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1. 发明授权

US11919980B2 Dual catalyst composition 有权
公开(公告)号：US11919980B2
公开(公告)日：2024-03-05
申请号：US16633673
申请日：2018-08-02
申请人： TOTAL RESEARCH & TECHNOLOGY FELUY
发明人： Virginie Cirriez , Alexandre Welle , Aurélien Vantomme
IPC分类号： C08F4/653 , B01J35/00 , C07F17/00 , C08F4/642 , C08F4/659 , C08F4/6592 , C08F210/16
CPC分类号： C08F210/16 , B01J35/0046 , C07F17/00 , C08F4/6428 , C08F4/65904 , C08F4/65912 , C08F4/65916 , C08F4/65927
摘要： The present invention relates to a catalyst composition comprising:

catalyst component A comprising a bridged metallocene compound with two tetrahydroindenyl groups, each group being unsubstituted or substituted;
catalyst component B comprising a bridged metallocene compound with a substituted or unsubstituted cyclopentadienyl group and a substituted or unsubstituted fluorenyl group;
an optional activator; an optional support; and an optional co-catalyst.

The present invention also relates to a polymerization process using said composition. The invention further relates to olefin polymers at least partially catalyzed by said catalyst composition and articles comprising said olefin polymers.

2. 发明授权

US11560469B2 Polypropylene composition and thermoformed sheet thereof 有权
公开(公告)号：US11560469B2
公开(公告)日：2023-01-24
申请号：US15741794
申请日：2016-07-14
申请人： Total Research & Technology Feluy
发明人： Philippe Lodefier , Marc Dufrenoy , Julie Dubuisson , Amélie Buffard , Cristo Boukalidis
IPC分类号： C08L23/14 , C08J3/00 , C08J5/18 , B29C51/02 , B29K23/00 , B29K105/00
摘要： The present invention relates to a polypropylene composition for thermoforming comprising: from 50% by weight to at most 90% by weight of a polypropylene A, wherein polypropylene A is a polypropylene random copolymer, based on the total weight of the polypropylene composition; and from 10% by weight to at most 50% by weight of a polypropylene B, wherein polypropylene B is a polypropylene homopolymer, based on the total weight of the polypropylene composition; wherein the melt flow index of polypropylene B is at most 1.0 g/10 min, as measured according to the method of standard ISO 1133, condition M, at 230° C. and under a load of 2.16 kg; and wherein the ratio of the melt flow index of polypropylene A to the melt flow index of polypropylene B is at least 80.

3. 发明授权

US11549062B2 Renewable diesel fuel production in retrofitted fossil petroleum refinery to produce biofuel and bio-feedstock for steam crackers 有权
公开(公告)号：US11549062B2
公开(公告)日：2023-01-10
申请号：US17059581
申请日：2019-05-28
申请人： Total Research & Technology Feluy
发明人： Walter Vermeiren
IPC分类号： C10G3/00 , C10G69/06 , C11C1/04 , C11C1/08 , B01J19/00 , B01J19/24 , C11C1/10
摘要： The present invention relates to a process for the conversion of a feedstock comprising at least 50 wt % related to the total weight of the feedstock of triglycerides, fatty acid esters and/or fatty acids having at least 10 carbon atoms into hydrogen, olefins, dienes, aromatics, gasoline, diesel fuel, jet fuel, naphtha and liquefied petroleum gas comprising: a) introducing of said feedstock in a first reactor to produce linear paraffins in presence of a hydrodesulfurization catalyst and hydrogen, b) separating the effluent of said first reactor in at least three parts to produce at least a first stream comprising part of said linear paraffins and at least a second stream comprising part of said linear paraffins, and at least a third stream comprising part of said linear paraffins c) sending said first stream to a steam cracker to produce hydrogen, olefins, dienes, aromatics and gasoline, diesel fuel being further fractionated; d) introducing said second stream into a second reactor in presence of a hydrocracking or hydroisomerization catalyst to produce a mixture comprising diesel fuel, jet fuel, naphtha and liquefied petroleum gas being further fractionated e) blending said third stream with the diesel fuel obtained at said step d) wherein said feedstock of said first reactor is diluted in order to limit the temperature increase within said first reactor; and wherein before entering the first reactor said dilution is performed with a weight ratio diluent:feedstock being 1:1, and wherein said diluent comprises at least part of said paraffins obtained at step b).

4. 发明授权

US11208504B2 Injection-molded articles comprising metallocene-catalyzed polyethylene resin 有权
公开(公告)号：US11208504B2
公开(公告)日：2021-12-28
申请号：US16629888
申请日：2018-07-11
申请人： TOTAL RESEARCH & TECHNOLOGY FELUY
发明人： Aurélien Vantomme , Jean-Léon Gielens , Armelle Sigwald , Christopher Willocq
IPC分类号： C08F10/02 , C08F4/6592 , B29C45/00 , C08F2/00 , C08L23/08 , C08F110/02 , C08F210/02
摘要： The present invention relates to an injection-molded article, comprising at least one metallocene-catalyzed polyethylene resin comprising at least two metallocene-catalyzed polyethylene fractions A and B, wherein the at least one metallocene-catalyzed polyethylene resin comprises:
at least 40% to at most 50% by weight of polyethylene fraction A based on the total weight of the at least one metallocene-catalyzed polyethylene resin, wherein fraction A has a melt index MI2 of at least 100.0 g/10 min as determined according to ISO 1133, condition D, at 190° C. and under a load of 2.16 kg; and wherein the at least one metallocene-catalyzed polyethylene resin has a density of at least 0.940 g/cm3 to at most 0.950 g/cm3 as measured on pellets according to ISO 1183 at 23° C.; a melt index MI2 of at least 1.4 g/10 min to at most 2.5 g/10 min as measured on pellets according to ISO 1133, condition D, at 190° C. and under a load of 2.16 kg. The present invention also relates to a process for preparing said injection-molded article, comprising the steps of a) providing at least one metallocene-catalyzed polyethylene resin as described herein; and b) injection-molding said polyethylene resin into an article.

5. 发明申请

US20210388133A1 Polyethylene Resins 有权
公开(公告)号：US20210388133A1
公开(公告)日：2021-12-16
申请号：US17285526
申请日：2019-10-14
申请人： TOTAL RESEARCH & TECHNOLOGY FELUY
发明人： Virginie Cirriez , Alexandre Welle , Aurélien Vantomme , Pierre Bernard
IPC分类号： C08F210/16 , C08F4/659 , C08F4/6592
摘要： The present invention relates to a polyethylene resin prepared using a continuous process having and at least one metallocene catalyst composition:
a molecular weight distribution Mw/Mn lower than 6.5;
a molecular weight distribution Mw/Mn of at least 3.5;
a melt index ranging from an HLMI of at least 1.20 g/10 min to an MI2 of at most 6.0 g/10 min wherein MI2 is determined according to ISO 1133:1997 at a temperature of 190° C. and under a load of 2.16 kg, and HLMI is determined according to ISO 1133:1997, at a temperature of 190° C. and under a load of 21.6 kg;
melt index ratio HLMI/MI2 below or equal to 30; and
a melt strength of X in Newtons, as determined by Göttfert Rheotens Melt Strength Apparatus, 190° C., as described in the Experimental section, satisfying the following equations (1) and/or (2) X is greater than −0.026 ln(MI2)+0.0498 (1) X is greater than −0.026 ln(HLMI)+0.1334 (2) with Mw being the weight-average molecular weight and Mn being the number-average molecular weight.
The present invention also relates to articles comprising said polyethylene resin as well as process for preparing said resin.

6. 发明申请

US20210371636A1 Process for Producing Monovinylaromatic Polymer Incorporating Post-Consumer Recycled Polystyrene, Monovinylaromatic Polymer Incorporating Post-Consumer Recycled Polystyrene and Articles Produced Thereof 有权
公开(公告)号：US20210371636A1
公开(公告)日：2021-12-02
申请号：US17404491
申请日：2021-08-17
申请人： Total Research & Technology Feluy
发明人： Jose-Maria Pere , Antonio Guinovart , Armelle Sigwald , Laetitia Urbanczyk , Martine Slawinski , Pascal Charlier , Elodie Perche , Serge Eon , Thierry Marcoux , Matthieu Adam-Berret
IPC分类号： C08L25/06 , B29B17/02 , C08F257/02 , C08J11/04
摘要： The invention relates to a process and an installation to produce a monovinylaromatic polymer (3) comprising post-consumer recycled polystyrene (PCR-PS) wherein the process comprises the steps of mixing the PCR-PS (5) and the monovinylaromatic monomer (7) within a dissolver (9) to dissolve the PCR-PS (5) in the monovinylaromatic monomer (7) so as to produce a polymerization mixture (13); and a step of filtering the polymerization mixture (13) that includes continuously redirecting at least a part of the stream of the filtered polymerization mixture (17) back to the dissolver (9) and mixing it with the polymerization mixture (13) so as to continuously reduce the content of insoluble material in the polymerization mixture (13) contained in the dissolver (9).

7. 发明申请

US20210317238A1 Bis(Metallocene) Compounds and Catalyst Compositions Employing Such Compounds 有权
公开(公告)号：US20210317238A1
公开(公告)日：2021-10-14
申请号：US16330612
申请日：2017-09-07
申请人： Total Research & Technology Feluy , CENTRE NATIONAL DE LA RECHERCHE SCIENTIFIQUE (CNRS)
发明人： Alexandre Welle , Aurélien Vantomme , Jean-François Carpentier , Gilles Schnee , Olivier Miserque , Evgueni Kirillov
IPC分类号： C08F4/6592 , C08F4/642 , C08F210/02 , C08F210/06
摘要： The present invention relates to new bis(metallocene) compounds, new catalyst compositions, process for preparing the new bis(metallocene) compounds and use of said new catalyst compositions to polymerise olefins. The bis(metallocene) compounds of the invention are homo- or hetero bis(metallocene) molecules in which same or different metallocene moieties are connected by a phenylene bridge. The phenylene bridge is either para-substituted, meta-substituted or ortho-substituted by the two metallocene moieties.

8. 发明授权

US11124638B2 Process for producing monovinylaromatic polymer incorporating post-consumer recycled polystyrene, monovinylaromatic polymer incorporating post-consumer recycled polystyrene and articles produced thereof 有权
公开(公告)号：US11124638B2
公开(公告)日：2021-09-21
申请号：US16489231
申请日：2018-02-28
申请人： Total Research & Technology Feluy
发明人： Jose-Maria Pere , Antonio Guinovart , Armelle Sigwald , Laetitia Urbanczyk , Martine Slawinski , Pascal Charlier , Elodie Perche , Serge Eon , Thierry Marcoux , Matthieu Adam-Berret
IPC分类号： C08L25/06 , B29B17/02 , C08F257/02 , C08J11/04 , B29B17/00 , B29B17/04 , B29K25/00
摘要： The invention relates to a process and an installation to produce a monovinylaromatic polymer (3) comprising post-consumer recycled polystyrene (PCR-PS) wherein the process comprises the steps of mixing the PCR-PS (5) and the monovinylaromatic monomer (7) within a dissolver (9) to dissolve the PCR-PS (5) in the monovinylaromatic monomer (7) so as to produce a polymerization mixture (13); and a step of filtering the polymerization mixture (13) that includes continuously redirecting at least a part of the stream of the filtered polymerization mixture (17) back to the dissolver (9) and mixing it with the polymerization mixture (13) so as to continuously reduce the content of insoluble material in the polymerization mixture (13) contained in the dissolver (9).

9. 发明授权

US11117844B2 Method for dehydrating alcohols to obtain olefins, involving a step of catalyst selectivation 有权
公开(公告)号：US11117844B2
公开(公告)日：2021-09-14
申请号：US16629620
申请日：2018-07-10
申请人： TOTAL RESEARCH & TECHNOLOGY FELUY , IFP Energies Nouvelles
发明人： Nicolas Aribert , Vincent Coupard , Nikolai Nesterenko , Christophe Thille , Julie Mounier
IPC分类号： C07C1/24 , C07C11/09
摘要： The invention relates to a process for dehydrating alcohols to olefins, comprising a reaction step and a catalyst selectivation step.

10. 发明申请

US20210221985A1 Polyolefin Compositions 有权
公开(公告)号：US20210221985A1
公开(公告)日：2021-07-22
申请号：US16095886
申请日：2017-04-25
申请人： Total Research & Technology Feluy
发明人： Claire Bouvy , Olivier Miserque , Jaques Michel
IPC分类号： C08L23/06 , B29C48/00
摘要： The present invention relates to a polyolefin composition comprising: a) at least one first polyolefin having a multimodal molecular weight distribution and prepared in the presence of at least one metallocene catalyst; and b) at least one second polyolefin having a Mw/Mn of at least 10.0 and a long chain branching index grheo of at least 0.85, wherein said second polyolefin is present in an amount of at least 1.0% by weight based on the total weight of the polyolefin composition; wherein the second polyolefin has a High Load Melt Index of at least 0.60 times the High Load Melt Index HLMI of the first polyolefin and of at most 1.40 times the High Load Melt Index HLMI of the first polyolefin, as measured following the procedure of ISO 1133 condition G using a temperature of 190° C. and a load of 21.6 kg. The present invention also relates to processes for preparing said composition, and articles made therefrom.

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