的锂二次电池。

9. 发明授权

US08333950B2 Process for the preparation of lithium metal oxides involving fluidized bed techniques 失效
标题翻译：涉及流化床技术的锂金属氧化物的制备方法
公开(公告)号：US08333950B2
公开(公告)日：2012-12-18
申请号：US12858048
申请日：2010-08-17
申请人： Horst Krampitz , Michael Fooken , Wilhelm Sellmann
发明人： Horst Krampitz , Michael Fooken , Wilhelm Sellmann
IPC分类号： C01D1/02 , C01G45/12
CPC分类号： C01G37/00 , C01G23/005 , C01G25/02 , C01G31/00 , C01G33/00 , C01G39/00 , C01G41/00 , C01G45/1221 , C01G45/1228 , C01G45/1235 , C01G51/42 , C01G53/42 , C01G55/00 , C01P2002/72 , C01P2006/12 , C01P2006/40
摘要： A method of producing lithium metal oxides can include mixing lithium salt and a metal oxide to form a composition, heating the composition in a first reactor, transferring the composition to a second reactor, and passing the composition through the second reactor to anneal the composition to form lithium metal oxides. The second reactor can be a fluidized bed reactor. The lithium metal oxide can have an average crystal size of between about 5 microns and about 20 microns.
摘要翻译：制备锂金属氧化物的方法可以包括混合锂盐和金属氧化物以形成组合物，在第一反应器中加热组合物，将组合物转移到第二反应器中，并使组合物通过第二反应器将组合物退火至形成锂金属氧化物。第二反应器可以是流化床反应器。锂金属氧化物的平均晶体尺寸可以在约5微米至约20微米之间。

10. 发明申请

US20120149907A1 PROCESS FOR PREPARING TRICHLOROAMMINEPLATINATE SALT AND THE PRODUCTS OBTAINED THEREIN 有权
标题翻译：制备三氯蔗糖盐的方法及其获得的产品
公开(公告)号：US20120149907A1
公开(公告)日：2012-06-14
申请号：US13379336
申请日：2009-06-20
申请人： Vladimir Kysilka , Jan Mengler , Petr Kacer , Libor Cerveny , Karel Havlovic , Lucie Potucka
发明人： Vladimir Kysilka , Jan Mengler , Petr Kacer , Libor Cerveny , Karel Havlovic , Lucie Potucka
IPC分类号： C07F15/00 , C09K3/00
CPC分类号： A61K31/282 , C01G55/00
摘要： The present invention relates to a process for preparing a trichloroammineplatinate salt by reacting a tetrachloroplatinate salt in aqueous solution in the presence of ammonium chloride and an alkali chloride with one or more carbonate salts selected from the group consisting of potassium, sodium and ammonium carbonate while keeping the pH value below 7 during the reaction; the product obtained therein and a use thereof.
摘要翻译：本发明涉及一种通过在氯化铵和碱金属氯化物存在下，将四氯铂酸盐与一种或多种选自碳酸钾，碳酸钠和碳酸铵的碳酸盐反应的水溶液中，使四氯铂酸盐进行反应来制备三氯苯胺五乙酸盐，同时保持反应期间pH值低于7; 其中获得的产品及其用途。

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