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1. 发明申请

US20060272546A1 Inks containing water-soluble perylene dyes and their use in ink-jet printing 失效
标题翻译：含有水溶性苝染料的油墨及其在喷墨印刷中的用途
公开(公告)号：US20060272546A1
公开(公告)日：2006-12-07
申请号：US10558072
申请日：2004-04-07
申请人： Clive Foster , David Schofield , Helen O'Shaughnessy
发明人： Clive Foster , David Schofield , Helen O'Shaughnessy
IPC分类号： C09D11/00 , C09D11/02 , C07D221/22
CPC分类号： C09K19/3483 , C09B5/62 , C09D11/328 , C09K19/60 , C09K19/606
摘要： An ink comprising a liquid medium and a colorant, wherein the liquid medium comprises water and a water-miscible organic solvent and the colorant is of Formula (1), wherein the colorant is dissolved in the liquid medium: Formula (1) wherein: each independently is a water-solubilising group selected from sulfo, carboxy, phosphato and poly(ethylene oxide); each Z independently is optionally substituted alkyl, optionally substituted aryl or optionally substituted aralkyl; each Q independently is a direct bond or —NR— wherein R is H, optionally substituted aryl or optionally substituted alkyl; rings A,B,C and D are each independently unsubstituted or carry a substituent selected from optionally substituted alkyl, optionally substituted aryl and optionally substituted aralkyl; each n independently is from 1 to 3; and each m independently is 0, 1 or 2; provided that when either or both of the groups represented by Q is a direct bond then at least one n has a value of at least 2. Also colourants and ink-jet printing processes, cartridges and prints.
摘要翻译：一种包含液体介质和着色剂的油墨，其中所述液体介质包括水和水混溶性有机溶剂，并且所述着色剂具有式（1），其中所述着色剂溶解在液体介质中：式（1）其中：独立地是选自磺基，羧基，磷酸酯和聚（环氧乙烷）的水溶性基团; 每个Z独立地是任选取代的烷基，任选取代的芳基或任选取代的芳烷基; 每个Q独立地是直接键或-NR-，其中R是H，任选取代的芳基或任选取代的烷基; 环A，B，C和D各自独立地是未取代的或携带选自任选取代的烷基，任选取代的芳基和任选取代的芳烷基的取代基; 每个n独立地为1至3; 并且每个m独立地为0,1或2; 条件是当由Q表示的基团中的任一个或两个是直接键合时，至少一个n的值至少为2.还有着色剂和喷墨印刷方法，墨盒和印刷品。

2. 发明授权

US07138548B2 Process for the preparation of aryl hydrazone and aryl hydrazine 失效
标题翻译：芳基腙和芳基肼的制备方法
公开(公告)号：US07138548B2
公开(公告)日：2006-11-21
申请号：US10493503
申请日：2002-10-02
申请人： Andrew John Blacker , David Dodman , David Anthony Jackson , Jan Michael Fielden , John Heathcote Atherton
发明人： Andrew John Blacker , David Dodman , David Anthony Jackson , Jan Michael Fielden , John Heathcote Atherton
IPC分类号： C07C249/16 , C07C241/02
CPC分类号： C07C249/16 , C07C251/86
摘要： A process for the preparation of a compound of formula (I): wherein Ar represents an optionally substituted aromatic carbocycle or heterocycle, and R1 and R2 independently represent hydrogen, C1-10 alkyl, C(O)C1-10 alkyl or optionally substituted aryl provided that R1 and R2 are not both hydrogen which process comprises reacting together a compound of formula (II): Ar—X (II) wherein Ar is as defined in relation to formula (I) and X represents a leaving group with a a compound of formula (III) wherein R1 and R2 are as defined in relation to formula (I) under aqueous conditions in the presence of a Pd (II) salt, a ligand and a Group I or Group II metal hydroxide base at a pH greater than 7. Compounds of formula (I) may be hydrolysed to the corresponding hydrazine.
摘要翻译：制备式（I）化合物的方法：其中Ar表示任选取代的芳族碳环或杂环，R 1和R 2独立地表示氢，C C（O）C 1-10烷基或任选取代的芳基，条件是R 1和R 2可以相同或不同，（II）的化合物反应：式中，式（II）所示的化合物与式（II）化合物反应：＆lt;线内公式描述=“In-Line Formula”end =“lead”→Ar-X 其中Ar如关于式（I）所定义，X表示具有式（III）化合物的离去基团，其中R

3. 发明授权

US07019158B1 Chiral organometallic compounds for use in asymmetric synthesis 失效
标题翻译：用于不对称合成的手性有机金属化合物
公开(公告)号：US07019158B1
公开(公告)日：2006-03-28
申请号：US10485315
申请日：2002-08-02
申请人： Richard John Whitby
发明人： Richard John Whitby
IPC分类号： C07F17/00 , B01J31/00
CPC分类号： B01J31/20 , B01J31/1805 , B01J31/1845 , B01J31/2295 , B01J31/24 , B01J31/2404 , B01J2231/32 , B01J2231/34 , B01J2531/60 , B01J2531/72 , B01J2531/821 , B01J2531/822 , B01J2531/824 , B01J2531/827 , B01J2531/828 , B01J2531/84 , C07F17/00 , C07F17/02
摘要： Chiral organometallic compounds are provided which comprise certain non-symmetrically substituted cyclopentadiene complexed to a transition metal. The cyclopentadiene has a second coordinating group which also complexes the transition metal and is attached to the cyclopentadiene by means of a chiral connecting chain. Preferred transition metals include rhodium, ruthenium, iridium, cobalt, iron, manganese, chromium, tungsten, molybdenum, nickel, palladium, or platinum. These chiral organometallic compounds find use in asymmetric synthesis to produce chiral compounds.
摘要翻译：提供手性有机金属化合物，其包含与过渡金属络合的某些非对称取代的环戊二烯。环戊二烯具有第二配位基团，其也与过渡金属络合并通过手性连接链连接到环戊二烯上。优选的过渡金属包括铑，钌，铱，钴，铁，锰，铬，钨，钼，镍，钯或铂。这些手性有机金属化合物用于不对称合成以产生手性化合物。

4. 发明授权

US07019127B2 Solution phase synthesis of oligonucleotides 有权
公开(公告)号：US07019127B2
公开(公告)日：2006-03-28
申请号：US10294794
申请日：2002-11-15
申请人： Colin Bernard Reese , Quanlai Song
发明人： Colin Bernard Reese , Quanlai Song
IPC分类号： C07H21/00 , C07H21/02 , C07H21/04
CPC分类号： C07D265/33 , C07D207/48 , C07F9/165 , C07F9/18 , C07H19/10 , C07H19/20 , C07H21/00 , C07H21/04 , Y02P20/55
摘要： A process for the synthesis in solution phase of a phosphorothioate triester is provided. The process comprises the solution phase coupling of an H-phosphonate with an alcohol in the presence of a coupling agent to form an H-phosphonate diester. The H-phosphonate diester is oxidised in situ with a sulfur transfer agent to produce the phosphorothioate triester. Preferably, the H-phosphonate and alcohol are protected nucleosides or oligonucleotides. Oligonucleotide H-phosphonates which can be used in the formation of phosphorothioate triesters are also provided.

5. 发明授权

US06979364B2 Metal chelate compounds and inks 失效
标题翻译：金属螯合物和油墨
公开(公告)号：US06979364B2
公开(公告)日：2005-12-27
申请号：US10441286
申请日：2003-05-20
申请人： Gavin Wright , Kevin Johnson , Mairi Elizabeth Raggatt , Prakash Patel
发明人： Gavin Wright , Kevin Johnson , Mairi Elizabeth Raggatt , Prakash Patel
IPC分类号： C09D11/00 , B41J2/01 , C09B33/00 , C09B45/00
CPC分类号： C09D11/32 , C09D11/328
摘要： A metal chelate compound of the Formula (1) and salts thereof: wherein: one of A and B is OH and the other is an azotriazole group; and M is a metal or boron; and n is 0 to 4; compositions and inks containing a compound of Formula (1), a process for ink jet printing using the inks and an ink jet printer cartridge containing the ink.
摘要翻译：式（1）的金属螯合物及其盐：其中：A和B中的一个为OH，另一个为氮杂三唑基; M是金属或硼; n为0〜4; 含有式（1）化合物的组合物和油墨，使用该油墨的喷墨印刷方法和含有该油墨的喷墨打印机墨盒。

6. 发明申请

US20050274280A1 Metal chelate compounds and inks 审中-公开
标题翻译：金属螯合物和油墨
公开(公告)号：US20050274280A1
公开(公告)日：2005-12-15
申请号：US11197579
申请日：2005-08-05
申请人： Gavin Wright , Kevin Johnson , Mairi Raggatt , Prakash Patel
发明人： Gavin Wright , Kevin Johnson , Mairi Raggatt , Prakash Patel
IPC分类号： C09D11/00
CPC分类号： C09D11/32 , C09D11/328
摘要： A metal chelate compound of the Formula (1) and salts thereof: wherein: one of A and B is OH and the other is an azotriazole group; and M is a metal or boron; and n is 0 to 4; compositions and inks containing a compound of Formula (1), a process for ink jet printing using the inks and to an ink jet printer cartridge containing the ink.
摘要翻译：式（1）的金属螯合物及其盐：其中：A和B中的一个为OH，另一个为氮杂三唑基; M是金属或硼; n为0〜4; 含有式（1）化合物的组合物和油墨，使用该油墨的喷墨印刷方法和含有该油墨的喷墨打印机墨盒。

7. 发明申请

US20040027399A1 Processes, compositions and compounds 失效
标题翻译：方法，组合物和化合物
公开(公告)号：US20040027399A1
公开(公告)日：2004-02-12
申请号：US10441278
申请日：2003-05-20
申请人： Avecia Limited
发明人： Gavin Wright , Kevin Johnson , Mairi Elizabeth Raggatt , Prakash Patel
IPC分类号： B41J002/01 , B41J002/015 , B32B003/10 , C09D011/00 , C09B027/00 , C09B031/00 , C09B033/00 , C09B035/00 , C09B037/00 , C09B039/00 , C09B041/00 , C07C245/00 , C07C321/00 , C07C323/00 , C07C381/00 , C09B056/00
CPC分类号： C09D11/328 , Y10T428/24802
摘要： A process for printing an image on a substrate comprising applying thereto by means of an ink jet printer an ink containing a metal chelate compound of the Formula (1) and salts thereof: 1 wherein: one of A and B is OH and the other is an azotriazole group; each W independently is a carboxy or carbonamido group; each X independently is a substituent other than H, sulphonamido, carboxy, sulpho and carbonamido; J is a sulphonamido group; M is a metal or boron; a, p, q and n are each independently 0, 1, 2, 3 or 4; and (pnullqnullanulln) is 0, 1, 2, 3 or 4. Also claimed are compounds of Formula (1), compositions and inks containing a compound of Formula (1) and an ink jet printer cartridge containing the ink.
摘要翻译：一种用于在基材上印刷图像的方法，包括通过喷墨印刷机向其施加含有式（1）的金属螯合物及其盐的油墨：其中：A和B之一为OH，另一个为氮杂三唑基每个W独立地是羧基或碳酰氨基; 每个X独立地是除H，磺酰氨基，羧基，磺基和碳酰氨基以外的取代基; J是磺酰胺基; M是金属或硼; a，p，q和n各自独立地为0,1,2,3或4; 并且还要求保护的是式（1）的化合物，含有式（1）化合物的组合物和油墨，以及含有（P + 墨水。

8. 发明申请

US20040020405A1 Metal chelate compounds and inks 失效
标题翻译：金属螯合物和油墨
公开(公告)号：US20040020405A1
公开(公告)日：2004-02-05
申请号：US10441286
申请日：2003-05-20
申请人： Avecia Limited
发明人： Gavin Wright , Kevin Johnson , Mairi Elizabeth Raggatt , Prakash Patel
IPC分类号： C09D011/00 , B41J002/01 , C09B045/00 , C09B033/00
CPC分类号： C09D11/32 , C09D11/328
摘要： A metal chelate compound of the Formula (1) and salts thereof: 1 wherein: one of A and B is OH and the other is an azotriazole group; and M is a metal or boron; and n is 0 to 4. Also claimed are compositions and inks containing a compound of Formula (1), a process for ink jet printing using the inks and to an ink jet printer cartridge containing the ink.
摘要翻译：式（1）的金属螯合物及其盐：其中：A和B中的一个为OH，另一个为氮杂三唑基; M是金属或硼; 并且n为0至4.还要求保护含有式（1）化合物，使用该油墨的喷墨印刷方法和含有该油墨的喷墨打印机墨盒的组合物和油墨。

9. 发明申请

US20010011396A1 Phthalocyanine ink-jet dyes 失效
标题翻译：酞菁喷墨染料
公开(公告)号：US20010011396A1
公开(公告)日：2001-08-09
申请号：US09793497
申请日：2001-02-27
申请人： Avecia Limited
发明人： Kathryn Carr
IPC分类号： D06P005/00
CPC分类号： C09D11/328 , Y10S8/919
摘要： Phthalocyanine compounds of Formula (1) have utility as colorants in inks for ink jet printing, where Formula (1) represents: 1 and all IJP-effective forms of such compounds; and in which M represents a metal or H; Pc represents a phthalocyanine nucleus of Formula (2) 2 xnullynullz represents an average from 3 to 4; and z may be zero. A represents C1-4-alkylene; R1, R3 each independently represent H or C1-4-alkyl; R4 represents H; or C1-4-alkyl optionally substituted with hydroxy; R5 represents a carboxylic acid substituted aryl group; and R2 represents H, C1-4-alkyl or a group of formula BD where: B represents C1-4-alkylene; and D represents NR6R7;or SC1-4alkyleneSO3H; where: R6 represents H; or C1-4alkyl, optionally subsititued by hydroxy; R7 represents H; C1-4alkyl, optionally subsititued by hydroxy or morphlino; or R6 and R7 together with the N atom to which they are attached form a morpholino or piperazino ring.
摘要翻译：式（1）的酞菁化合物可用作喷墨印刷用油墨中的着色剂，其中式（1）表示：和所有这些化合物的所有IJP有效形式; 并且其中M表示金属或H; Pc表示式（2）的酞菁核，x + y + z表示3〜4的平均值。 z可以为零。 A表示C 1-4 - 亚烷基; R 1，R 3各自独立地表示H或C 1-4 - 烷基; R4表示H; 或任选被羟基取代的C 1-4 - 烷基; R5表示羧酸取代的芳基; 并且R 2表示H，C 1-4 - 烷基或式BD基团，其中：B表示C 1-4 - 亚烷基; 和D表示NR6R7;或SC1-4亚烷基-SO3H; 其中：R6表示H; 或任选被羟基取代的C 1-4烷基; R7表示H; 任选地被羟基或吗啉代取代的C 1-4烷基; 或R6和R7与它们所连接的N原子一起形成吗啉代或哌嗪子环。

10. 发明授权

US07227017B2 Process for the preparation of phosphorothioate oligonucleotides 有权
标题翻译：硫代磷酸酯寡核苷酸的制备方法
公开(公告)号：US07227017B2
公开(公告)日：2007-06-05
申请号：US10454841
申请日：2003-06-05
申请人： Ben James Mellor , Donald Alfred Wellings , Mark Edward Douglas
发明人： Ben James Mellor , Donald Alfred Wellings , Mark Edward Douglas
IPC分类号： C07H21/00
CPC分类号： C07H21/00
摘要： A process for the synthesis of phosphorothioate oligonucleotides is provided which comprises assembling an oligonucleotide bound to a solid support in the presence of acetonitrile; prior to cleaving the oligonucleotide from the solid support removing the acetonitrile; and cleaving the oligonucleotide from the solid support. The process is particularly suited to the large scale synthesis of nucleotides. The acetonitrile may be removed from the solid support by one or both of drying and by washing with solvents. Preferred washing solvents comprise trialkylamines.
摘要翻译：提供了一种合成硫代磷酸酯寡核苷酸的方法，其包括在乙腈存在下组装与固体支持物结合的寡核苷酸; 之前从固相支持物上切下寡核苷酸，除去乙腈; 并从固体支持物上切割寡核苷酸。该方法特别适用于大规模合成核苷酸。可以通过干燥和用溶剂洗涤一次或两次从固体支持物除去乙腈。优选的洗涤溶剂包括三烷基胺。

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