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1. 发明申请

US20120211706A1 POLYDENTATE LIGAND METAL COMPLEX 审中-公开
标题翻译：聚氨酯金属复合物
公开(公告)号：US20120211706A1
公开(公告)日：2012-08-23
申请号：US13504275
申请日：2010-10-25
申请人： Yusuke Kuramochi , Takeshi Ishiyama , Hideyuki Higashimura
发明人： Yusuke Kuramochi , Takeshi Ishiyama , Hideyuki Higashimura
IPC分类号： C07F5/00 , H01B1/12
CPC分类号： C07D233/64 , C07D235/14 , C07D417/12 , C07F5/003 , C07F5/022 , C07F9/65583 , C09K11/06 , C09K2211/1011 , C09K2211/1014 , C09K2211/1044
摘要： The present invention provides a metal complex that has excellent durability, and a device and the like having excellent durability that uses such a metal complex. Specifically, the present invention provides a metal complex comprising (a) a polydentate ligand having denticity of five or more that includes a heteroaromatic ring which contains two or more atoms selected from the group consisting of a nitrogen atom, an oxygen atom, and a sulfur atom, and (b) an ion of a metal selected from the group consisting of cerium, praseodymium, ytterbium, and lutetium; a composition comprising the metal complex and a charge transport material; an organic thin film obtained by using the metal complex or composition; and a device obtained by using the metal complex, composition, or organic thin film.
摘要翻译：本发明提供了耐久性优异的金属络合物和使用这种金属络合物的耐久性优良的装置等。具体地说，本发明提供一种金属配合物，其特征在于，具有（a）具有5以上的牙齿的多齿配体，所述多齿配体包括含有选自氮原子，氧原子和硫原子中的2个以上的原子的杂芳香环原子，和（b）选自铈，镨，镱和镥的金属离子; 包含金属络合物和电荷输送材料的组合物; 通过使用金属络合物或组合物获得的有机薄膜; 以及通过使用金属络合物，组合物或有机薄膜获得的器件。

2. 发明申请

US20120049167A1 ORGANIC ELECTROLUMINESCENT DEVICE 审中-公开
标题翻译：有机电致发光器件
公开(公告)号：US20120049167A1
公开(公告)日：2012-03-01
申请号：US13145718
申请日：2010-01-21
申请人： Yusuke Kuramochi , Norifumi Kobayashi , Hideyuki Higashimura
发明人： Yusuke Kuramochi , Norifumi Kobayashi , Hideyuki Higashimura
IPC分类号： H01L51/54 , C08F26/06
CPC分类号： C07D213/18 , C07D233/58 , C08G61/02 , C08G61/10 , C08G61/12 , C08G2261/312 , C08G2261/3142 , C08G2261/3162 , C08G2261/5242 , C09K11/06 , C09K2211/1029 , C09K2211/1044 , C09K2211/1466 , C09K2211/188 , H01L51/0035 , H01L51/0037 , H01L51/004 , H01L51/0091 , H01L51/5012 , H05B33/14
摘要： An organic electroluminescent device in which an organic layer containing a metal coordination compound represented by the following formula (1) is sandwiched between the pair of electrodes composed of an anode and a cathode, MLaXb (1) wherein M is an ion of a metal of Group 11 of the Periodic Table, L is a ligand represented by the formula (2) shown below, X is an anion, and a and b are defined in the specification, wherein A is a divalent group formed by removing two hydrogen atoms from the formula (3) or (4) shown below, and D1, k1, m1, A, D1, Q1, and Q2 are defined in the specification, wherein X1, X2, X3, X4, X5, R1, R5, R6, and R9 are defined in the specification.
摘要翻译：一种有机电致发光器件，其中含有由下式（1）表示的金属配位化合物的有机层夹在由阳极和阴极组成的一对电极之间，MLaXb（1）其中M是金属的离子 L是由下述式（2）表示的配体，X是阴离子，a和b在本说明书中定义，其中A是通过除去二个氢原子而形成的二价基团在本说明书中定义了D1，k1，m1，A，D1，Q1和Q2，其中X1，X2，X3，X4，X5，R1，R5，R6和 R9在本说明书中定义。

3. 发明申请

US20130001472A1 THIN FILM AND COMPOUND USED IN THE SAME 审中-公开
标题翻译：薄膜及其使用的化合物
公开(公告)号：US20130001472A1
公开(公告)日：2013-01-03
申请号：US13583177
申请日：2011-03-04
申请人： Joji Ohshita , Toshihiro Murafuji , Yusuke Kuramochi , Takashi Kaikoh , Hideyuki Higashimura
发明人： Joji Ohshita , Toshihiro Murafuji , Yusuke Kuramochi , Takashi Kaikoh , Hideyuki Higashimura
IPC分类号： C07F9/94 , C09K11/06 , B82Y30/00
CPC分类号： C07F9/94 , C09K2211/1029 , C09K2211/1044 , C09K2211/1088 , C09K2211/1092 , C09K2211/188 , H01L51/0077 , H01L51/5016 , H05B33/145
摘要： To provide a novel material exhibiting excellent light-emitting characteristics using a heavy metal element having relatively abundant reserve.A thin film containing a compound of Formula (1): wherein Ar1 and Ar2 are each independently a C3-30 aromatic ring; R1 and R2 are a substituent; a and b are each independently an integer of 0 to 12, wherein when a is 2 or more, each R1 is optionally different from each other and two R1 are optionally bonded with each other to form a ring structure, and when b is 2 or more, each R2 is optionally different from each other and two R2 are optionally bonded with each other to form a ring structure; A1 is any of direct bond, —O—, —S—, —S(═O)—, —S(═O)2—, —PR3—, —NR4—, and —C(—R5)2—; R3 is a hydrogen atom or a substituent; R4 is a hydrogen atom or a substituent; R5 is a hydrogen atom or a substituent and two R5 are optionally different from each other; E1 is a monovalent group having 50 or less carbon atoms; L1 is a ligand having 50 or less carbon atoms; c is an integer of 0 to 3, wherein when c is 2 or more, each L1 is optionally different from each other; and each combination of a combination of E1 and Ar1 and a combination of E1 and Ar2 optionally forms a bond; and when c is 1 to 3, each combination of a combination of L1 and E1, a combination of L1 and Ar1, a combination of L1 and Ar2, and a combination of L1 and L1 optionally forms a bond.
摘要翻译：使用具有相对丰富的储备的重金属元素提供显示出优异的发光特性的新型材料。含有式（1）化合物的薄膜：其中Ar1和Ar2各自独立地为C3-30芳环; R1和R2是取代基; a和b各自独立地为0〜12的整数，其中当a为2以上时，每个R 1可以彼此不同，并且两个R 1彼此任意地键合形成环结构，当b为2或更优选地，每个R 2彼此可选地彼此不同，并且两个R 2彼此可选地键合以形成环结构; A1是直接键合，-O - ， - S - ， - S（= O） - ， - S（= O）2 - ， - PR 3 - ， - NR 4 - 和-C（ - R 5） R3是氢原子或取代基; R4是氢原子或取代基; R5是氢原子或取代基，两个R5任选地彼此不同; E1是具有50个或更少碳原子的一价基团; L1是具有50个或更少碳原子的配体; c为0〜3的整数，其中，当c为2以上时，各L1彼此不同; 并且E1和Ar1的组合以及E1和Ar2的组合的每个组合可以任选地形成键; 当c为1〜3时，L1和E1的组合，L1和Ar1的组合，L1和Ar2的组合以及L1和L1的组合的组合可以任意地形成键。

4. 发明申请

US20120041203A1 METAL COMPLEX HAVING AROMATIC RING LIGAND CONTAINING NITROGEN ATOM 审中-公开
标题翻译：金属复合物具有包含氮原子的芳族环状配体
公开(公告)号：US20120041203A1
公开(公告)日：2012-02-16
申请号：US13265749
申请日：2010-04-19
申请人： Yusuke Kuramochi , Norifumi Kobayashi , Hideyuki Higashimura
发明人： Yusuke Kuramochi , Norifumi Kobayashi , Hideyuki Higashimura
IPC分类号： C07F1/10 , C07F1/08
CPC分类号： C07D213/16 , C07D471/04 , C07D471/10 , C07F1/005 , C07F9/5022 , C07F9/5325 , C07F9/5765 , C07F9/58 , C07F9/60 , C07F9/62 , C07F9/65068 , C07F9/65335 , C07F9/65515 , C07F9/65517 , C07F9/65522 , C07F9/65683 , C07F9/6596 , C09K11/06 , C09K2211/1007 , C09K2211/1011 , C09K2211/1029 , C09K2211/188 , H01L51/0091 , H01L51/0095 , H01L51/5016 , H05B33/14
摘要： A metal complex containing a nitrogen-containing aromatic ring ligand which has a dendritic molecular chain, and a copper(I) ion or a silver(I) ion. For example, the metal complex which is represented by compositional formula (8): (wherein M+ is a copper(I) ion or a silver(I) ion, L is a ligand, and X is a counter ion; p is a positive number, and q and r are each independently numerical numbers of 0 or more; R represents a hydrogen atom, a halogen atom, a cyano group, a nitro group, a carboxyl group, an amino group, an acylamino group, a silyl group, a hydroxyl group, an acyl group, a hydrocarbyl group, a hydrocarbyloxy group, a hydrocarbylthio group, or a heterocyclic group, wherein the amino group, the silyl group, the hydrocarbyl group, the hydrocarbyloxy group and the hydrocarbylthio group optionally have a substituent) has excellent heat resistance.
摘要翻译：含有具有树枝状分子链的含氮芳族环配体和铜（I）离子或银（I）离子的金属络合物。例如，由组成式（8）表示的金属络合物：（其中M +为铜（I）离子或银（I）离子，L为配体，X为抗衡离子; p为正数，q和r各自独立地为0以上的数; R表示氢原子，卤素原子，氰基，硝基，羧基，氨基，酰氨基，甲硅烷基，羟基，酰基，烃基，烃氧基，烃硫基或杂环基，其中氨基，甲硅烷基，烃基，烃氧基和烃硫基任选具有取代基）具有优异的耐热性。

5. 发明申请

US20090062110A1 METAL COMPLEX AND USE THEREOF 审中-公开
标题翻译：金属复合物及其用途
公开(公告)号：US20090062110A1
公开(公告)日：2009-03-05
申请号：US12278180
申请日：2007-01-01
申请人： Nobuyoshi Koshino , Takeshi Ishiyama , Tadafumi Matsunaga , Hideyuki Higashimura
发明人： Nobuyoshi Koshino , Takeshi Ishiyama , Tadafumi Matsunaga , Hideyuki Higashimura
IPC分类号： C07F15/00 , B01J31/06 , B01J31/12
CPC分类号： B01J31/2243 , B01J31/1815 , B01J31/223 , B01J35/002 , B01J37/082 , B01J2531/0205 , B01J2531/0241 , B01J2531/025 , B01J2531/16 , B01J2531/56 , B01J2531/72 , B01J2531/842 , B01J2531/845 , B01J2531/847 , C07D257/10
摘要： A polynuclear metal complex having in each molecule not only at least one large cyclic ligand having 5 to 15 coordinating atoms but also multiple metal atoms is subjected to any of heating treatment, radiation exposure treatment and electric discharge treatment, thereby providing a polynuclear metal complex exhibiting a ratio of weight loss by the treatment of 5 to 90 wt. % and a carbon content after the treatment of 5 wt. % or more.
摘要翻译：在每个分子中不仅具有至少一个具有5至15个配位原子的大环配体，而且具有多个金属原子的多核金属络合物经受加热处理，辐射暴露处理和放电处理中的任一种，从而提供多核金属络合物，通过处理5至90wt。的重量损失比率。％，处理后的碳含量为5wt。％或者更多。

6. 发明申请

US20090011929A1 MULTINUCLEAR COMPLEX AND POLYMER THEREOF 审中-公开
标题翻译：多核苷酸复合物及其聚合物
公开(公告)号：US20090011929A1
公开(公告)日：2009-01-08
申请号：US12278188
申请日：2007-02-07
申请人： Takeshi Ishiyama , Hideyuki Higashimura
发明人： Takeshi Ishiyama , Hideyuki Higashimura
IPC分类号： B01J31/18 , C08F214/18 , C07F13/00 , C07D403/14
CPC分类号： C07D235/14 , B01J31/183 , B01J31/2243 , B01J2231/62 , B01J2531/0216 , B01J2531/0258 , B01J2531/16 , B01J2531/72 , B01J2531/842 , B01J2531/845 , B01J2531/847 , C07D403/14 , C07D405/14 , C07F1/005 , C07F9/65583 , C07F13/005 , C07F15/025 , C07F15/045 , C07F15/065 , C08F4/26 , C08F4/40
摘要： To provide a multinuclear complex including at least one ligand L satisfying the following requirements (i) r (ii) and (iii), and a plurality of metal atoms in a molecule: (i) having a group having polymerizable reactive multiple bonds, and/or a ring-opening polymerizable ring, (ii) having five or more coordination atoms bonding to the metal atoms, and (iii) being soluble in a solvent.
摘要翻译：提供包含满足以下要求（i）r（ii）和（iii））的至少一种配体L和分子中多个金属原子的多核络合物：（i）具有可聚合反应性多重键的基团，以及 /或可开环聚合的环，（ii）具有五个或更多个配位原子键合到金属原子上，和（iii）可溶于溶剂。

7. 发明授权

US07988944B2 Peroxide decomposition catalyst 有权
标题翻译：过氧化物分解催化剂
公开(公告)号：US07988944B2
公开(公告)日：2011-08-02
申请号：US11993892
申请日：2006-06-20
申请人： Takeshi Ishiyama , Hideyuki Higashimura , Hiroshi Takigawa
发明人： Takeshi Ishiyama , Hideyuki Higashimura , Hiroshi Takigawa
IPC分类号： C01B13/00 , G01N33/44 , C07F3/12
CPC分类号： B01J31/2243 , B01J23/30 , B01J23/34 , B01J31/1815 , B01J31/183 , B01J31/2239 , B01J2531/0216 , B01J2531/025 , B01J2531/0258 , B01J2531/16 , B01J2531/72 , B01J2531/842 , B01J2531/845
摘要： An object of the present invention is to provide a catalyst which decomposes a peroxide effectively and economically under a high temperature while suppressing generation of free radicals, and the present invention provides a peroxide decomposition catalyst containing a base metal atom, wherein a value A indicating a free radical generation amount represented by the (equation 1) is not more than 0.20, and a value B indicating a reaction rate represented by the (equation 2), which can be easily applied to utility such as an agent for preventing deterioration of a polymer electrolyte-type fuel cell and a water electrolysis apparatus, and an antioxidant for medicaments, agrochemicals and foods. A=(Mw(S)/Mw)−1 (equation 1) (wherein Mw is a weight average molecular weight of poly(sodium 4-styrenesulfonate) after a hydrogen peroxide decomposition test in the test at 80° C. in the presence of poly(sodium 4-styrenesulfonate), and Mw(S) is a weight average molecular weight of poly(sodium 4-styrenesulfonate) before the test) B=N(PO)/N(cat) (equation 2) (wherein N(po) is a mole number of hydrogen peroxide decomposed per 20 minutes in a hydrogen peroxide decomposition test in the (equation 1), and N(cat) is a mole number per metal atom of a catalyst used).
摘要翻译：本发明的目的在于提供一种在高温下有效且经济地分解过氧化物同时抑制自由基产生的催化剂，本发明提供了含有贱金属原子的过氧化物分解催化剂，其中A表示由（式1）表示的自由基产生量不大于0.20，表示由（式2）表示的反应速度的值B，其可以容易地应用于防止聚合物劣化的试剂电解质型燃料电池和水电解装置，以及用于药物，农药和食品的抗氧化剂。 A =（Mw（S）/ Mw）-1（式1）（式中，Mw是在80℃下在过氧化氢分解试验中聚（4-苯乙烯磺酸钠）的重均分子量，的聚（4-苯乙烯磺酸钠），Mw（S）是试验前的聚（4-苯乙烯磺酸钠）的重均分子量）B = N（PO）/ N（cat）（式2）（式中，N （po）是在（式1）的过氧化氢分解试验中每20分钟分解的过氧化氢的摩尔数，N（cat）是使用的催化剂的每个金属原子的摩尔数）。

8. 发明申请

US20100197886A1 MODIFIED POLYMER COMPLEX, COMPLEX MONOMER, POLYMER COMPLEX, AND REDOX,CATALYST 审中-公开
标题翻译：改性聚合物复合物，复合单体，聚合物复合物和还原剂，催化剂
公开(公告)号：US20100197886A1
公开(公告)日：2010-08-05
申请号：US12671066
申请日：2008-08-05
申请人： Takeshi Ishiyama , Hideyuki Higashimura , Sho Kanesaka
发明人： Takeshi Ishiyama , Hideyuki Higashimura , Sho Kanesaka
IPC分类号： C08G79/00 , C07D233/61
CPC分类号： C07D233/54 , B01J31/1805 , B01J31/183 , B01J31/2208 , B01J2531/0238 , B01J2531/16 , B01J2531/842 , B01J2531/845 , B01J2531/847 , C07D235/04 , C07D235/14 , C07F1/08 , C07F13/005 , C07F15/025 , C07F15/045 , C07F15/065 , C08F12/26 , C08F12/32 , C08F12/34 , C08F212/32 , C08F220/06 , C08F220/44 , C08F212/34 , C08F212/14
摘要： A modified polymer complex, which is obtained by intermolecular and/or intramolecular crosslinking of a polymer complex via side chains thereof, wherein the polymer complex is a copolymer of a complex monomer meeting the following conditions (i) to (iii) and a comonomer expressed by the following general formula (1): R02R03═R01E (The definitions of R01, R02, R03 and E are omitted.)(i) the complex monomer has two or more transition metal atoms;(ii) the complex monomer has a polydentate ligand containing three or more coordinating atoms that are coordinately bonded to the transition metal atoms; and(iii) the polydentate ligand has one or more polymerizable functional groups.
摘要翻译：通过其侧链通过聚合物配合物的分子间和/或分子内交联获得的改性聚合物络合物，其中所述聚合物配合物是满足以下条件（i）至（iii）的共轭单体和表达的共聚单体的共聚物通过以下通式（1）表示：R02R03 = R01E（R01，R02，R03和E的定义被省略。）（i）复合单体具有两个以上的过渡金属原子; （ii）复合单体具有多齿配体，其含有三个或更多个与过渡金属原子配位键合的配位原子; 和（iii）多齿配体具有一个或多个可聚合官能团。

9. 发明申请

US20090036687A1 MULTINUCLEAR COMPLEX AND CONDENSATION PRODUCT THEREOF 审中-公开
标题翻译：多功能复合物和凝结产品
公开(公告)号：US20090036687A1
公开(公告)日：2009-02-05
申请号：US12278415
申请日：2007-02-08
申请人： Yoshiyuki Sugahara , Takeshi Ishiyama , Hideyuki Higashimura
发明人： Yoshiyuki Sugahara , Takeshi Ishiyama , Hideyuki Higashimura
IPC分类号： C07D403/14 , C07F7/10
CPC分类号： C07F15/025 , B01J31/183 , B01J31/2243 , B01J2231/62 , B01J2531/0216 , B01J2531/0258 , B01J2531/16 , B01J2531/72 , B01J2531/842 , B01J2531/845 , B01J2531/847 , C07F7/1804
摘要： A multinuclear complex comprising a plurality of metal atoms and a ligand L coordinating to the metal atoms, and satisfying the following conditions (i), (ii), (iii) and (iv):(i) The ligand L has a monovalent group represented by the following general formula (1) and/or a divalent group represented by the following general formula (2), (ii) The ligand L has at least 5 coordination atoms bonding to the metal atom, (iii) At least one of the coordination atoms bonds to two of the metal atoms, or the minimum number of covalent bonds between any two selected coordination atoms is 1-5, and (iv) The ligand L is soluble in the solvent.
摘要翻译：包含多个金属原子的多核络合物和与金属原子配位的配位体L，并满足下列条件（i），（ii），（iii）和（iv）：（i）配体L具有一价基团由下述通式（1）表示的化合物和/或由以下通式（2）表示的二价基团，（ii）配体L具有至少5个与金属原子键合的配位原子，（iii）至少一个配位原子与两个金属原子键合，或任意两个选定的配位原子之间的最小共价键数为1-5，和（ⅳ）配体L可溶于溶剂中。

10. 发明申请

US20080219916A1 Peroxide Decomposition Catalyst 有权
标题翻译：过氧化物分解催化剂
公开(公告)号：US20080219916A1
公开(公告)日：2008-09-11
申请号：US11993892
申请日：2006-06-20
申请人： Takeshi Ishiyama , Hideyuki Higashimura , Hiroshi Takigawa
发明人： Takeshi Ishiyama , Hideyuki Higashimura , Hiroshi Takigawa
IPC分类号： C01B13/00 , C07F13/00 , G01N33/44
CPC分类号： B01J31/2243 , B01J23/30 , B01J23/34 , B01J31/1815 , B01J31/183 , B01J31/2239 , B01J2531/0216 , B01J2531/025 , B01J2531/0258 , B01J2531/16 , B01J2531/72 , B01J2531/842 , B01J2531/845
摘要： An object of the present invention is to provide a catalyst which decomposes a peroxide effectively and economically under a high temperature while suppressing generation of free radicals, and the present invention provides a peroxide decomposition catalyst containing a base metal atom, wherein a value A indicating a free radical generation amount represented by the (equation 1) is not more than 0.20, and a value B indicating a reaction rate represented by the (equation 2), which can be easily applied to utility such as an agent for preventing deterioration of a polymer electrolyte-type fuel cell and a water electrolysis apparatus, and an antioxidant for medicaments, agrochemicals and foods. A=(Mw(S)/Mw)−1 (equation 1) (wherein Mw is a weight average molecular weight of poly(sodium 4-styrenesulfonate) after a hydrogen peroxide decomposition test in the test at 80° C. in the presence of poly(sodium 4-styrenesulfonate), and Mw(S) is a weight average molecular weight of poly(sodium 4-styrenesulfonate) before the test) B=N(PO)/N(cat) (equation 2) (wherein N(po) is a mole number of hydrogen peroxide decomposed per 20 minutes in a hydrogen peroxide decomposition test in the (equation 1), and N(cat) is a mole number per metal atom of a catalyst used)
摘要翻译：本发明的目的在于提供一种在高温下有效且经济地分解过氧化物同时抑制自由基产生的催化剂，本发明提供了含有贱金属原子的过氧化物分解催化剂，其中A表示由（式1）表示的自由基产生量不大于0.20，表示由（式2）表示的反应速度的值B，其可以容易地应用于防止聚合物劣化的试剂电解质型燃料电池和水电解装置，以及用于药物，农药和食品的抗氧化剂。 A =（Mw（S）/ Mw）-1（等式1）<？in-line-formula description =“In-line-formula description =”In-line-formula description = （式中，Mw是在80℃下在聚（4-苯乙烯磺酸钠）存在下的过氧化氢分解试验后的聚（4-苯乙烯磺酸钠）的重均分子量，苯乙烯磺酸盐），Mw（S）是测试前的聚（4-苯乙烯磺酸钠）的重均分子量）<？在线公式描述=“在线公式”end =“lead”→> B = N（PO）/ N（cat）（式2）<？in-line-formula description =“In-line Formulas”end =“tail”？>（其中N（po）是每分解的过氧化氢的摩尔数（式1）中的过氧化氢分解试验为20分钟，N（cat）为所用催化剂的每个金属原子的摩尔数）

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