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    • 4. 发明授权
    • Method for the preparation of a high-quality powder of amorphous silicic
acid
    • 制备无定形硅酸高品质粉末的方法
    • US6068825A
    • 2000-05-30
    • US213376
    • 1998-12-17
    • Shuji Tsunematsu
    • Shuji Tsunematsu
    • B01D37/02C01B33/18C01B33/187C01B33/193C01B33/12
    • C01B33/187C01P2002/02C01P2004/61C01P2006/10C01P2006/12C01P2006/60
    • Disclosed is an improvement in the process for the preparation of amorphous silicic acid particles useful, for example, as a filtration aid comprising the steps of a hydrothermal reaction to prepare calcium silicate particles and decalcification of the calcium silicate particles, after or without undertaking carbonation by the reaction of carbon dioxide, with an acid to form particles of amorphous silicic acid followed by drying of the amorphous silicic acid particles. Different from the conventional methods in which great shrinkage of the amorphous silicic acid cakes wet with water is unavoidable in the drying step to adversely affect the quality of the product, the final step of treatment preceding drying of the wet cake is undertaken in a liquid medium which is a mixture of water and a water-miscible organic solvent such as ethyl alcohol in a specified proportion so that the drying of the wet cake is performed without the disadvantage due to the large surface tension of water responsible to the drying shrinkage of wet cakes.
    • 公开了用于制备无定形硅酸颗粒的方法的改进,所述无定形硅酸颗粒可用作例如作为过滤助剂,其包括以下步骤:水热反应以制备硅酸钙颗粒和脱硅钙硅酸盐颗粒,在或不进行碳酸化之后 二氧化碳与酸反应形成无定形硅酸颗粒,然后干燥无定形硅酸颗粒。 与在干燥步骤中不可避免地使无定形硅酸蛋糕用水湿润的大的收缩率不利地影响产品质量的常规方法不同,在湿滤饼干燥之前的处理的最后步骤在液体介质中进行 其是水和水混溶性有机溶剂如乙醇的混合物,以规定的比例进行,从而干燥湿滤饼的干燥不会因为湿蛋糕的干燥收缩引起的水的表面张力大而不利 。