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1. 发明授权

US4824979A Method for the preparation of partial esters and ortho esters of titanium, zirconium or hafnium 失效
标题翻译：钛，锆或铪的偏酯和原酸酯的制备方法
公开(公告)号：US4824979A
公开(公告)日：1989-04-25
申请号：US810514
申请日：1985-12-18
申请人： Hans-Joachim Kotzsch , Hans-Gunther Srebny , Hans-Joachim Vahlensieck
发明人： Hans-Joachim Kotzsch , Hans-Gunther Srebny , Hans-Joachim Vahlensieck
IPC分类号： C08F4/00 , C07F7/00 , C07F7/28 , C08F4/42 , C08F4/76 , C08G85/00
CPC分类号： C07F7/006
摘要： Disclosed is a new method for the preparation of metallic acid esters of titanium, zirconium or hafnium wherein a halide of the metal reacts with an organosilane ester, resulting in the formation of partial esters of the metallic acids. The degree of esterification of the metallic acid ester can be controlled based on the organosilane ester and it is possible to obtain complete esterification of the metal halides. The metallic acid partial esters prepared by the method are very pure, and can be separated selectively from the mixture in a simple manner. The metallic acid alkyl esters obtained can very easily be further esterified to the metallic acid tetraalkyl esters with the formation of very pure tetraalkyl esters.
摘要翻译：公开了一种制备钛，锆或铪的金属酸酯的新方法，其中金属的卤化物与有机硅烷酯反应，导致形成金属酸的偏酯。可以基于有机硅烷酯来控制金属酸酯的酯化程度，并且可以获得金属卤化物的完全酯化。通过该方法制备的金属酸偏酯是非常纯的，并且可以以简单的方式从混合物中选择性地分离。获得的金属酸性烷基酯可以非常容易地进一步酯化成金属酸四烷基酯，形成非常纯的四烷基酯。

2. 发明授权

US4946977A Method for the preparation of organosilanes containing methacryloxy or acryloxy groups 失效
标题翻译：含有甲基丙烯酰氧基或丙烯酰氧基的有机硅烷的制备方法
公开(公告)号：US4946977A
公开(公告)日：1990-08-07
申请号：US246317
申请日：1988-09-19
申请人： Gunther Bernhardt , Jurgen Amort , Margret Haas , Horst Hanisch , Heinz Kragl
发明人： Gunther Bernhardt , Jurgen Amort , Margret Haas , Horst Hanisch , Heinz Kragl
IPC分类号： B01J31/02 , C07B61/00 , C07F7/18
CPC分类号： C07F7/1892
摘要： The present invention is in the preparation of methacrylic or acryloxyalkylalkoxysilanes by the reaction at a temperature of from 80.degree. and 130.degree. C. of an alkali (meth) acrylate with a halogen alkylalkoxysilane in the presence of a quaternary ammonium salt which has long-chin alkyl moieties, in which the sum of all carbon atoms is between 10 and 40 as a phase-transfer catalyst. In the new procedure no solvents need to be used. The yields are better than 95%.
摘要翻译：本发明是在碱性（甲基）丙烯酸烷基酯与卤代烷基烷氧基硅烷的存在下，在具有长下巴的季铵盐的存在下，在80℃和130℃的温度下反应制备甲基丙烯酸或丙烯酰氧基烷基烷氧基硅烷烷基部分，其中所有碳原子的总和为10〜40，作为相转移催化剂。在新程序中，不需要使用溶剂。收益率优于95％。

3. 发明授权

US4908471A Method for the production of benzene carboxylic acids and benzene dicarboxylic acid esters 失效
标题翻译：苯羧酸和苯二羧酸酯的制备方法
公开(公告)号：US4908471A
公开(公告)日：1990-03-13
申请号：US156257
申请日：1988-02-16
申请人： Hans Leuck , Hans-Jorg Westermann
发明人： Hans Leuck , Hans-Jorg Westermann
IPC分类号： C07C69/82 , B01J19/00 , B01J19/26 , B01J31/04 , C07B61/00 , C07C27/00 , C07C27/12 , C07C51/265 , C07C63/04 , C07C63/06 , C07C67/00 , C07C67/39
CPC分类号： C07C51/265 , B01J19/26 , C07C67/39 , B01J2219/00103 , B01J2219/00126
摘要： Disclosed is a method for the production of benzene carboxylic acids and benzene carboxylic acid esters or their mixtures, while p-toloylic acid is made from p-xylene and terephthalic acid monomethyl ester is simultaneously prepared from p-toluylic acid ester. The oxidation is performed by the addition of oxidator liquid and gases containing oxygen in single orifice mixing nozzles with the formation of a highly disperse reaction phase and the single orifice mixing nozzles open into the oxidator liquid.
摘要翻译：公开了用于制备苯羧酸和苯羧酸酯或其混合物的方法，而对甲苯酸由对二甲苯制备，对苯二甲酸单甲酯由对甲苯甲酸酯同时制备。通过在单孔混合喷嘴中加入氧化剂液体和含氧气体，形成高度分散的反应相，并且单孔混合喷嘴通入氧化剂液体中进行氧化。

4. 发明授权

US4783564A Method for the preparation of 1,2-dichloroethane 失效
标题翻译： 1,2-二氯乙烷的制备方法
公开(公告)号：US4783564A
公开(公告)日：1988-11-08
申请号：US102291
申请日：1987-09-25
申请人： Bernhard Piotrowski , Roland Schildhauer , Kurt Deselaers , Wolfgang Merkel
发明人： Bernhard Piotrowski , Roland Schildhauer , Kurt Deselaers , Wolfgang Merkel
IPC分类号： B01J23/00 , C07B61/00 , C07C17/00 , C07C17/02 , C07C19/045 , C07C67/00
CPC分类号： C07C17/02
摘要： A method is disclosed for the preparation of 1,2-dichloroethane in a reactor by the reaction of gaseous ethylene with chlorine dissolved in a hot, catalyst-containing, liquid circulating stream that is under elevated pressure and consists of chlorinated hydrocarbons. All of the chlorine is absorbed outside of the reactor, at a temperature above 90.degree. C., a pressure of more than 4 bar, and an average residence time of less than 120 seconds. The reaction takes place at the phase boundary surface of a dispersion produced from gaseous ethylene and the chlorine-containing, liquid, circulating stream, at an energy dissipation density of 0.05 to 1000 kilowatts per cubic meter, a temperature of 90.degree. to 200.degree. C., and a pressure of 7 to 20 bar. Iron(III) chloride is used preferably as catalyst. Oxygen is used preferably as inhibitor for preventing the formation of byproducts. The separation of the unreacted amounts of ethylene and chlorine as well as other gaseous components from the product-containing circulating stream is performed preferably in an expansion tank.
摘要翻译：公开了一种在反应器中通过气态乙烯与氯溶解在热的含催化剂的液体循环流中的氯气的反应来制备1,2-二氯乙烷的方法，所述热的含催化剂的液体循环流在升高的压力下由氯代烃组成。所有氯在反应器外部被吸收，温度高于90℃，压力大于4巴，平均停留时间小于120秒。反应发生在由气态乙烯和含氯液体循环流产生的分散体的相界面处，能量耗散密度为0.05〜1000千瓦/立方米，温度为90〜200℃ 压力为7至20巴。优选使用氯化铁（III）作为催化剂。氧优选用作防止副产物形成的抑制剂。优选在膨胀罐中进行未反应量的乙烯和氯以及其它气态成分从含产物循环流中的分离。

5. 发明授权

US2249835A Magnetostrictive vibrator 失效
公开(公告)号：US2249835A
公开(公告)日：1941-07-22
申请号：US17396937
申请日：1937-11-11
申请人： BELL TELEPHONE LABOR INC
发明人： EMORY LAKATOS
IPC分类号： H04R15/00
CPC分类号： H04R15/00 , Y10T156/1317

6. 发明授权

US2023596A Method of and apparatus for making scales 失效
标题翻译：秤的制作方法及装置
公开(公告)号：US2023596A
公开(公告)日：1935-12-10
申请号：US57458431
申请日：1931-11-12
申请人： WESTERN ELECTRIC CO
发明人： JOSEPH KOCI LUDVIK
IPC分类号： B41F17/00
CPC分类号： B41F17/00

7. 发明授权

US5244942A Homogenous, particularly multicolor-structured synthetic resin sheet or panel, as well as process for its production 失效
标题翻译：均匀的，特别是多色结构的合成树脂板或面板，以及其生产方法
公开(公告)号：US5244942A
公开(公告)日：1993-09-14
申请号：US936889
申请日：1992-08-31
申请人： Alexander Hover , Manfred Simon , Herbert Schulte , Josef Becker , Richard Weiss , Hans-Joachim Kaseler
发明人： Alexander Hover , Manfred Simon , Herbert Schulte , Josef Becker , Richard Weiss , Hans-Joachim Kaseler
IPC分类号： B29C43/00 , C08K3/00 , D06N7/00
CPC分类号： B29C43/003 , C08K3/0033 , D06N7/0028 , B29K2105/251 , B29K2995/0021 , Y10S524/914
摘要： The invention concerns a homogenous, in particular multicolored plastic sheet or panel, based on ethylene vinyl acetate copolymer (EVA) as binder with a filler content of 30 to 80 wt. % and a process for producing it. In other embodiments the binder contains, in addition to the 70 to 85 wt. % of EVA, polypropylenes to improve the processability (tendency to adhere), EPDM to improve the flexibility, and polyethylenes to reduce the tendency to soiling. In the process described, several additives, each consisting of a binder containing at least some ethylene vinyl acetate copolymer, up to 80 wt. % of fillers and up to 5 wt. % of pigments, are mixed, plasticized and granulated or comminuted to form granules or chips of assorted colours which are mixed and, possibly after other processing operations, pressed to form the plastic web or plates.
摘要翻译：本发明涉及基于乙烯醋酸乙烯酯共聚物（EVA）作为粘合剂的均匀的，特别是多色塑料片或面板，填料含量为30至80重量％。％和一个生产过程。在其它实施方案中，除70至85wt。％的EVA，聚丙烯提高加工性（倾向于粘附），改善EPDM的柔韧性，并减少聚乙烯的污染倾向。在所描述的方法中，几种添加剂，每种添加剂由含有至少一些乙烯 - 乙酸乙烯酯共聚物的粘合剂组成，最多80wt。填料％和最多5wt。颜料的百分比被混合，塑化和造粒或粉碎以形成混合的各种颜色的颗粒或碎片，并且可能在其它加工操作之后被压制以形成塑料网或板。

8. 发明授权

US4931094A Titanium(IV)-chelates and their use in printing inks 失效
标题翻译：钛（IV） - 它们在印刷油墨中的应用
公开(公告)号：US4931094A
公开(公告)日：1990-06-05
申请号：US252700
申请日：1988-10-03
申请人： Dieter Barfurth , Claus Lindzus , Heinz Nestler
发明人： Dieter Barfurth , Claus Lindzus , Heinz Nestler
IPC分类号： C07F7/28 , C07F7/00 , C09D11/02 , C09D11/14
CPC分类号： C07F7/006 , C09D11/14
摘要： Novel alkoxy titanium(IV)-chelates are used to modify printing inks based on nitrocellulose or other cellulose ester derivatives. The novel chelates comprise citric acid alkyl esters as chelate formers. They delay, as other titanium chelates do, the well-known catalytic effect of the titanium component in cross-linking reactions. When used in printing inks, the novel titanium chelates and their alcoholic solutions have the advantage that they have an insignificant color of their own, so that they practically do not discolor the printing inks. A further advantage of the novel chelates resides in that they do not enter into alteration effects with antioxidants based on phenol, so that they can also be used for printing inks which are to be applied to polymeric substrates containing such antioxidants without the occurence of discoloration.
摘要翻译：新型烷氧基钛（IV） - 螯合物用于改性基于硝化纤维素或其它纤维素酯衍生物的印刷油墨。新型螯合物包括柠檬酸烷基酯作为螯合物。与其他钛螯合物一样，它们延迟钛组分在交联反应中的众所周知的催化作用。当用于印刷油墨时，新型钛螯合物及其醇溶液的优点在于它们本身具有无色的颜色，因此它们实际上不会使印刷油墨变色。新型螯合物的另一个优点在于它们不会以基于苯酚的抗氧化剂引起改变效果，因此它们也可以用于印刷油墨，这些油墨应用于含有这种抗氧化剂的聚合物基材上，而不发生变色。

9. 发明授权

US4923658A Process for the production of dyed, flat articles from thermoplastic synthetic resins 失效
标题翻译：从热塑性合成树脂生产染色扁平制品的方法
公开(公告)号：US4923658A
公开(公告)日：1990-05-08
申请号：US250151
申请日：1988-09-28
申请人： Alexander Hover , Manfred Simon , Richard Weiss
发明人： Alexander Hover , Manfred Simon , Richard Weiss
IPC分类号： B05D7/02 , B29B17/00 , B29C43/00 , B29C43/22 , B29C43/30 , B29C43/48 , B29C67/04 , B44C1/04 , B44C3/08
CPC分类号： B44C3/08 , B05D7/04 , B29B17/00 , B29C43/006 , B29C43/22 , B29C43/30 , B29C43/48 , B29C67/04 , B44C1/04 , B05D5/06 , B29C2791/002 , B29K2027/06 , B29K2105/251 , B29K2995/0021 , Y02W30/62
摘要： A process for the production of homogeneous flat articles of thermoplastic synthetic resins wherein a starting mixture based on thermoplastic synthetic resins is processed into agglomerate or granulated material by a thermal pretreatment above the softening temperature and subsequently, optionally after additional intermediate steps, is mechanically comminuted to a mixture of particles having a random grain size distribution. The mixture of particles is piled continuously onto a conveyor belt to form a uniform layer and is sintered, under the action of heat up to the plasticization of the thermoplastic synthetic resin, into a coherent flat articles and is then press-molded under the effect of pressure and heat. The pourable powders or particles are formed from a blend of differently colored agglomerates or granules prepared in a predetermined mixing ratio; the blend being obtained from several colored batches of thermoplastic resin, each batch having a different color from the other and each batch being heat treated above the softening point of the thermoplastic resin. In one variation of the process, at least one liquid or pourable, meltable, colored medium is applied in predetermined patterns and penetrates into the sintered layer up to a desired depth, in particular throughout the entire layer thickness; and thereafter the dyed, sintered layer is compressed under the action of pressure and heat into a compact flat article.
摘要翻译：一种用于生产热塑性合成树脂的均匀扁平制品的方法，其中基于热塑性合成树脂的起始混合物通过高于软化温度的热预处理而被加工成附聚物或造粒材料，随后任选地在另外的中间步骤之后机械粉碎成具有随机粒度分布的颗粒的混合物。将颗粒混合物连续堆积在输送带上以形成均匀的层，并在加热至热塑性合成树脂的塑化作用下烧结成粘合的平坦物品，然后在压力和热量。可倾倒粉末或颗粒由以预定混合比制备的不同颜色的附聚物或颗粒的共混物形成; 该混合物由几批彩色批次的热塑性树脂获得，每批具有不同的颜色，每批在热塑性树脂的软化点之上进行热处理。在该方法的一个变型中，以预定图案施加至少一种液体或可倾倒的，可熔化的有色介质，并且穿透到所需的深度，特别是贯穿整个层厚度; 然后将染色的烧结层在压力和热力的作用下压缩成紧凑的扁平制品。

10. 发明授权

US4876337A Method and apparatus for the preparation of cyanoalkyl-alkoxysilanes 失效
标题翻译：用于制备氰基烷基 - 烷氧基硅烷的方法和设备
公开(公告)号：US4876337A
公开(公告)日：1989-10-24
申请号：US278736
申请日：1988-12-02
申请人： Hartwig Rauleder , Claus-Dietrich Seiler , Hans-Joachim Vahlensieck
发明人： Hartwig Rauleder , Claus-Dietrich Seiler , Hans-Joachim Vahlensieck
IPC分类号： C07F7/18
CPC分类号： C07F7/1892
摘要： In a method of preparing cyanoalkyl-akoxysilanes, which is suitable for the production of these silanes on a large technical scale, the reaction of a chloroalkyl-alkoxysilane with an alkali metal cyanide in the presence of a solvent takes place in a stirring reactor which is provided with means for loading these starting materials and with an outlet opening for the alkali metal chloride by-product, and which is connected through a bypass valve to a column with a superimposed condenser. After the reaction in the reactor has ended, first the solvent is distilled out through the column and then the main part of the cyanosilane, and then the rest of the cyanosilane is distilled out while bypassing the column. The alkali metal chloride is then removed from the reactor through a lock.
摘要翻译：在适用于大规模生产这些硅烷的氰基烷基 - 烷氧基硅烷的制备方法中，在溶剂存在下氯烷基烷氧基硅烷与碱金属氰化物的反应在搅拌反应器中进行，提供了用于装载这些原料的装置和用于碱金属氯化物副产物的出口，并且通过旁通阀连接到具有叠加的冷凝器的塔。在反应器中的反应结束后，首先通过柱蒸馏除去溶剂，然后将氰基硅烷的主要部分蒸馏掉，然后在绕过柱子的同时蒸馏掉其余的氰基硅烷。然后通过锁从反应器中除去碱金属氯化物。

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