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1. 发明申请

US20180170764A1 PROCESS FOR PREPARING SMALL SIZE LAYERED DOUBLE HYDROXIDE PARTICLES 审中-公开
公开(公告)号：US20180170764A1
公开(公告)日：2018-06-21
申请号：US15551643
申请日：2016-02-19
申请人： SCG Chemicals Co., Ltd.
发明人： Dermot O'Hare , Miaosen Yang
IPC分类号： C01F7/66 , C01F7/16 , B01D9/00
CPC分类号： C01F7/66 , B01D9/0063 , B82Y30/00 , B82Y40/00 , C01F7/002 , C01F7/162 , C01F7/164 , C01P2002/22 , C01P2002/60 , C01P2002/72 , C01P2002/82 , C01P2002/86 , C01P2002/88 , C01P2004/03 , C01P2004/04 , C01P2004/22 , C01P2004/60 , C01P2004/61 , C01P2004/62 , C01P2004/64 , C01P2006/12
摘要： A process for preparing particles of a layered double hydroxide of the general formula [Mpz+M′qy+(OH)2]a+(Xn−)a/n.bH2O (I) wherein Mz+ and M′y+ are metal cations or mixtures of metal cations, z=1 or 2; y=3 or 4; p+q=1; b=0 to 10, Xn− is an anion, n is 1 to 5 and a is determined by p, q, y and z such that a=zp+yq−2, comprises (a) mixing, in aqueous solution, Mz+ cations, M′y+ cations and Xn− anions, with a base; and (b) allowing the layered double hydroxide of formula (I) to precipitate from the solution mixed in step (a). Preferably, M is Li, Mg, Zn, Fe, Ni, Co, Cu, Ca, or a mixture of two or more. Preferably, y is 3, and M′ is Al, Ga, In, Fe or a mixture of two or more thereof. Also provided are particles obtainable by the process, especially wherein M is Ca, M′ is Al, and Xn− is NO3−. Particles of a layered double hydroxide wherein the particles have a particle size of not greater than 2000 nm, preferably not greater than 300 nm and especially not greater than 100 nm, are also provided. The layered double hydroxides according to the invention are useful in certain applications, for example, as adsorbents, coatings and catalyst supports.

2. 发明授权

US09764964B2 Application of lactam as solvent in nanomaterial preparation 有权
公开(公告)号：US09764964B2
公开(公告)日：2017-09-19
申请号：US14372864
申请日：2012-01-19
申请人： Housheng Xia , Guisheng Yang
发明人： Housheng Xia , Guisheng Yang
IPC分类号： C01F17/00 , C01G23/053 , C01G49/06 , C01G49/08 , C01F5/20 , C01G3/02 , C01G5/00 , C01G9/02 , C01G5/02 , C01G9/08 , C01G11/00 , C01B19/04 , C01B33/18 , C01F5/14 , C01F5/24 , C01F7/16 , C01F11/46 , C22B3/04 , C22B3/00 , C22B15/00 , C01F7/00 , C01F7/34 , C01B19/00
CPC分类号： C01F17/0043 , C01B19/007 , C01B19/04 , C01B33/18 , C01F5/14 , C01F5/20 , C01F5/24 , C01F7/005 , C01F7/162 , C01F7/34 , C01F11/462 , C01G3/02 , C01G5/00 , C01G5/02 , C01G9/02 , C01G9/08 , C01G11/00 , C01G23/053 , C01G23/0532 , C01G23/0536 , C01G49/06 , C01G49/08 , C01P2002/72 , C01P2002/86 , C01P2004/03 , C01P2004/04 , C01P2004/64 , C01P2006/42 , C22B3/04 , C22B11/04 , C22B15/0065
摘要： The present invention disclosed use of lactam as a solvent in the preparation of nanomaterials by precipitation method, sol-gel method or high temperature pyrolysis. These methods are able to recycle lactam solvent, which meet requirements of environmental protection.

3. 发明授权

US09260308B2 Nanomaterials and process for making the same 有权
标题翻译：纳米材料和制造过程相同
公开(公告)号：US09260308B2
公开(公告)日：2016-02-16
申请号：US13864080
申请日：2013-04-16
申请人： Graphene Technologies, Inc.
发明人： Robert Wayne Dickinson , Oliver Douglas Ousterhout , Lawrence Joseph Musetti , Douglas Paul DuFaux
IPC分类号： C09C1/44 , C01B31/04 , C01F5/02 , C01G23/04 , C01G23/07 , B82Y30/00 , B82Y40/00 , C01G9/02 , C01G9/03 , C01F7/16
CPC分类号： C01B31/0446 , B82Y30/00 , B82Y40/00 , C01B32/184 , C01F5/02 , C01F7/162 , C01G9/02 , C01G9/03 , C01G23/04 , C01G23/07 , C01P2004/04 , C01P2004/38 , C01P2004/64
摘要： Process for producing nanomaterials such as graphenes, graphene composites, magnesium oxide, magnesium hydroxides and other nanomaterials by high heat vaporization and rapid cooling. In some of the preferred embodiments, the high heat is produced by an oxidation-reduction reaction of carbon dioxide and magnesium as the primary reactants, although additional materials such as reaction catalysts, control agents, or composite materials can be included in the reaction, if desired. The reaction also produces nanomaterials from a variety of other input materials, and by varying the process parameters, the type and morphology of the carbon nanoproducts and other nanoproducts can be controlled. The reaction products include novel nanocrystals of MgO (percilase) and MgAl2O4 (spinels) as well as composites of these nanocrystals with multiple layers of graphene deposited on or intercalated with them.
摘要翻译：通过高热蒸发和快速冷却来生产纳米材料如石墨烯，石墨烯复合材料，氧化镁，氢氧化镁和其他纳米材料的方法。在一些优选实施方案中，通过二氧化碳和镁作为主要反应物的氧化还原反应产生高热，尽管反应催化剂，控制剂或复合材料等附加材料可以包括在反应中，如果想要的该反应还从各种其他输入材料制备纳米材料，通过改变工艺参数，可以控制碳纳米产品和其他纳米产品的类型和形态。反应产物包括MgO（percilase）和MgAl 2 O 4（尖晶石）的新型纳米晶体以及这些纳米晶体与沉积在其上或与其嵌入的多层石墨烯的复合材料。

4. 发明授权

US09242224B2 Method for the production of multiphase composite materials using microwave plasma process 有权
标题翻译：使用微波等离子体工艺生产多相复合材料的方法
公开(公告)号：US09242224B2
公开(公告)日：2016-01-26
申请号：US14208955
申请日：2014-03-13
申请人： AMASTAN TECHNOLOGIES LLC
发明人： Makhlouf Redjdal , Kamal Hadidi
IPC分类号： B01J19/00 , B01J19/12 , C04B35/44 , C04B35/443 , C04B35/626 , C04B35/645 , C01B13/34 , C01F7/16 , C01F17/00
CPC分类号： B01J19/126 , C01B13/34 , C01F7/162 , C01F17/0025 , C01P2002/02 , C01P2002/72 , C01P2004/03 , C01P2004/32 , C01P2004/61 , C04B35/44 , C04B35/443 , C04B35/6263 , C04B35/62665 , C04B35/645 , C04B35/6455 , C04B2235/3222 , C04B2235/3224 , C04B2235/3225 , C04B2235/528 , C04B2235/764
摘要： Disclosed herein is a method to produce multiphase composite materials directly from solution precursor droplets by a fast pyrolysis process using a microwave plasma embodiment containing a microwave generating source, a dielectric plasma torch, and a droplet maker. Here, using homogenous solution precursors, droplets are generated with a narrow size distribution, and are injected and introduced into the microwave plasma torch with generally uniform thermal path. The generally uniform thermal path in the torch is achieved by axial injection of droplets into an axisymmetric hot zone with laminar flows. Upon exposing to high temperature within the plasma with controlled residence time, the droplets are pyrolyzed and converted into particles by quenching with a controlled rate of the exhaust gas in a gas chamber. The particles generated have generally uniform sizes and uniform thermal history, and can be used for a variety of applications.
摘要翻译：本文公开了一种通过使用包含微波发生源，介电等离子体焰炬和液滴制造器的微波等离子体实施例的快速热解法直接从溶液前驱体液滴产生多相复合材料的方法。在这里，使用均匀的溶液前体，产生具有窄尺寸分布的液滴，并注入并引入具有大致均匀热路径的微波等离子体焰炬中。通过将液滴轴向注入到具有层流的轴对称热区域中，可实现手电筒中大致均匀的热路径。当以受控的停留时间暴露于等离子体内的高温时，液滴被热解并通过在气室中以受控的排气速率淬火而转化为颗粒。产生的颗粒具有大致均匀的尺寸和均匀的热历史，并可用于各种应用。

5. 发明申请

US20150315442A1 Production Method of a Novel Polishing Alumina 审中-公开
标题翻译：新型抛光氧化铝的生产方法
公开(公告)号：US20150315442A1
公开(公告)日：2015-11-05
申请号：US14648283
申请日：2013-12-23
申请人： ALBEMARLE EUROPE SPRL
发明人： Henning Hofius
IPC分类号： C09K3/14
CPC分类号： C09K3/1427 , C01F5/08 , C01F7/162 , C01F7/30 , C01F7/441 , C01F7/442 , C01G15/00 , C01G23/006 , C01G25/02 , C01G37/00 , C01G45/1242 , C01G49/0045 , C01G49/0054 , C01G51/40 , C01P2004/03 , C01P2004/52 , C01P2004/61 , C01P2004/62 , C01P2006/12 , C09D1/02 , C09K3/1436
摘要： Provided is a method for the formation of particulate compounds of selectable size characteristics, which method includes supporting a slurried particulate precursor on a porous support; heating the support such that aggregates of the particulate compound are formed, and desagglomerating the aggregates into their component particulate. In a preferred embodiment, an aqueous slurry of alumina particulate which has not undergone the alpha transition is contacted with a porous support having defined pore and cavity sizes, such that the slurry occupies at least some of the interstices of the porous support. The slurry and support are heated such that the alumina precursor slurry undergoes the alpha transition. The alpha alumina product is then particulated. The support is of such a material that it is either lost through combustion during heating or otherwise removable after heating, such as during or after particulation, without destroying the particle characteristics imparted by the porous support. Additionally, in a further embodiment, co-components are added to the slurry in order to impart desired properties to the particulated product.
摘要翻译：提供了形成可选尺寸特性的颗粒化合物的方法，该方法包括在多孔载体上支撑浆状颗粒前体; 加热支撑体使得形成颗粒化合物的聚集体，并将聚集体解散聚集成它们的组分颗粒。在优选的实施方案中，未经历α转变的氧化铝颗粒的水性浆料与具有确定的孔和空腔尺寸的多孔载体接触，使得浆料占据多孔载体的至少一些间隙。加热浆料和载体使得氧化铝前体浆料经历α转变。然后将α氧化铝产物粉碎。支撑件具有这样的材料，即它在加热期间通过燃烧而失去，或者在加热之后，例如在雾化期间或之后，或者在不破坏由多孔载体赋予的颗粒特性的情况下被去除。另外，在另一个实施方案中，向浆料中加入共组分，以赋予微粒产物所需的性能。

6. 发明授权

US09139448B2 Heat-insulating material 有权
标题翻译：绝热材料
公开(公告)号：US09139448B2
公开(公告)日：2015-09-22
申请号：US13972040
申请日：2013-08-21
申请人： Covalent Materials Corporation
发明人： Shuko Akamine , Mitsuhiro Fujita
IPC分类号： C04B38/00 , C01F7/02 , C01F7/16 , C04B35/44 , C04B35/443 , C04B111/28
CPC分类号： C01F7/02 , C01F7/162 , C04B35/44 , C04B35/443 , C04B38/0074 , C04B2111/28 , C04B2235/3262 , C04B2235/3272 , C04B2235/3279 , C04B2235/3284 , C04B2235/763 , C04B2235/9607 , C04B38/0054
摘要： A heat-insulating material is provided in which thermal conductivity is controlled not to increase and good insulation properties are held even in a high temperature range. The heat-insulating material is formed of a spinel porous sintered body having a porosity of 65 to 90 vol. % and represented by a chemical formula XAl2O4 (X=Zn, Fe, Mg, Ni, or Mn) which is arranged such that large pores having a diameter of greater than 1000 μm occupy 25 vol. % or less of the total pore volume, fine pores having a diameter of 0.45 μm or less occupy 5 to 40 vol. % of the volume of the pores having a diameter of 1000 μm or less, at least one pore-diameter distribution peak is within a range of 0.14 to 10 μm, and is formed of sintered particles having a calculated average particle diameter of 0.04 to 1 μm.
摘要翻译：提供了一种绝热材料，其中热导率被控制为不增加，并且即使在高温度范围内也保持良好的绝缘性能。隔热材料由孔隙率为65〜90体积的尖晶石多孔质烧结体构成。％，由化学式XAl2O4（X = Zn，Fe，Mg，Ni或Mn）表示，其排列使得直径大于1000μm的大孔占据25体积％。总孔体积的％以下，直径为0.45μm以下的细孔占据5〜40体积％。直径为1000μm以下的孔的体积的％，至少一个孔径分布峰在0.14〜10μm的范围内，由计算出的平均粒径为0.04〜1的烧结体形成 μm。

7. 发明申请

US20150210558A1 Process for Producing Magnesium Oxide 审中-公开
标题翻译：生产氧化镁的方法
公开(公告)号：US20150210558A1
公开(公告)日：2015-07-30
申请号：US14615163
申请日：2015-02-05
申请人： Graphene Technologies, Inc.
发明人： Robert Wayne Dickinson , Jon K. Myers , Oliver Douglas Ousterhout , Lawrence Joseph Musetti , Douglas Paul DuFaux
IPC分类号： C01F5/04 , C01F7/16
CPC分类号： C01F5/04 , B82Y30/00 , B82Y40/00 , C01B7/03 , C01B32/184 , C01F5/30 , C01F7/162 , C01P2002/32 , C01P2004/03 , C01P2004/04 , C01P2004/13 , C01P2004/64 , C01P2006/80 , C25C1/02 , Y02P10/212
摘要： Process for producing nanomaterials such as graphenes, graphene composites, magnesium oxide, magnesium hydroxides and other nanomaterials by high heat vaporization and rapid cooling. In some of the preferred embodiments, the high heat is produced by an oxidation-reduction reaction of carbon dioxide and magnesium as the primary reactants, although additional materials as reaction catalysts, control agents, or composite materials can be included in the reaction, if desired. The carbon dioxide and magnesium are combusted together in a reactor to produce nano-magnesium oxide, graphenes, graphene composites, and possibly other products which are then separated or excluded by suitable processes or reactions to provide the individual reaction products. The reaction is highly energetic, producing very high temperatures on the order of 5610° F. (3098° C.), or higher, and also produces large amounts of useful energy in the form of heat and light, including infrared and ultraviolet radiation, all of which can be captured and reused in the invention or utilized in other applications. The products of combustion, particularly the magnesium oxide, can be recycled to provide additional oxidizing agents for combustion with the carbon dioxide. By varying the process parameters, such as reaction temperature and pressure, the type and morphology of the carbon nanoproducts and other nanoproducts can be controlled. The reaction also produces nanomaterials from a variety of input materials. The reaction products include novel nanocrystals of MgO (percilase) and MgAl2O4 (spinels) as well as composites of these nanocrystals with multiple layers of graphene deposited on or intercalated with them.
摘要翻译：通过高热蒸发和快速冷却来生产纳米材料如石墨烯，石墨烯复合材料，氧化镁，氢氧化镁和其他纳米材料的方法。在一些优选实施方案中，通过二氧化碳和镁作为主要反应物的氧化 - 还原反应产生高热，但如果需要，反应催化剂，控制剂或复合材料可以包括在反应中。。二氧化碳和镁在反应器中一起燃烧以产生纳米氧化镁，石墨烯，石墨烯复合物和可能的其它产物，然后通过合适的方法或反应分离或排除以提供单独的反应产物。该反应是高能量的，产生大约5610°F（3098℃）或更高的非常高的温度，并且还产生大量的热和光形式的有用能量，包括红外和紫外线辐射，所有这些可以在本发明中被捕获和重复使用或用于其它应用中。燃烧产物，特别是氧化镁可以再循环，以提供用于与二氧化碳燃烧的附加氧化剂。通过改变工艺参数，如反应温度和压力，可以控制碳纳米产物和其他纳米产物的类型和形态。该反应还从各种输入材料生产纳米材料。反应产物包括MgO（percilase）和MgAl 2 O 4（尖晶石）的新型纳米晶体以及这些纳米晶体与沉积在其上或与其嵌入的多层石墨烯的复合材料。

8. 发明申请

US20150098883A1 APPLICATION OF LACTAM AS SOLVENT IN NANOMATERIAL PREPARATION 有权
标题翻译： LACTAM作为溶剂在纳米制备中的应用
公开(公告)号：US20150098883A1
公开(公告)日：2015-04-09
申请号：US14372864
申请日：2012-01-19
申请人： Housheng Xia , Guisheng Yang
发明人： Housheng Xia , Guisheng Yang
IPC分类号： C01F17/00 , C01F5/24 , C01B33/18 , C01G9/08 , C01G5/02 , C01F5/14 , C01F7/16 , C01G5/00 , C01G49/08 , C01F11/46 , C01G23/053 , C01G3/02 , C22B3/00 , C22B15/00 , C22B3/04 , C01B19/04
CPC分类号： C01F17/0043 , C01B19/007 , C01B19/04 , C01B33/18 , C01F5/14 , C01F5/20 , C01F5/24 , C01F7/005 , C01F7/162 , C01F7/34 , C01F11/462 , C01G3/02 , C01G5/00 , C01G5/02 , C01G9/02 , C01G9/08 , C01G11/00 , C01G23/053 , C01G23/0532 , C01G23/0536 , C01G49/06 , C01G49/08 , C01P2002/72 , C01P2002/86 , C01P2004/03 , C01P2004/04 , C01P2004/64 , C01P2006/42 , C22B3/04 , C22B11/04 , C22B15/0065
摘要： The present invention disclosed use of lactam as a solvent in the preparation of nanomaterials by precipitation method, sol-gel method or high temperature pyrolysis. These methods are able to recycle lactam solvent, which meet requirements of environmental protection.
摘要翻译：本发明公开了通过沉淀法，溶胶 - 凝胶法或高温热解制备纳米材料中的内酰胺作为溶剂的用途。这些方法能够回收符合环保要求的内酰胺溶剂。

9. 发明申请

US20140050842A1 SPINEL POWDER AND MANUFACTURING PROCESS THEREFOR, AND PROCESSES FOR PRODUCING THERMAL SPRAYING FILM AND GAS SENSOR ELEMENTS 有权
标题翻译：旋风粉末及其制造方法及其生产热喷涂膜和气体传感器元件的方法
公开(公告)号：US20140050842A1
公开(公告)日：2014-02-20
申请号：US14113453
申请日：2012-03-29
申请人： Namitsugu Fujii , Ryo Nishizawa , Takuji Nabeta
发明人： Namitsugu Fujii , Ryo Nishizawa , Takuji Nabeta
IPC分类号： C09D1/00
CPC分类号： C09D1/00 , C01F7/162 , C01P2002/32 , C01P2002/72 , C01P2004/03 , C01P2004/51 , C01P2004/61 , C01P2006/12 , C23C4/11 , G01N27/407 , Y10T428/2991
摘要： Disclosed is a spinel powder obtained by mixing a magnesia raw-material with an electrically fused alumina, followed by firing of the mixture. The particles of the spinel powder are coated with granular spinel particles. Therefore, there are provided a spinel powder and a simple method for producing the same, which is superior in thermal spraying property and has a unique particle shape. In particular, there is provided a method for producing a spinel powder which contributes to a reduction in the variation of characteristics of sensors, for example, as a thermal spraying powder for forming a protective coating of a gas sensor element.
摘要翻译：公开了通过将氧化镁原料与电熔融氧化铝混合，然后烧结混合物得到的尖晶石粉末。尖晶石粉末的颗粒涂覆有颗粒尖晶石颗粒。因此，提供了一种尖晶石粉末及其制造方法，其喷涂性优异，具有独特的颗粒形状。特别是提供一种制造尖晶石粉末的方法，该方法有助于降低传感器的特性变化，例如作为用于形成气体传感器元件的保护涂层的热喷涂粉末。

10. 发明申请

US20110129670A1 NANOMETRIC-SIZED CERAMIC MATERIALS, PROCESS FOR THEIR SYNTHESIS AND USES THEREOF 有权
标题翻译：纳米尺寸陶瓷材料及其合成方法及用途
公开(公告)号：US20110129670A1
公开(公告)日：2011-06-02
申请号：US12994430
申请日：2009-05-26
申请人： João Manuel Calado Da Silva , Elsa Marisa Dos Santos Antunes
发明人： João Manuel Calado Da Silva , Elsa Marisa Dos Santos Antunes
IPC分类号： C04B35/00 , B82Y30/00
CPC分类号： C04B35/6267 , B01J3/08 , B82Y30/00 , C01B13/185 , C01B21/0724 , C01F7/162 , C01G49/08 , C01P2002/32 , C01P2002/60 , C01P2004/64 , C01P2006/10 , C01P2006/12 , C01P2006/60 , C04B35/04 , C04B35/105 , C04B35/119 , C04B35/26 , C04B35/265 , C04B35/443 , C04B35/45 , C04B35/581 , C04B35/62625 , C04B2235/3213 , C04B2235/3227 , C04B2235/3241 , C04B2235/401 , C04B2235/402 , C04B2235/443 , C04B2235/5409 , C04B2235/5454 , C04B2235/83
摘要： The disclosed subject concerns nanometric-sized ceramic materials in the form of multiple crystalline structures, composites, or solid solutions, the process for their synthesis, and uses thereof. These materials are mainly obtained by detonation of two water-in-oil (W/O) emulsions, one of which is prepared with precursors in order to present a detonation regime with temperature lower than 2000° C., and they present a high chemical and crystalline phase homogeneity, individually for each particle, as well as a set of complementary properties adjustable according to the final applications, such as a homogeneous distribution of the primary particles, very high chemical purity level, crystallite size below 50 nm, surface areas by mass unit between 25 and 500 m2/g, and true particle densities higher than 98% of the theoretical density. This set of characteristics makes this materials particularly suitable for a vast range of applications in the nanotechnology field, such as, for example, nanocoatings, magnetic nanofluids, nanocatalysts, nanosensors, nanopigments, nanoadditives, ultra light nanocomposites, drug release nanoparticles, nanomarkers, nanometric films, etc.
摘要翻译：所公开的主题涉及多晶形结构，复合材料或固溶体形式的纳米尺寸陶瓷材料，其合成方法及其用途。这些材料主要通过引爆两种油包水（W / O）乳液获得，其中一种乳液是用前体制备的，以提供温度低于2000℃的爆轰方式，并且它们呈现出高度的化学和每个颗粒的晶相均匀性，以及根据最终应用可调整的一组互补性质，例如初级颗粒的均匀分布，非常高的化学纯度水平，低于50nm的微晶尺寸，表面积由质量单位为25-500m2 / g，真实颗粒密度高于理论密度的98％。这种特性使得该材料特别适用于纳米技术领域的广泛应用，例如纳米涂层，磁性纳米流体，纳米催化剂，纳米传感器，纳米颗粒，纳米添加剂，超轻纳米复合材料，药物释放纳米颗粒，纳米标记物，纳米尺度电影等

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