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1. 发明授权

US07393467B2 Wholly aromatic liquid-crystalline polyester and method for preparing the same 有权
标题翻译：全芳族液晶聚酯及其制备方法
公开(公告)号：US07393467B2
公开(公告)日：2008-07-01
申请号：US11341625
申请日：2006-01-30
申请人： Motoki Asahara , Tetsuhide Sawada , Hiroyuki Kato
发明人： Motoki Asahara , Tetsuhide Sawada , Hiroyuki Kato
IPC分类号： C09K19/52 , C09K19/32 , C09K19/20 , C09K19/38 , C08G63/00
CPC分类号： C08G63/605 , C08G63/80
摘要： Provided is a liquid-crystalline polyester with good properties obtainable by subjecting a prepolymer consisting of the repeating units represented by formulae (I), (II), (III) and (IV): to heat treatment in a substantially solid state.
摘要翻译：本发明提供一种具有良好性能的液晶聚酯，其通过使由式（I），（II），（III）和（IV）表示的重复单元组成的预聚物以基本上固态进行热处理而得到。

2. 发明授权

US07355071B2 Method for preparing 2,6-naphthalene dicarboxylic acid 有权
标题翻译： 2,6-萘二甲酸的制备方法
公开(公告)号：US07355071B2
公开(公告)日：2008-04-08
申请号：US11090054
申请日：2005-03-28
申请人： Masaya Kitayama , Hiroyuki Wakamori
发明人： Masaya Kitayama , Hiroyuki Wakamori
IPC分类号： C07C51/42
CPC分类号： C07C51/09 , C07C63/38
摘要： Disclosed is an improved method for preparing 2,6-naphthalene dicarboxylic acid from di-lower alkyl 2,6-naphthalene dicarboxylate, which is characterized in that hydrolyzing di-lower alkyl 2,6-naphthalene dicarboxylate in a specified amount of water in the presence of specified amount of hydrophobic organic solvent and an additive; that hydrolyzing di-lower alkyl 2,6-naphthalene dicarboxylate in a specific amount of a mixed solvent of non-water miscible alcohol and water; or in that di-lower alkyl 2,6-naphthalene dicarboxylate is hydrolyzed in two steps wherein the 1st step comprises hydrolyzing said ester in a water miscible organic solvent in the presence of a small amount of water, and the 2nd step comprises further hydrolyzing the reaction.
摘要翻译：本发明公开了一种从2,6-二萘基二羧酸二低级烷基酯制备2,6-萘二羧酸的改进方法，其特征在于将2,6-萘二羧酸二低级烷基酯在规定量的水中存在规定量的疏水性有机溶剂和添加剂; 在特定量的非水混溶性醇和水的混合溶剂中水解2,6-萘二甲酸二低级烷基酯; 或者在2,6-二羧酸二低级烷基酯中以两个步骤水解，其中第一步包括在少量水存在下在水混溶性有机溶剂中水解所述酯，第二步包括进一步水解反应。

3. 发明申请

US20060084747A1 Method for manufacturing wholly aromatic liquid-crystalline polyester resin 失效
标题翻译：全芳香族液晶聚酯树脂的制造方法
公开(公告)号：US20060084747A1
公开(公告)日：2006-04-20
申请号：US11245200
申请日：2005-10-07
申请人： Motoki Asahara , Toshiki Nishino
发明人： Motoki Asahara , Toshiki Nishino
IPC分类号： C08K3/34 , C08K3/40
CPC分类号： C08G63/78 , C08G63/065 , C08G63/19 , C08G63/605
摘要： The present invention provides a method for manufacturing a wholly aromatic liquid-crystalline polyester resin comprising the steps of: 1) acylating the hydroxy group of major monomer components selected from the group consisting of aromatic hydroxycarboxylic acid, aromatic diol and aromatic dicarboxylic acid, with an acylating agent, provided that said major monomer components comprise at least one of aromatic hydroxycarboxylic acid and aromatic diol; and 2) polycondensing said major monomer components of which hydroxy group is acylated, wherein, the polycondensation reaction is carried out in the presence of a metal dihydrogen phosphate in an amount of 1-5000 ppm based on the total monomer components, and a liquid-crystalline polyester resin manufactured by the method and a composition comprising said resin.
摘要翻译：本发明提供一种全芳香族液晶聚酯树脂的制造方法，包括以下步骤：1）将选自芳族羟基羧酸，芳族二醇和芳族二羧酸的主要单体成分的羟基与所述主要单体组分包含芳族羟基羧酸和芳族二醇中的至少一种; 和2）缩聚其羟基被酰化的所述主要单体成分，其中缩聚反应在磷酸金属盐存在下以基于总单体组分的1-5000ppm的量存在下进行，通过该方法制造的结晶性聚酯树脂和包含所述树脂的组合物。

4. 发明授权

US06984712B2 Liquid-crystal polyester resin 有权
标题翻译：液晶聚酯树脂
公开(公告)号：US06984712B2
公开(公告)日：2006-01-10
申请号：US10496490
申请日：2002-11-25
申请人： Ryuzo Ueno , Masaya Kitayama , Kiichi Kometani , Hiroyuki Kato , Kazunori Ueda
发明人： Ryuzo Ueno , Masaya Kitayama , Kiichi Kometani , Hiroyuki Kato , Kazunori Ueda
IPC分类号： C08G63/06 , C08F20/00 , C09K19/32
CPC分类号： C08G63/605 , C08G63/06 , C08G63/19 , C08G63/20 , C09K19/3809
摘要： The present invention provides a liquid-crystalline polyester resin which comprises monomer units derived from 2-hydroxy-3-naphthoic acid and/or 2-hydroxynaphthalene-3,6-dicarboxylic acid in an amount of 1-5000 mmol % based on the total monomer components of the resin and an alkaline metal compound in an amount of 10-3000 ppm as alkaline metal based on the total monomer components of the resin. The liquid-crystalline polyester resin of the present invention has good colorability, improved heat resistance and good mechanical properties.
摘要翻译：本发明提供一种液晶聚酯树脂，其包含基于总量为1-5000mmol％的来源于2-羟基-3-萘甲酸和/或2-羟基萘-3,6-二羧酸的单体单元树脂的单体组分和碱金属化合物，其量为基于树脂总单体成分的碱金属为10-3000ppm。本发明的液晶聚酯树脂具有良好的着色性，耐热性和良好的机械性能。

5. 发明申请

US20050256289A1 Method for joining liquid-crystalline polyester resin composition parts and jointed article made of liquid-crystalline polyester resin composition 有权
标题翻译：液晶聚酯树脂组合物部分的接合方法和由液晶聚酯树脂组合物制成的接合体
公开(公告)号：US20050256289A1
公开(公告)日：2005-11-17
申请号：US11125240
申请日：2005-05-10
申请人： Masaya Kitayama , Naoshi Saito
发明人： Masaya Kitayama , Naoshi Saito
IPC分类号： C08J5/12 , C08G63/60 , F16B19/00 , C08G63/00
CPC分类号： C08G63/605 , B29C65/02 , B29C65/04 , B29C65/06 , B29C65/0672 , B29C65/08 , B29C65/222 , B29C65/224 , B29C65/36 , B29C65/38 , B29C66/126 , B29C66/54 , B29C66/71 , B29C66/721 , B29C66/7212 , B29C66/73115 , B29C66/73776 , B29C66/73921 , B29C66/73941 , B29K2509/10 , B29K2067/00 , B29K2309/08 , B29K2309/02 , B29K2307/04 , B29K2277/10
摘要： The present invention provides a method for joining liquid-crystalline polyester resin composition parts, characterized in that the melting point of the liquid crystalline polyester resin measured by differential scanning calorimeter is 190-250° C. and that the parts are jointed by means of welding. By using the method of the present invention, jointed articles with sufficient joint strength are provided with accuracy.
摘要翻译：本发明提供了一种用于接合液晶聚酯树脂组合物部件的方法，其特征在于用差示扫描量热计测量的液晶聚酯树脂的熔点为190-250℃，通过焊接将部件接合。通过使用本发明的方法，提供了具有足够接合强度的接合制品。

6. 发明申请

US20050192442A1 Method for preparing 2-hydroxy-6-ureidocarbonyl naphthalene derivative 失效
标题翻译： 2-羟基-6-脲基羰基萘衍生物的制备方法
公开(公告)号：US20050192442A1
公开(公告)日：2005-09-01
申请号：US11048876
申请日：2005-02-03
申请人： Masaya Kitayama , Hiroyuki Wakamori , Nobuhiro Yonetani
发明人： Masaya Kitayama , Hiroyuki Wakamori , Nobuhiro Yonetani
IPC分类号： C07C275/54 , C07C273/02 , C07C273/06 , C07C273/18 , C07D235/22 , C07C273/00
CPC分类号： C07C273/1827 , C07C275/54
摘要： Disclosed is a method for preparing a 2-hydroxy-6-ureidocarbonyl naphthalene derivative. The method comprises the step of reacting 2-hydroxy-6-aminocarbonyl naphthalene and a isocyanate in an organic solvent at a temperature of 90-200° C. According to the present invention, 2-hydroxy-6-ureidocarbonyl naphthalene derivative can easily be obtained within relatively short time and high yield.
摘要翻译：公开了2-羟基-6-脲基羰基萘衍生物的制备方法。该方法包括在90-200℃的温度下，使2-羟基-6-氨基羰基萘与异氰酸酯在有机溶剂中反应的步骤。根据本发明，2-羟基-6-脲基羰基萘衍生物可容易地在相对较短的时间内获得较高的产量。

7. 发明授权

US06891072B2 Process for production of dimers or aromatic monohydroxyl compounds 失效
标题翻译：二聚体或芳族单羟基化合物的制备方法
公开(公告)号：US06891072B2
公开(公告)日：2005-05-10
申请号：US10433908
申请日：2002-04-18
申请人： Ryuzo Ueno , Masaya Kitayama , Kenji Minami , Hiroyuki Wakamori , Hikari Hirai
发明人： Ryuzo Ueno , Masaya Kitayama , Kenji Minami , Hiroyuki Wakamori , Hikari Hirai
IPC分类号： C07B61/00 , C07C37/11 , C07C39/14 , C07C45/39 , C07C46/08 , C07C49/653 , C07C67/343 , C07C69/94 , C07C231/12 , C07C235/66 , C07C273/18 , C07C275/54 , C07D307/52 , C07C39/12
CPC分类号： C07D307/52 , C07C37/11 , C07C46/08 , C07C67/343 , C07C231/12 , C07C273/1854 , C07C2603/50 , C07C50/10 , C07C50/08 , C07C69/94 , C07C235/66 , C07C275/54 , C07C39/14
摘要： The present invention provides a method for preparing dimer of a monohydroxy aromatic compound. In the method of the present invention, oxidative coupling reaction of a monohydroxy aromatic compound represented by formula [I]: Ar—OH [I] wherein Ar represents an optionally substituted aromatic group is carried out in a nitrogen containing polar solvent in the presence of a copper salt. By the method of the instant invention, dimer of the monohydroxy aromatic compound can be obtained in high yield.
摘要翻译：本发明提供一种制备单羟基芳族化合物的二聚体的方法。在本发明的方法中，由式[I]表示的单羟基芳族化合物的氧化偶联反应：<？in-line-formula description =“In-line Formulas”end =“lead”→Ar-OH [I ]其中Ar表示可以具有取代基的芳族基团，在含铜极性溶剂中，在铜盐存在下进行。通过本发明的方法，可以高产率获得单羟基芳族化合物的二聚体。

8. 发明授权

US06849742B2 Binaphthol derivative and process for producing the same 失效
标题翻译：联萘酚衍生物及其制备方法
公开(公告)号：US06849742B2
公开(公告)日：2005-02-01
申请号：US10250442
申请日：2002-04-18
申请人： Ryuzo Ueno , Masaya Kitayama , Kenji Minami , Hiroyuki Wakamori
发明人： Ryuzo Ueno , Masaya Kitayama , Kenji Minami , Hiroyuki Wakamori
IPC分类号： C07B57/00 , C07B61/00 , C07C51/09 , C07C51/353 , C07C51/367 , C07C51/60 , C07C65/11 , C07C65/24 , C07C67/31 , C07C67/343 , C07C69/94 , C07C231/12 , C07C235/66 , C07C273/18 , C07C275/54 , C07D263/56 , C07D263/57 , C07D263/62 , C07D263/64 , C07D277/66 , C07D307/52 , C07D277/62
CPC分类号： C07D263/57 , C07B2200/07 , C07C51/09 , C07C51/367 , C07C51/60 , C07C65/11 , C07C65/24 , C07C67/31 , C07C67/343 , C07C69/94 , C07C235/66 , C07C2603/50 , C07D263/64 , C07D277/66 , C07D307/52
摘要： The present invention provides a binaphthol compound represented by formula [1]: and a salt thereof. The binaphthol compound of the present invention is useful for manufacturing antiseptic compounds or chiral catalysts. According to the method of the present invention, binaphthol compounds can be prepared in high yield with low cost.
摘要翻译：本发明提供由式[1]表示的联萘酚化合物及其盐。本发明的联萘酚化合物可用于制备防腐化合物或手性催化剂。根据本发明的方法，可以低成本高收率制备联萘酚化合物。

9. 发明授权

US5468880A Method of producing .alpha., .beta.-unsaturated ketones 失效
标题翻译：生产α，β-不饱和酮的方法
公开(公告)号：US5468880A
公开(公告)日：1995-11-21
申请号：US244566
申请日：1994-05-31
申请人： Ryuji Ueno , Tomio Oda
发明人： Ryuji Ueno , Tomio Oda
IPC分类号： C07C405/00 , C07D307/935 , C07D309/12 , C07D313/00 , C07D407/12 , C07D305/00
CPC分类号： C07D307/935 , C07C405/00 , C07D309/12 , C07D313/00 , C07D407/12
摘要： Improvement in the technique of synthesizing prostaglandins, particularly those having at least one halogen atom at the 16- or 17-position, which comprises introducing a .omega. chain into the aldehyde thereby to enable considerable yield improvement in the production of .alpha.,.beta.-unsaturated ketones, and which does not involve hydrogen generation and can insure safe operation.A method of producing .alpha.,.beta.-unsaturated ketones by reacting aldehyde with 2-oxoalkyl phosphonate, wherein the reaction was carried out under the presence of a base and a zinc compound.
摘要翻译：合成前列腺素的技术的改进，特别是在16位或17位具有至少一个卤原子的前列腺素的技术，其包括将ω-链引入醛中，从而使α，β-不饱和酮的产生显着提高产量，不涉及氢气生成，可以保证安全运行。一种通过醛与2-氧代烷基膦酸酯反应制备α，β-不饱和酮的方法，其中反应在碱和锌化合物的存在下进行。

10. 发明授权

US5362751A Tracheobronchodilator using 16-substituted PGEs 失效
标题翻译：气管支气管扩张剂使用16取代的PGE
公开(公告)号：US5362751A
公开(公告)日：1994-11-08
申请号：US77495
申请日：1993-06-17
申请人： Ryuzo Ueno , Ryuji Ueno , Tomio Oda
发明人： Ryuzo Ueno , Ryuji Ueno , Tomio Oda
IPC分类号： A61K31/557 , A61K31/215 , A61K31/20
CPC分类号： A61K31/557
摘要： The present invention provides a tracheobronchodilator comprising 15-keto-PGEs, reduced in stimuli against bronchi and other side effects.
摘要翻译：本发明提供一种气管支气管扩张剂，其包含减少对支气管的刺激和其它副作用的15-酮-PGE。

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