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    • 3. 发明授权
    • High purity silica crucible by electrolytic refining, and its production method and pulling method
    • 高纯度二氧化硅坩埚通过电解精炼及其制备方法和拉拔方法
    • US07160387B2
    • 2007-01-09
    • US10781682
    • 2004-02-20
    • Hiroshi KishiMasanori FukuiYoshiyuki Tsuji
    • Hiroshi KishiMasanori FukuiYoshiyuki Tsuji
    • C30B13/06
    • C03C3/06C03B19/095C03B2201/03C30B15/10C30B29/06Y10S117/90Y10T117/1032Y10T117/1052
    • This invention provides a high purity silica crucible having low impurity concentration in its inner portion, and its production method. The crucible, in which at least each content of Na and Li being contained in the depth of 1 mm from the inside surface is less than 0.05 ppm, is given by a production method of a high purity silica glass crucible, wherein a purity of the melted silica powder layer is increased by applying a voltage between a mold and an arc electrode to move impurity metals being contained in the melted silica glass layer to the outside, when the silica crucible is produced by arc plasma heating a raw material powder of silica in an inside surface of a hollow rotary mold. The method comprises, keeping an arc electrode potential of within ±500 V during an arc melting, applying a voltage of from −1000 V to −20000 V to a mold being insulated to the ground, and applying a high voltage to the un-melted silica powder layer of the outside.
    • 本发明提供了内部杂质浓度低的高纯度二氧化硅坩埚及其制造方法。 通过高纯度二氧化硅玻璃坩埚的制造方法给出至少含有内表面1mm以内的Na和Li的含量小于0.05ppm的坩埚,其中,纯度为 通过在模具和电弧电极之间施加电压来增加熔融二氧化硅粉末层,以将熔融石英玻璃层中所含的杂质金属移动到外部,当通过电弧等离子体加热二氧化硅原料粉末 中空旋转模具的内表面。 该方法包括:在电弧熔化期间将电弧电极电位保持在±500V以内,向-1000V至-20000V施加电压至与地绝缘的模具,并将高电压施加到未熔化 二氧化硅粉末层外面。
    • 6. 发明授权
    • Packing-packaging apparatus
    • 包装包装设备
    • US08776481B2
    • 2014-07-15
    • US12920746
    • 2009-01-15
    • Fumio MiyaharaYoshiyuki TsujiTomohiro Takemoto
    • Fumio MiyaharaYoshiyuki TsujiTomohiro Takemoto
    • B65B1/06
    • B65B29/02B65B9/20B65B9/2056B65B29/04B65B37/12B65B39/001
    • A packing-packaging machine includes: sheet feeding means; a horizontal bonding unit for forming a bag body by forming horizontal bonding on a tubular body at predetermined intervals; and an object dispensing unit for dispensing an object to be packaged to the bag body during a repetition of the formation of the horizontal bonding. The object dispensing unit includes a shutter for opening and closing a falling path of a predetermined amount of the object into the bag body. The shutter is opened and closed such that the predetermined amount of the object and another predetermined amount of the object fall with a spacing therebetween, and that before the horizontal bonding is formed on the bag body packed with the predetermined amount of the object which has been dropped during opening-closing operation of the shutter, the other predetermined amount of the object for a next bag body starts falling.
    • 包装机包括:送纸装置; 水平接合单元,用于通过在管状体上以预定间隔形成水平结合来形成袋体; 以及物体分配单元,用于在重复形成水平粘合期间将待包装物体分配到袋体。 物体分配单元包括用于打开和关闭预定量的物体到袋体中的下落路径的挡板。 快门被打开和关闭,使得预定量的物体和另一个预定量的物体以其间隔开而下降,并且在水平接合之前形成在装有预定量的物体的袋体上 在快门的打开 - 关闭操作期间下降,另一个预定量的下一个袋体的物体开始下降。
    • 7. 发明申请
    • METHOD FOR PURIFICATION OF SILICA PARTICLES, PURIFIER, AND PURIFIED SILICA PARTICLES
    • 纯化二氧化硅颗粒,净化剂和纯化二氧化硅颗粒的方法
    • US20110165028A1
    • 2011-07-07
    • US13047433
    • 2011-03-14
    • Minoru KANDAYoshiyuki Tsuji
    • Minoru KANDAYoshiyuki Tsuji
    • B01J8/18B01J19/08
    • C01B33/18B01J8/1836B01J8/42B01J2208/00407B01J2208/00415B03C1/288B03C1/30B03C1/32B03C2201/16B03C2201/18C03C1/02
    • [Problems] To provide a treatment method having excellent purification effect, in which impurities having high ionicity in a silica powder can be removed in a short time, a apparatus thereof, and a purified silica powder.[Means for Solving the Problems] A purification method of a silica powder comprises: making a silica powder into a fluid state; contacting a purified gas to the silica powder in the fluid state at high temperature; and thereby removing impurity components of the silica powder. In the method, the silica powder in the fluid state is positioned in a magnetic field region. Further, the silica powder is contacted with the purified gas, while applying voltage to the silica powder by an electric field generated by moving of the silica powder. Preferably, the silica powder in a fluid state is positioned in the magnetic region of 10 gausses or more, and contacted with the purification gas at a temperature of 1000° C. or more.
    • [问题]提供一种具有优异的净化效果的处理方法,其中可以在短时间内除去二氧化硅粉末中的高离子性的杂质,其装置和纯化的二氧化硅粉末。 解决问题的方法二氧化硅粉末的净化方法包括:将二氧化硅粉末制成流体状态; 在高温下将纯化气体以流体状态与二氧化硅粉末接触; 从而除去二氧化硅粉末的杂质成分。 在该方法中,处于流体状态的二氧化硅粉末位于磁场区域中。 此外,二氧化硅粉末与纯化气体接触,同时通过二氧化硅粉末移动产生的电场向二氧化硅粉末施加电压。 优选地,处于流体状态的二氧化硅粉末位于10高斯或更高的磁性区域中,并且在1000℃以上的温度下与净化气体接触。
    • 8. 发明授权
    • Silica glass crucible
    • 二氧化硅玻璃坩埚
    • US07695787B2
    • 2010-04-13
    • US10801683
    • 2004-03-17
    • Yoshiyuki TsujiToshio Tsujimoto
    • Yoshiyuki TsujiToshio Tsujimoto
    • B44C1/22C04B35/00F16L9/10F27B14/10
    • C03C19/00B24C1/08C03C15/00C30B15/10Y10T117/1032Y10T117/108Y10T428/13Y10T428/131
    • To provide a silica glass crucible, wherein there are no problems of generating a sinking and buckling when said crucible is used for pulling up silicon single crystal at a high temperature. The silica glass crucible used for pulling up the silicon single crystal, wherein at least an outer surface of a wall part of the crucible is covered with fine grooves having a length of less than 200 μm, a width of less than 30 μm and a depth of from more than 3 μm to less than 30 μm. Preferably, said fine groves are formed by carrying out a sand-blast treatment and a hydrofluoric acid etching and exist on more than 10% of the outer surface of the crucible, and a sliding frictional coefficient of the outer surface of the crucible to a carbon at 1500 degree C. is more than 0.6.
    • 为了提供一种二氧化硅玻璃坩埚,其中当在高温下使用所述坩埚拉起硅单晶时,不存在产生下沉和翘曲的问题。 用于提升硅单晶的二氧化硅玻璃坩埚,其中至少坩埚的壁部的外表面被细长的小于200μm,宽度小于30μm的细槽和深度 大于3μm至小于30μm。 优选地,通过进行喷砂处理和氢氟酸蚀刻而形成所述细小花纹,并且存在于坩埚的外表面的10%以上,坩埚的外表面的滑动摩擦系数为碳 在1500摄氏度,大于0.6。
    • 9. 发明授权
    • Method for purification of silica particles, purifier, and purified silica particles
    • 纯化二氧化硅颗粒,净化剂和纯化二氧化硅颗粒的方法
    • US08506890B2
    • 2013-08-13
    • US13047433
    • 2011-03-14
    • Minoru KandaYoshiyuki Tsuji
    • Minoru KandaYoshiyuki Tsuji
    • B01J8/24B01J19/08
    • C01B33/18B01J8/1836B01J8/42B01J2208/00407B01J2208/00415B03C1/288B03C1/30B03C1/32B03C2201/16B03C2201/18C03C1/02
    • To provide a treatment method having excellent purification effect, in which impurities having high ionicity in a silica powder can be removed in a short time, an apparatus thereof, and a purified silica powder. A purification method of a silica powder comprises making a silica powder into a fluid state; contacting a purified gas to the silica powder in the fluid state at high temperature; and thereby removing impurity components of the silica powder. In the method, the silica powder in the fluid state is positioned in a magnetic field region. Further, the silica powder is contacted with the purified gas, while applying voltage to the silica powder by an electric field generated by moving of the silica powder. Preferably, the silica powder in a fluid state is positioned in the magnetic region of 10 gausses or more, and contacted with the purification gas at a temperature of I000° C. or more.
    • 为了提供具有优异的纯化效果的处理方法,其中可以在短时间内除去二氧化硅粉末中的高离子性的杂质,其装置和纯化的二氧化硅粉末。 二氧化硅粉末的纯化方法包括将二氧化硅粉末制成流体状态; 在高温下将纯化气体以流体状态与二氧化硅粉末接触; 从而除去二氧化硅粉末的杂质成分。 在该方法中,处于流体状态的二氧化硅粉末位于磁场区域中。 此外,二氧化硅粉末与纯化气体接触,同时通过二氧化硅粉末移动产生的电场向二氧化硅粉末施加电压。 优选地,处于流体状态的二氧化硅粉末位于10高斯或更高的磁性区域中,并且在1000℃以上的温度下与净化气体接触。