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1. 发明授权

US07683137B2 Color reduction polyethylene modified by radical initiation 有权
标题翻译：通过自由基引发改性的减色聚乙烯
公开(公告)号：US07683137B2
公开(公告)日：2010-03-23
申请号：US11174854
申请日：2005-07-05
申请人： Vincent Henri Barre , Tim J. Coffy , Cyril Chevillard
发明人： Vincent Henri Barre , Tim J. Coffy , Cyril Chevillard
IPC分类号： C08F8/06 , C08F210/02
CPC分类号： C08F6/02 , C08K3/22 , C08K5/05 , C08K5/098 , Y10T428/1334 , Y10T428/1352 , Y10T428/2967 , C08L23/04
摘要： Polyethylene modified by using radical initiators such as oxygen and peroxides sometimes has a yellow color which may be reduced or eliminated by incorporating additives such as polyethylene glycol, and/or neutralizing species such as alkali metal stearates, particularly calcium stearate, and zinc oxide.
摘要翻译：通过使用自由基引发剂如氧和过氧化物改性的聚乙烯有时具有黄色，其可以通过掺入添加剂如聚乙二醇和/或中和物质如碱金属硬脂酸盐，特别是硬脂酸钙和氧化锌而被还原或消除。

2. 发明申请

US20100081746A1 Color Reduction in Polyethylene Modified by Radical Initiation 有权
标题翻译：由自由基引发改性的聚乙烯中的降色
公开(公告)号：US20100081746A1
公开(公告)日：2010-04-01
申请号：US12568357
申请日：2009-09-28
申请人： Vincent Henri Barre , Tim J. Coffy , Cyril Chevillard
发明人： Vincent Henri Barre , Tim J. Coffy , Cyril Chevillard
IPC分类号： C08K5/098 , C08K5/05 , C08K3/22
CPC分类号： C08F6/02 , C08K3/22 , C08K5/05 , C08K5/098 , Y10T428/1334 , Y10T428/1352 , Y10T428/2967 , C08L23/04
摘要： Polyethylene modified by using radical initiators such as oxygen and peroxides sometimes has a yellow color which may be reduced or eliminated by incorporating additives such as polyethylene glycol, and/or neutralizing species such as alkali metal stearates, particularly calcium stearate, and zinc oxide.
摘要翻译：通过使用自由基引发剂如氧和过氧化物改性的聚乙烯有时具有黄色，其可以通过掺入添加剂如聚乙二醇和/或中和物质如碱金属硬脂酸盐，特别是硬脂酸钙和氧化锌而被还原或消除。

3. 发明授权

US08759446B2 Compatibilized polypropylene and polylactic acid blends and methods of making and using same 有权
标题翻译：增容的聚丙烯和聚乳酸混合物及其制备和使用方法
公开(公告)号：US08759446B2
公开(公告)日：2014-06-24
申请号：US12165051
申请日：2008-06-30
申请人： Fengkui Li , Tim J. Coffy , Michel Daumerie
发明人： Fengkui Li , Tim J. Coffy , Michel Daumerie
IPC分类号： C08G63/08 , C08F10/06 , C08L23/10 , C08L33/06 , C08L23/08 , C08L51/06 , C08L67/04
CPC分类号： C08L23/12 , B29C45/0001 , B29C47/0004 , B29C49/0005 , B29C51/002 , C08L23/0884 , C08L23/10 , C08L33/068 , C08L51/06 , C08L67/04 , C08L2205/02 , C08L2205/03 , C08L2666/02
摘要： A composition comprising a blend of a polyolefin, polylactic acid, and a reactive modifier. A method of producing an oriented film comprising reactive extrusion compounding a mixture comprising polypropylene, polylactic acid, a reactive modifier to form a compatibilized polymeric blend, casting the compatibilized polymeric blend into a film, and orienting the film. A method of preparing a reactive modifier comprising contacting a polyolefin, a multifunctional acrylate comonomer, and an initiator under conditions suitable for the formation of an epoxy-functionalized polyolefin wherein the epoxy-functionalized polyolefin has a grafting yield of from 0.2 wt. % to 15 wt. %.
摘要翻译：一种组合物，其包含聚烯烃，聚乳酸和反应性改性剂的共混物。一种制备定向膜的方法，其包括将包含聚丙烯，聚乳酸，反应性改性剂的混合物的反应性挤出混合以形成相容的聚合物共混物，将相容的聚合物共混物浇铸成膜，以及使膜定向。一种制备反应性改性剂的方法，包括在适于形成环氧官能化聚烯烃的条件下使聚烯烃，多官能丙烯酸酯共聚单体和引发剂接触，其中环氧官能化聚烯烃的接枝收率为0.2wt。％至15wt。％。

4. 发明申请

US20120296044A1 Polymeric Blends and Methods of Using Same 有权
公开(公告)号：US20120296044A1
公开(公告)日：2012-11-22
申请号：US13562096
申请日：2012-07-30
申请人： Fengkui Li , Tim J. Coffy , Michel Daumerie
发明人： Fengkui Li , Tim J. Coffy , Michel Daumerie
IPC分类号： C08L23/16 , C08L67/04
CPC分类号： C08L67/00 , B29C45/0001 , B29K2105/0088 , B29K2623/10 , B29K2667/046 , C08J5/18 , C08J2323/10 , C08J2467/04 , C08L9/00 , C08L23/08 , C08L23/10 , C08L23/12 , C08L23/16 , C08L51/06 , C08L67/04 , C08L2205/03 , Y10T428/24 , Y10T428/269 , C08L2666/18
摘要： A film comprising a polylactic acid and polypropylene blend having a haze of from about 10% to about 95% and a gloss 45° of from about 50 to about 125. A method of producing an oriented film comprising blending polypropylene and polylactic acid to form a polymeric blend, forming the polymeric blend into a film, and orienting the film. A method of producing an injection molded article comprising blending polypropylene and polylactic acid to form a polymeric blend, injecting the polymeric blend into a mold, and forming the article.

5. 发明申请

US20110269923A1 MULTI-COMPONENT CATALYST SYSTEMS AND POLYMERIZATION PROCESSES FOR FORMING IN-SITU HETEROPHASIC COPOLYMERS AND/OR VARYING THE XYLENE SOLUBLES CONTENT OF POLYOLEFINS 有权
标题翻译：多组分催化剂体系和形成异源共聚物的聚合方法和/或改变聚烯烃的二甲苯溶液含量
公开(公告)号：US20110269923A1
公开(公告)日：2011-11-03
申请号：US13180672
申请日：2011-07-12
申请人： Tim J. Coffy , Michel Daumerie , Kenneth P. Blackmon , William Gauthier , Jun Tian , Joseph Thorman
发明人： Tim J. Coffy , Michel Daumerie , Kenneth P. Blackmon , William Gauthier , Jun Tian , Joseph Thorman
IPC分类号： C08F4/76 , C08F4/42
CPC分类号： C08F10/00 , C08F4/65912 , C08F4/65916 , C08F4/65927 , C08F210/06 , Y10S526/943 , C08F4/65904 , C08F210/16 , C08F2500/12 , C08F2500/05
摘要： Embodiments of the invention generally include multi-component catalyst systems, polymerization processes and heterophasic copolymers formed by the processes. The multi-component catalyst system generally includes a first catalyst component selected from Ziegler-Natta catalyst systems including a diether internal electron donor and a metallocene catalyst represented by the general formula XCpACpBMAn, wherein X is a structural bridge, CpA and CpB each denote a cyclopentadienyl group or derivatives thereof, each being the same or different and which may be either substituted or unsubstituted, M is a transition metal and A is an alkyl, hydrocarbyl or halogen group and n is an integer between 0 and 4. The multi-component catalyst system further includes a second catalyst component generally represented by the formula XCpACpBMAn, wherein X is a structural bridge, CpA and CpB each denote a cyclopentadienyl group or derivatives thereof, each being the same or different and which may be either substituted or unsubstituted, M is a transition metal and A is an alkyl, hydrocarbyl or halogen group and n is an integer between 0 and 4 and wherein the second catalyst component exhibits a higher ethylene response than the first catalyst component.
摘要翻译：本发明的实施方案通常包括通过该方法形成的多组分催化剂体系，聚合方法和多相共聚物。多组分催化剂体系通常包括选自齐格勒 - 纳塔催化剂体系的第一催化剂组分，其包括二醚内电子给体和由通式XCpACpBMAn表示的茂金属催化剂，其中X是结构桥，CpA和CpB各自表示环戊二烯基基团或其衍生物，各自相同或不同，并且可以是取代或未取代的，M是过渡金属，A是烷基，烃基或卤素基团，n是0和4之间的整数。多组分催化剂系统还包括通常由式XCpACpBMAn表示的第二催化剂组分，其中X是结构桥，CpA和CpB各自表示环戊二烯基或其衍生物，各自相同或不同，并且可以是取代或未取代的，M是过渡金属，A是烷基，烃基或卤素基团，n是0至4之间的整数， nd催化剂组分表现出比第一催化剂组分更高的乙烯响应。

6. 发明申请

US20090105433A1 Multi-component catalyst systems and polymerization processes for forming in-situ heterophasic copolymers and/or varying the xylene solubles content of polyolefins 有权
标题翻译：用于形成原位多相共聚物和/或改变二甲苯可溶物的多组分催化剂体系和聚合方法聚烯烃含量
公开(公告)号：US20090105433A1
公开(公告)日：2009-04-23
申请号：US11975014
申请日：2007-10-17
申请人： Tim J. Coffy , Michel Daumerie , Kenneth P. Blackmon , William Gauthier , Jun Tian , Joseph Thorman
发明人： Tim J. Coffy , Michel Daumerie , Kenneth P. Blackmon , William Gauthier , Jun Tian , Joseph Thorman
IPC分类号： C08F4/06 , B01J31/12
CPC分类号： C08F10/00 , C08F4/65912 , C08F4/65916 , C08F4/65927 , C08F210/06 , Y10S526/943 , C08F4/65904 , C08F210/16 , C08F2500/12 , C08F2500/05
摘要： Embodiments of the invention generally include multi-component catalyst systems, polymerization processes and heterophasic copolymers formed by the processes. The multi-component catalyst system generally includes a first catalyst component selected from Ziegler-Natta catalyst systems including a diether internal electron donor and a metallocene catalyst represented by the general formula XCpACpBMAn, wherein X is a structural bridge, CpA and CpB each denote a cyclopentadienyl group or derivatives thereof, each being the same or different and which may be either substituted or unsubstituted, M is a transition metal and A is an alkyl, hydrocarbyl or halogen group and n is an integer between 0 and 4. The multi-component catalyst system further includes a second catalyst component generally represented by the formula XCpACpBMAn, wherein X is a structural bridge, CpA and CpB each denote a cyclopentadienyl group or derivatives thereof, each being the same or different and which may be either substituted or unsubstituted, M is a transition metal and A is an alkyl, hydrocarbyl or halogen group and n is an integer between 0 and 4 and wherein the second catalyst component exhibits a higher ethylene response than the first catalyst component.
摘要翻译：本发明的实施方案通常包括通过该方法形成的多组分催化剂体系，聚合方法和多相共聚物。多组分催化剂体系通常包括选自齐格勒 - 纳塔催化剂体系的第一催化剂组分，其包括二醚内电子给体和由通式XCpACpBMAn表示的茂金属催化剂，其中X是结构桥，CpA和CpB各自表示环戊二烯基基团或其衍生物，各自相同或不同，并且可以是取代或未取代的，M是过渡金属，A是烷基，烃基或卤素基团，n是0和4之间的整数。多组分催化剂系统还包括通常由式XCpACpBMAn表示的第二催化剂组分，其中X是结构桥，CpA和CpB各自表示环戊二烯基或其衍生物，各自相同或不同，并且可以是取代或未取代的，M是过渡金属，A是烷基，烃基或卤素基团，n是0至4之间的整数， nd催化剂组分表现出比第一催化剂组分更高的乙烯响应。

7. 发明授权

US07468339B2 Diketonate complex-derived catalysts useful for preparing polyolefins 失效
标题翻译：用于制备聚烯烃的衍生自二酮衍生物衍生的催化剂
公开(公告)号：US07468339B2
公开(公告)日：2008-12-23
申请号：US11016103
申请日：2004-12-17
申请人： Tim J. Coffy , Steven D. Gray
发明人： Tim J. Coffy , Steven D. Gray
IPC分类号： C08F4/642 , B01J31/02
CPC分类号： C08F10/00 , C07C45/77 , C07C49/92 , C07F3/003 , C08F110/02 , C08F4/651 , C08F4/6557 , C08F4/6548 , C08F2500/18 , C08F2500/12 , C08F2500/24 , C08F2500/07
摘要： An olefin polymerization catalyst may be prepared using a process including contacting a metal compound of the formula M(OR1)2 with a diketone to form a catalyst precursor having the general formula: wherein M is a Group IIA metal; O is oxygen; n=1 or 2; R1, R2, R3, and R4 are the same or different; and are a hydrogen or a substituted or unsubstituted alkyl or aryl moiety having from about 1 to about 20 carbons atoms.
摘要翻译：可以使用包括使式M（OR1）2的金属化合物与二酮接触以形成具有以下通式的催化剂前体的方法来制备烯烃聚合催化剂：其中M是IIA族金属; O是氧; n = 1或2; R1，R2，R3和R4相同或不同; 并且是具有约1至约20个碳原子的氢或取代或未取代的烷基或芳基部分。

8. 发明授权

US06916895B2 Ziegler-Natta catalyst for tuning MWD of polyolefin, method of making, method of using, and polyolefins made therewith 有权
标题翻译：用于调谐聚烯烃的MWD的齐格勒 - 纳塔催化剂，其制备方法，使用方法和由其制备的聚烯烃
公开(公告)号：US06916895B2
公开(公告)日：2005-07-12
申请号：US10687126
申请日：2003-10-16
申请人： Steven D. Gray , Tim J. Coffy
发明人： Steven D. Gray , Tim J. Coffy
IPC分类号： C08F4/654 , C08F4/658 , C08F10/00 , C08F10/02 , C08F110/02
CPC分类号： C08F10/00 , C08F4/6567 , C08F4/6557
摘要： A new synthesis of a Ziegler-Natta catalyst uses a multi-step preparation that includes treating a magnesium dialkoxide compound with halogenating/titanating agents, an organoaluminum preactivating agent, and a heat treatment. The catalyst may be used in the polymerization of olefins, particularly ethylene, to control the molecular weight distribution of the resulting polyolefins.
摘要翻译：齐格勒 - 纳塔催化剂的新合成使用多步骤制备方法，包括用卤化/钛化剂处理二烷氧基镁化合物，有机铝预活化剂和热处理。该催化剂可用于烯烃，特别是乙烯的聚合中，以控制得到的聚烯烃的分子量分布。

9. 发明授权

US06486274B1 Hydrogen response Ziegler-Natta catalyst for narrowing MWD of polyolefin, method of making, method of using, and polyolefins made therewith 有权
标题翻译：用于使聚烯烃的MWD变窄的齐格勒 - 纳塔催化剂，制造方法，使用方法和由此制成的聚烯烃
公开(公告)号：US06486274B1
公开(公告)日：2002-11-26
申请号：US09687688
申请日：2000-10-13
申请人： Steven D. Gray , Tim J. Coffy
发明人： Steven D. Gray , Tim J. Coffy
IPC分类号： C08F4614
CPC分类号： C08F10/00 , C08F4/6567 , C08F4/6557
摘要： A Ziegler-Natta type catalyst having an improved hydrogen response provides for narrowing of the MWD of resulting polyolefins polymerized using such catalyst, with such catalyst generally made by a) contacting a soluble magnesium dialkoxide compound of the general formula Mg(OR″)2 with a halogenating agent capable of exchanging one halogen for one alkoxide to form a reaction product A, where R″ is a hydrocarbyl or substituted hydrocarbyl having from 1 to 20 carbon atoms; b) contacting reaction product A with a first halogenating/titanating agent to form reaction product B; and c) contacting reaction product B with a second halogenating/titanating agent to form a catalyst component; wherein in at least one of steps b) and c), the halogenating/titanating agent is a blend of Ti(OPr)4 and TiCl4. Catalyst components, catalysts, catalyst systems, polyolefin polymers, and methods of forming each are disclosed.
摘要翻译：具有改善的氢气响应的齐格勒 - 纳塔型催化剂使得使用这种催化剂聚合的所得聚烯烃的MWD变窄，通常用以下方法制备的催化剂：a）使通式Mg（OR“）2的可溶性二烷氧基镁化合物与一种能够与一个卤素交换一个醇盐形成反应产物A的卤化剂，其中R“是具有1至20个碳原子的烃基或取代的烃基; b）使反应产物A与第一卤化/钛化剂接触以形成反应产物B; 和c）使反应产物B与第二卤化/钛化剂接触以形成催化剂组分; 其中在步骤b）和c）中的至少一个中，卤化/钛化剂是Ti（OPr）4和TiCl 4的共混物。公开了催化剂组分，催化剂，催化剂体系，聚烯烃聚合物和各种形成方法。

10. 发明申请

US20130197161A1 Injection Molded Article Comprising Polypropylene and Polylactic Acid 有权
标题翻译：包含聚丙烯和聚乳酸的注射成型制品
公开(公告)号：US20130197161A1
公开(公告)日：2013-08-01
申请号：US13795270
申请日：2013-03-12
申请人： Fengkui Li , Tim J. Coffy , Michel Daumerie
发明人： Fengkui Li , Tim J. Coffy , Michel Daumerie
IPC分类号： C08L23/16
CPC分类号： C08L67/00 , B29C45/0001 , B29K2105/0088 , B29K2623/10 , B29K2667/046 , C08J5/18 , C08J2323/10 , C08J2467/04 , C08L9/00 , C08L23/08 , C08L23/10 , C08L23/12 , C08L23/16 , C08L51/06 , C08L67/04 , C08L2205/03 , Y10T428/24 , Y10T428/269 , C08L2666/18
摘要： A film comprising a polylactic acid and polypropylene blend having a haze of from about 10% to about 95% and a gloss 45° of from about 50 to about 125. A method of producing an oriented film comprising blending polypropylene and polylactic acid to form a polymeric blend, forming the polymeric blend into a film, and orienting the film. A method of producing an injection molded article comprising blending polypropylene and polylactic acid to form a polymeric blend, injecting the polymeric blend into a mold, and forming the article.
摘要翻译：一种包含聚乳酸和聚丙烯共混物的薄膜，其雾度为约10％至约95％，光泽度为45°为约50至约125.一种制备定向膜的方法，包括将聚丙烯和聚乳酸共混以形成聚合物共混物，将聚合物共混物形成膜并使膜定向。一种制备注射成型制品的方法，包括将聚丙烯和聚乳酸共混以形成聚合共混物，将聚合物共混物注入模具中，并形成制品。

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